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    Process for preparing organic hydroperoxide containing product
    1.
    发明授权
    Process for preparing organic hydroperoxide containing product 失效
    制备含有机氢过氧化物的产品的方法

    公开(公告)号：US06974888B2

    公开(公告)日：2005-12-13

    申请号：US10757657

    申请日：2004-01-14

    Applicant: Antoon Paul Michael Kremers ,  Eduardus Petrus Simon Schouten ,  Cornelis Willem Adriaan Schram

    Inventor： Antoon Paul Michael Kremers ,  Eduardus Petrus Simon Schouten ,  Cornelis Willem Adriaan Schram

    IPC: C07C407/00 ,  C07B61/00 ,  C07C1/24 ,  C07C15/46 ,  C07C27/00 ,  C07C33/22 ,  C07C409/02 ,  C07C409/08 ,  C07D301/19 ,  C07C15/44 ,  C07C5/327 ,  C07C5/333

    CPC classification number: C07D301/19

    Abstract: Process for preparing alkylaryl hydroperoxide containing product, which process comprises: (a) oxidation of an alkylaryl compound to obtain reaction product containing alkylaryl hydroperoxide, (b) contacting with water at least part of the alkylaryl hydroperoxide containing reaction product obtained in step (a) which reaction product contains less than 0.05 % wt of sodium, (c) separating the product of step (b) into a hydrocarbonaceous phase containing alkylaryl hydroperoxide and an aqueous phase, (d) optionally repeating process steps (b) and (c) one or more times, (e) contacting at least part of the hydrocarbonaceous phase containing alkylaryl hydroperoxide obtained in step (c) or (d) with olefin and catalyst to obtain alkylaryl hydroxide and oxirane compound, and (f) separating at least part of the oxirane compound from the alkylaryl hydroxide.

    Abstract translation: 制备含烷基芳基氢过氧化物的产品的方法，该方法包括：（a）烷基芳基化合物的氧化以获得含有烷基芳基氢过氧化物的反应产物，（b）与步骤（a）获得的至少部分含烷基芳基氢过氧化物的反应产物与水接触， 该反应产物含有小于0.05重量％的钠，（c）将步骤（b）的产物分离成含有烷基芳基氢过氧化物和水相的烃相，（d）任选重复的方法步骤（b）和（c） 或更多次，（e）将步骤（c）或（d）中获得的含有烷基芳基氢过氧化物的至少一部分含烃相与烯烃和催化剂接触以获得烷基芳基氢氧化物和环氧乙烷化合物，和（f）将至少部分 来自烷基芳基氢氧化物的环氧乙烷化合物。

    Control of molecular weight and end group functionality in polymers using unsaturated peroxy compounds as chain transfer agents
    4.
    发明授权
    Control of molecular weight and end group functionality in polymers using unsaturated peroxy compounds as chain transfer agents 失效
    使用不饱和过氧化合物作为链转移剂控制聚合物中的分子量和端基官能度

    公开(公告)号：US6034263A

    公开(公告)日：2000-03-07

    申请号：US468305

    申请日：1995-06-06

    Applicant: Ezio Rizzardo ,  Gordon Francis Meijs ,  San Hoa Thang

    Inventor： Ezio Rizzardo ,  Gordon Francis Meijs ,  San Hoa Thang

    IPC: C07C409/04 ,  C07C409/08 ,  C07C409/00

    CPC classification number: C07C409/04 ,  C07C409/08 ,  C07C409/40

    Abstract: A process for the production of lower molecular weight polymers by free radical polymerization, characterized in that there is added to the polymerization system a compound of the general formula I ##STR1## wherein R.sup.1 is hydrogen, chlorine, an alkyl group, or a group capable of activating the vinylic carbon towards free radical addition;R.sup.2 is hydrogen or an optionally substituted alkyl, alkenyl, aryl, cycloalkenyl or cycloalkyl group or the group --COZ, where Z is R.sup.3 or OR.sup.3, where R.sup.3 is hydrogen or an optionally substituted alkyl, alkenyl or aryl group.X is a hydrogen atom, an alkyl or aryl group, or a halogen, and the two X groups may be the same or different.The invention also includes polymers or oligomers made by the process and novel compounds of the generated formula I as defined above.

    Abstract translation: 一种通过自由基聚合生产低分子量聚合物的方法，其特征在于在聚合体系中加入通式Ⅰ化合物，其中R 1是氢，氯，烷基或能够活化 乙烯基碳向自由基添加; R2是氢或任选取代的烷基，烯基，芳基，环烯基或环烷基或基团-COZ，其中Z是R3或OR3，其中R3是氢或任选取代的烷基，烯基或芳基。 X是氢原子，烷基或芳基或卤素，两个X基可以相同或不同。 本发明还包括通过该方法制备的聚合物或低聚物和如上定义的所产生的式I的新化合物。

    Peroxides
    5.
    发明授权
    Peroxides 失效
    过氧化物

    公开(公告)号：US5981805A

    公开(公告)日：1999-11-09

    申请号：US893693

    申请日：1997-07-11

    Applicant: Fredrick F. Nelson

    Inventor： Fredrick F. Nelson

    IPC: C07C409/08 ,  C07C409/00 ,  C07C409/16 ,  C08K5/14 ,  C07C49/00

    CPC classification number: C07C409/16 ,  C08K5/14

    Abstract: Blends of meta and para isomers of .alpha., .alpha.'-bis(t-butylperoxy) diisopropylbenzene are disclosed as well as methods of producing blends of .alpha., .alpha.'-bis(t-butylperoxy) diisopropylbenzene with desired ratios of meta and para isomers.Additionally, blends of meta and para isomers of .alpha., .alpha.'-bis(t-butylperoxy) diisopropylbenzene and tertiary alkyl cumyl peroxides are disclosed.The peroxides are useful for absorbing in polymers and subsequently crosslinking the polymers. The peroxide blends may be adjusted to have melt points below temperatures at which the polymers become difficult to process during the absorption step because of stickiness.

    Abstract translation: 公开了α，α'-双（叔丁基过氧）二异丙基苯的间位和对位异构体的共混物以及产生α，α'-双（叔丁基过氧）二异丙基苯与所需比例的间位和对位异构体的共混物的方法。 另外，公开了α，α'-双（叔丁基过氧）二异丙基苯和叔烷基枯基过氧化物的间位和对位异构体的共混物。 过氧化物可用于吸收聚合物并随后交联聚合物。 可以调节过氧化物共混物以使熔点低于由于粘性而在吸收步骤期间聚合物难以加工的温度以下。

    Initiated peroxidation of secondary carbon in alkanes and cycloalkanes
    8.
    发明授权
    Initiated peroxidation of secondary carbon in alkanes and cycloalkanes 失效
    在烷烃和环烷烃中引发二次碳的过氧化

    公开(公告)号：US5220075A

    公开(公告)日：1993-06-15

    申请号：US915897

    申请日：1992-07-17

    Applicant: George Ember

    Inventor： George Ember

    IPC: C07C409/04 ,  C07C409/08 ,  C07C409/14

    CPC classification number: C07C407/00 ,  C07C409/14 ,  C07C2101/14

    Abstract: A secondary carbon atom in an alkane, including alkyl groups attached to aromatic rings, or cycloalkane is oxidized by molecular oxygen to the corresponding hydroperoxide in the absence of a catalyst. The oxidation is carried out in the presence of a tertiary hydroperoxide initiator which provides the free radicals needed to maintain the reaction. The amount of tertiary alcohol in the initiator is limited.

    Abstract translation: 在不存在催化剂的情况下，链烷烃中的仲碳原子（包括连接到芳环上的烷基）或环烷烃被分子氧氧化成相应的氢过氧化物。 在叔氢过氧化物引发剂的存在下进行氧化，其提供维持反应所需的自由基。 引发剂中叔醇的量受到限制。

    Propylene oxide-styrene monomer process
    9.
    发明授权
    Propylene oxide-styrene monomer process 失效
    环氧丙烷 - 苯乙烯单体法

    公开(公告)号：US5210354A

    公开(公告)日：1993-05-11

    申请号：US880836

    申请日：1992-05-08

    Applicant: Walter S. Dubner ,  Robert N. Cochran

    Inventor： Walter S. Dubner ,  Robert N. Cochran

    IPC: C07C1/24 ,  C07C15/46 ,  C07C27/12 ,  C07C31/135 ,  C07C407/00 ,  C07C409/08 ,  C07D301/19 ,  C07D303/04

    CPC classification number: C07D301/19 ,  C07C15/46 ,  Y10S585/905

    Abstract: In the co-production oxide and styrene monomer, there is produced a sodium-containing heavy residue stream previously suitable only as a low grade fuel. In accordance with the invention, the heavy residue stream is contacted with aqueous acid, and the resulting mixture is phase separated into an aqueous sodium-containing phase and an organic phase reduced in sodium, and at least a portion of the organic phase reduced in sodium is converted to styrene monomer.

    Abstract translation: 在共生产氧化物和苯乙烯单体中，产生仅仅作为低级燃料的钠盐重残渣物流。 根据本发明，将重质残余物流与酸水溶液接触，将所得混合物相分离为含钠水相，还原为钠的有机相，并将至少部分有机相还原为钠 被转化为苯乙烯单体。

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