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公开(公告)号：US20190201880A1
公开(公告)日：2019-07-04
申请号：US15857184
申请日：2017-12-28
Applicant: UOP LLC
Inventor： Mark A. Miller , Christopher P. Nicholas , Melissa M. Galey , Mimoza Sylejmani , John Mowat , Collette Nicholas
CPC classification number: B01J29/70 , B01J37/0018 , B01J37/04 , B01J37/08 , C01B39/48 , C01P2002/72 , C01P2002/74 , C01P2002/76 , C01P2004/03 , C01P2004/04 , C07C4/06 , C07C2529/70
Abstract: A new aluminosilicate zeolite designated UZM-50, methods of making the zeolite, and its use as a catalyst in hydrocarbon conversion processes are described. This zeolite is represented by the empirical formula: M+mRrAl1-xExSiyOz where M is selected from the group consisting of hydrogen, sodium, potassium, magnesium, calcium or combinations thereof, R is the organic structure directing agent or agents derived from reactants R1 and R2 where R1 is an amine essentially incapable of undergoing pyramidal inversion and having 7 or fewer carbon atoms, and R2 is a dihaloalkane, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. UZM-50 has utility in various hydrocarbon conversion reactions such as conversion of an aromatic molecule to another aromatic molecule.
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公开(公告)号：US20190030511A1
公开(公告)日：2019-01-31
申请号：US16036709
申请日：2018-07-16
Applicant: UOP LLC
Inventor： Benjamin D. Yuhas , Mark A. Miller , Melissa M. Galey , John P. S. Mowat , Wharton Sinkler
Abstract: A new family of crystalline microporous metallophosphates designated AlPO-78 has been synthesized. These metallophosphates are represented by the empirical formula R+rMm2+EPxSiyOz where R is an organoammonium cation, M is a framework metal alkaline earth or transition metal of valence +2, and E is a trivalent framework element such as aluminum or gallium. The AlPO-78 compositions are characterized by a new unique ABC-6 net structure, and have catalytic properties suitable for carrying out various hydrocarbon conversion processes, as well as characteristics suitable for the efficient adsorption of water vapor in a variety of applications, such as adsorption heat pumps.
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公开(公告)号：US20180099267A1
公开(公告)日：2018-04-12
申请号：US15658681
申请日：2017-07-25
Applicant: UOP LLC
Inventor： Mark A. Miller , Christopher P. Nicholas , Melissa M. Galey , John P. S. Mowat , Wharton Sinkler
CPC classification number: B01J29/70 , B01J20/10 , B01J20/18 , B01J29/86 , B01J35/002 , C01B39/026 , C01B39/12 , C01B39/46 , C01B39/48 , C01P2002/01 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C07C1/20 , C07C2529/70 , Y02P30/42
Abstract: A new crystalline aluminosilicate zeolite comprising a MTT framework has been synthesized that has been designated UZM-55. This zeolite is represented by the empirical formula: M+mRrAl1-xExSiyOz where M represents a metal or metals selected from zinc or Group 1 (IUPAC 1), Group 2 (IUPAC 2), Group 3 (IUPAC 3) or the lanthanide series of the periodic table including sodium, potassium or a combination of sodium and potassium cations, R is an organic structure directing agent or agents derived from reactants R1 and R2 such as where R1 is diisopropanolamine and R2 is a chelating diamine, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. Catalysts made from UZM-55 have utility in various hydrocarbon conversion reactions.
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公开(公告)号：US10654817B2
公开(公告)日：2020-05-19
申请号：US15981148
申请日：2018-05-16
Applicant: UOP LLC
Inventor： Christopher P. Nicholas , Mark A. Miller , Melissa M. Galey , Benjamin D. Yuhas , Sesh Prabhakar
IPC: C07D295/037 , C07D295/023 , C07D295/027
Abstract: Novel 1-oxa-4-azonium cyclohexane salts are described. These compounds can be used as structure directing agents, and they overcome many of the typical problems associated with OSDA synthesis and subsequent zeolite synthesis. Methods for synthesis of the 1-oxa-4-azonium cyclohexane salts from a variety of starting materials are also described. A substituted hydrocarbon is added to water to form a mixture, and a 1-oxa-4-azacyclohexane derivative is then added. The reaction mixture stirred until a solution containing the 1-oxa-4-azonium cyclohexane salt is obtained.
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公开(公告)号：US10597373B2
公开(公告)日：2020-03-24
申请号：US15981435
申请日：2018-05-16
Applicant: UOP LLC
Inventor： Christopher P. Nicholas , Mark A. Miller , Melissa M. Galey , Benjamin D. Yuhas , Sesh Prabhakar
IPC: C07D295/037 , C07D295/023 , C07D295/027
Abstract: Novel 1-oxa-4-azonium cyclohexane salts are described. These compounds can be used as structure directing agents, and they overcome many of the typical problems associated with OSDA synthesis and subsequent zeolite synthesis. Methods for synthesis of the 1-oxa-4-azonium cyclohexane salts from a variety of starting materials are also described. A substituted hydrocarbon is added to water to form a mixture, and a 1-oxa-4-azacyclohexane derivative is then added. The reaction mixture stirred until a solution containing the 1-oxa-4-azonium cyclohexane salt is obtained.
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Patent Agency Ranking
6.发明授权公开(公告)号：US10384989B2
公开(公告)日：2019-08-20
申请号：US15814257
申请日：2017-11-15
Applicant: UOP LLC
Inventor： Rodrigo J. Lobo , Christopher P. Nicholas , Mark A. Miller , Melissa M. Galey
IPC: C07C5/13 , C07C5/27 , B01J29/70 , B01J35/00 , C07C15/08 , G01N23/20 , B01J29/064 , C07C15/073
Abstract: Isomerization processes such as the isomerization of ethylbenzene and xylenes, are catalyzed by the new crystalline aluminosilicate zeolite comprising a novel framework type that has been designated UZM-55. This zeolite is represented by the empirical formula: M+mRAl1-xExSiyOz where M represents a metal or metals selected from zinc or Group 1 (IUPAC 1), Group 2 (IUPAC 2), Group 3 (IUPAC 3) or the lanthanide series of the periodic table including sodium, potassium or a combination of sodium and potassium cations, R is an organic structure directing agent or agents derived from reactants R1 and R2 such as where R1 is diisopropanolamine and R2 is a chelating diamine, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. Catalysts made from UZM-55 have utility in various hydrocarbon conversion reactions.
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公开(公告)号：US10272420B2
公开(公告)日：2019-04-30
申请号：US15658681
申请日：2017-07-25
Applicant: UOP LLC
Inventor： Mark A. Miller , Christopher P. Nicholas , Melissa M. Galey , John P. S. Mowat , Wharton Sinkler
IPC: C01B39/48 , B01J29/70 , C01B39/46 , B01J20/10 , B01J20/18 , B01J29/86 , C01B39/02 , C01B39/12 , C07C1/20 , B01J35/00
Abstract: A new crystalline aluminosilicate zeolite comprising a MTT framework has been synthesized that has been designated UZM-55. This zeolite is represented by the empirical formula: M+mRrAl1-xExSiyOz where M represents a metal or metals selected from zinc or Group 1 (IUPAC 1), Group 2 (IUPAC 2), Group 3 (IUPAC 3) or the lanthanide series of the periodic table including sodium, potassium or a combination of sodium and potassium cations, R is an organic structure directing agent or agents derived from reactants R1 and R2 such as where R1 is diisopropanolamine and R2 is a chelating diamine, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. Catalysts made from UZM-55 have utility in various hydrocarbon conversion reactions.
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公开(公告)号：US20160159655A1
公开(公告)日：2016-06-09
申请号：US14561112
申请日：2014-12-04
Applicant: UOP LLC
Inventor： Christopher P. Nicholas , Mark A. Miller , Melissa M. Galey
CPC classification number: C01B39/32 , B01J29/60 , B01J37/0018 , C01B39/04 , C01B39/48
Abstract: A method for synthesizing a zeolite is described. The method may include the steps of: (a) preparing an aqueous mixture comprising water, a substituted hydrocarbon, and a 1-oxa-4-azacyclohexane derivative; (b) reacting the aqueous mixture; (c) obtaining a solution comprising an organo-1-oxa-4-azoniumcyclohexane compound; (d)) forming a reaction mixture comprising reactive sources of Al, and Si, and the solution; and (e) heating the reaction mixture to form the zeolite.
Abstract translation: 对沸石的合成方法进行说明。 该方法可以包括以下步骤：（a）制备含水，取代的烃和1-氧杂-4-氮杂环己烷衍生物的含水混合物; （b）使含水混合物反应; （c）得到包含有机-1-氧杂-4-氮鎓环己烷化合物的溶液; （d））形成包含Al和Si的反应性源的反应混合物和溶液; 和（e）加热反应混合物以形成沸石。
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公开(公告)号：US10888851B2
公开(公告)日：2021-01-12
申请号：US15857458
申请日：2017-12-28
Applicant: UOP LLC
Inventor： Christopher P. Nicholas , Mark A. Miller , Melissa M. Galey , John Mowat , Collette Nicholas
Abstract: A new aluminosilicate zeolite designated UZM-50, methods of making the zeolite, and its use as a catalyst in hydrocarbon conversion processes are described. This zeolite is represented by the empirical formula: M+mRrAl1−xExSiyOz where M is selected from the group consisting of hydrogen, sodium, potassium, magnesium, calcium or combinations thereof, R is the organic structure directing agent or agents derived from reactants R1 and R2 where R1 is an amine essentially incapable of undergoing pyramidal inversion and having 7 or fewer carbon atoms, and R2 is a dihaloalkane, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. UZM-50 has utility in various hydrocarbon conversion reactions such as conversion of an aromatic molecule to another aromatic molecule.
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公开(公告)号：US20190224656A1
公开(公告)日：2019-07-25
申请号：US16367562
申请日：2019-03-28
Applicant: UOP LLC
Inventor： Mark A. Miller , Christopher P. Nicholas , Melissa M. Galey , John P. S. Mowat , Wharton Sinkler
IPC: B01J29/70 , B01J20/10 , C07C1/20 , B01J20/18 , C01B39/48 , B01J29/86 , C01B39/02 , C01B39/12 , C01B39/46 , B01J35/00
Abstract: A new crystalline aluminosilicate zeolite comprising a new framework has been synthesized that has been designated UZM-55. This zeolite is represented by the empirical formula: M+mRrAl1-xExSiyOz where M represents a metal or metals selected from zinc or Group 1 (IUPAC 1), Group 2 (IUPAC 2), Group 3 (IUPAC 3) or the lanthanide series of the periodic table including sodium, potassium or a combination of sodium and potassium cations, R is an organic structure directing agent or agents derived from reactants R1 and R2 such as where R1 is diisopropanolamine and R2 is a chelating diamine, and E is an element selected from the group consisting of gallium, iron, boron and mixtures thereof. Catalysts made from UZM-55 have utility in various hydrocarbon conversion reactions. The calcined zeolite is used in hydrocarbon conversion reactions.
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