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    Calomel (Hg.sub.2 Cl.sub.2) purification process
    1.
    发明授权
    Calomel (Hg.sub.2 Cl.sub.2) purification process 失效
    甘汞（Hg2Cl2）净化过程

    公开(公告)号：US5601795A

    公开(公告)日：1997-02-11

    申请号：US551038

    申请日：1995-10-31

    申请人： Donald L. Ball ,  Richard S. Varley

    发明人： Donald L. Ball ,  Richard S. Varley

    IPC分类号： C01G13/04 ,  C01B9/00 ,  C01G13/00

    CPC分类号： C01G13/04

    摘要： This invention is directed to a novel method for purifying calomel (Hg.sub.2 Cl.sub.2). More particularly, this invention pertains to a novel process for treating impure calomel (Hg.sub.2 Cl.sub.2) to produce a highly purified calomel product that passes American Chemical Society requirements for calomel assay and mercuric chloride contamination. A process for treating impure calomel to produce purified calomel comprising: (a) incorporating impure calomel into an aqueous slurry; (b) oxidizing the aqueous slurry with an oxidizing agent to form soluble mercuric chloride; (c) filtering the aqueous slurry containing soluble mercuric chloride into liquid and solid components; (d) heating the liquid component to greater than 70.degree. C; (e) treating the liquid component with a reducing agent to precipitate purified calomel; and (f) separating the precipitated purified calomel from the filtrate.

    摘要翻译： 本发明涉及一种纯化甘汞（Hg2Cl2）的新方法。 更具体地说，本发明涉及一种用于处理不纯的甘汞（Hg2Cl2）以产生高度纯化的甘汞产品的新方法，其通过美国化学学会对甘汞测定和氯化汞氯化物污染的要求。 一种用于处理不纯的甘汞以产生纯化的甘汞的方法，包括：（a）将不纯的甘汞混合到含水浆料中; （b）用氧化剂氧化含水浆料以形成可溶性氯化汞; （c）将含有可溶性氯化汞的含水浆料过滤成液体和固体组分; （d）将液体组分加热到大于70℃; （e）用还原剂处理液体组分以沉淀纯化的甘汞; 和（f）从滤液中分离沉淀的纯化甘汞。

    Apparatus for producing halide particles
    5.
    发明授权
    Apparatus for producing halide particles 失效
    用于生产卤化物颗粒的装置

    公开(公告)号：US4010000A

    公开(公告)日：1977-03-01

    申请号：US570777

    申请日：1975-04-23

    申请人： Scott Anderson

    发明人： Scott Anderson

    IPC分类号： C01D3/20 ,  C01F17/00 ,  C01G1/06 ,  C01G13/04 ,  H01J61/12 ,  B01J1/00

    CPC分类号： H01J61/125 ,  C01D3/20 ,  C01F17/0031 ,  C01G1/06 ,  C01G13/04 ,  C01P2004/61 ,  C01P2006/40 ,  C01P2006/80

    摘要： Apparatus for producing purified metal halides, such as sodium iodide and mixtures of sodium iodide and mixtures of sodium iodide with scandium iodide, of accurately controlled particle size, particularly useful as a vaporizable fill for high pressure discharge devices. The apparatus may include means for evaporating volatiles from the solid impure metal halide, melting the impure halide, passing hydrogen, hydrogen halide, hydrogen and halogen, or mixtures thereof through the halide, and then passing the molten halide through a vibrating discharge conduit or nozzle into an inert quenching atmosphere to form the particles of purified halide.

    摘要翻译： 用于制备精确控制粒度的纯化金属卤化物，例如碘化钠和碘化钠与碘化钠与碘化钪的混合物的混合物的装置，其特别用作高压放电装置的可蒸发填充物。 该装置可以包括用于从固体不纯的金属卤化物蒸发挥发物，熔化不纯的卤化物，使氢，卤化氢，氢和卤素或其混合物通过卤化物蒸发的装置，然后使熔融的卤化物通过振动的排放导管或喷嘴 进入惰性猝灭气氛中以形成纯化的卤化物颗粒。

    Process for the removal of mercury from gases
    6.
    发明授权
    Process for the removal of mercury from gases 失效
    从气体中去除汞的过程

    公开(公告)号：US3838190A

    公开(公告)日：1974-09-24

    申请号：US21680772

    申请日：1972-01-10

    申请人： NORSKE ZINKKOMPANI AS

    发明人： EYSTEIN I ,  DYVIK F ,  BIRKE L ,  JEBENS A

    IPC分类号： B01D53/64 ,  C01G13/04 ,  B01D53/34

    CPC分类号： B01D53/64 ,  C01G13/04

    摘要： REMOVAL OF MERCURY FROM GASES, IN PARTICULAR GASES FROM COMBUSTION OR ROASTING, IS ACHIEVED BY WASHING THE GASES WITH SULPHURIC ACID OF AT LEAST 5% HAVING A TEMPERATURE OF 60 TO 180* C. THE WASHING ACID AND THE GASES CONTAIN CHLORIDE OR CHLORINE COMPOUNDS OR BOTH CHLORINE AND CHLORINE COMPOUNDS IN SUCH AN AMOUNT THAT THE ATOMIC RATIO C1/HG IS AT LEAST 1:1. PRACTICALLY ALL MERCURY AND OTHER MERCURY COMPOUNDS ARE CONVERTED TO MERCURY CHLORIDES WHICH ARE SEPARATED BY CONDENSATION IN A SUCCEEDING COOLING OF THE GAS.

    Process relating to ultra-pure metal halide particles
    7.
    发明授权
    Process relating to ultra-pure metal halide particles 失效
    与超纯金属卤化物颗粒相关的工艺

    公开(公告)号：US3676534A

    公开(公告)日：1972-07-11

    申请号：US3676534D

    申请日：1969-09-26

    申请人： ANDERSON SCOTT

    发明人： ANDERSON SCOTT

    IPC分类号： C01D3/20 ,  C01F17/00 ,  C01G1/06 ,  C01G13/04 ,  B01J2/18

    CPC分类号： C01G1/06 ,  C01D3/20 ,  C01F17/0031 ,  C01G13/04 ,  C01P2004/61 ,  C01P2006/40 ,  C01P2006/80

    摘要： Compositions are described including free-flowing particles of controlled size of purified metal halides such as sodium iodide and mixtures of sodium iodide with scandium iodide. These ultrapure metal halide particles are particularly useful as a vaporizable fill disposed within an arc tube of a high pressure electric discharge device. The preparation and identification of the coordination entity Na ScI 4 (III) is also described. The process for producing purified metal halides of accurately controlled particle size includes evaporating volatiles from the solid impure metal halide, melting the impure halide, passing hydrogen, hydrogen halide, hydrogen and halogen, or mixtures thereof through the halide, and then passing the molten halide through a vibrating discharge conduit or nozzle into an inert quenching atmosphere to form the particles of purified halide.

    摘要翻译： 描述了包含自由流动的精制金属卤化物如碘化钠和碘化钠与碘化钪的混合物的自由流动颗粒的组合物。 这些超纯金属卤化物颗粒特别可用作设置在高压放电装置的电弧管内的可蒸发填充物。 还描述了配位实体Na + ScI 4（III）的制备和鉴定。 用于生产精确控制颗粒尺寸的精制金属卤化物的方法包括从固体不纯的金属卤化物蒸发挥发物，熔化不纯的卤化物，使氢，卤化氢，氢和卤素或其混合物通过卤化物，然后使卤化物 通过振动排放导管或喷嘴进入惰性淬火气氛中以形成纯化的卤化物颗粒。