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    Method of purifying metal salt, method of deacidifying titanium material and method of producing the same
    1.
    发明申请
    Method of purifying metal salt, method of deacidifying titanium material and method of producing the same 审中-公开
    纯化金属盐的方法，钛材料脱酸方法及其制备方法

    公开(公告)号：US20050139483A1

    公开(公告)日：2005-06-30

    申请号：US10509250

    申请日：2003-04-21

    申请人： Shinji Shimosaki

    发明人： Shinji Shimosaki

    IPC分类号： C01D3/20 ,  C01F11/32 ,  C22B9/10 ,  C22B34/12 ,  C25C3/28

    CPC分类号： C01D3/20 ,  C01F11/32 ,  C22B34/1295

    摘要： A purification method of a metal salt which comprises bringing a metal salt formed by melting an alkali metal salt, an alkaline earth metal salt or a mixture thereof into contact with titanium or the like, thereby adsorbing impurities in the metal salt, a deoxidization method by melting metallic calcium into a molten product of the metal salt purified by the purification method and bringing the same into contact with a titanium material, and a production method of the titanium material which comprises conducting molten salt electrolysis by using the molten product of the purified metal salt for an electrolytic bath. Using the purification or production method the molten metal salt can be purified simply and conveniently at good efficiency. Then, use of the purified metal salt can minimize contamination caused by the metal impurities in the molten salt and the titanium material of high quality can be produced.

    摘要翻译： 一种金属盐的净化方法，其特征在于，将通过使碱金属盐，碱土金属盐或其混合物熔融而形成的金属盐与钛等接触，从而吸附金属盐中的杂质，脱氧法由 将金属钙熔融成通过纯化方法纯化的金属盐的熔融产物，并使其与钛材料接触，以及钛材料的制造方法，其包括通过使用纯化金属的熔融产物进行熔融盐电解 盐为电解浴。 使用纯化或生产方法，可以以良好的效率简单方便地纯化熔融金属盐。 然后，使用纯化的金属盐可以最小化由熔融盐中的金属杂质引起的污染，并且可以生产高质量的钛材料。

    Purification of alkali metal halides
    2.
    发明授权
    Purification of alkali metal halides 失效
    碱金属卤化物的纯化

    公开(公告)号：US3932597A

    公开(公告)日：1976-01-13

    申请号：US587746

    申请日：1975-06-17

    申请人： Ricardo C. Pastor

    发明人： Ricardo C. Pastor

    IPC分类号： C01D3/20 ,  C01D3/04 ,  C01D3/10 ,  C01D3/12

    CPC分类号： C01D3/20

    摘要： A new process or method has been developed whereby the purity of metal halides, prepared by conventional methods, can be significantly upgraded. The process, which includes a scrubbing of metal halides with a halide-source species in the vapor phase, has been shown to be effective not only in reducing the concentration of oxyanion impurities and volatile cation halide impurities, but effective in reducing hydroxyl ion (OH.sup.-) contaminations as well.Metal halides purified by this method are particularly useful as starting materials for growing optically pure metal halide crystals.

    摘要翻译： 已经开发了一种新方法或方法，由此通过常规方法制备的金属卤化物的纯度可以显着提高。 已经显示包括在气相中用卤化物源物质洗涤金属卤化物的方法不仅有效地降低氧阴离子杂质和挥发性阳离子卤化物杂质的浓度，而且有效地还原羟基离子（OH < - >）污染。

    Corrosion-resistant coolant salt and method for making same
    3.
    发明授权
    Corrosion-resistant coolant salt and method for making same 有权

    公开(公告)号：US12049408B2

    公开(公告)日：2024-07-30

    申请号：US16571414

    申请日：2019-09-16

    申请人： TerraPower, LLC

    发明人： Brian C. Kelleher

    IPC分类号： C01F5/30 ,  C01D3/20

    CPC分类号： C01F5/30 ,  C01D3/20

    摘要： This document describes a method for reducing the corrosivity of certain magnesium salts. The salt product resulting from the method exhibits reduced corrosion of steels that come into contact with the salt relative to salt compositions that are not so treated. This makes such treated salts more efficient coolant salts as they will require less equipment replacement over time. The method uses magnesium metal to reduce unwanted impurities in the salts the reduced impurities are then removed as either gas or precipitate from the now purified salt. Without being bound to one particular theory, it is believed that the reduction of the level of impurities in the salt results in a salt with substantially reduced corrosiveness to steel.

    Process for producing anhydrous magnesium chloride and suitable apparatus
    5.
    发明授权
    Process for producing anhydrous magnesium chloride and suitable apparatus 失效
    生产无水氯化镁的方法和合适的装置

    公开(公告)号：US4302433A

    公开(公告)日：1981-11-24

    申请号：US792911

    申请日：1977-05-02

    申请人： Richard B. Stein

    发明人： Richard B. Stein

    IPC分类号： C01D3/20 ,  C01F5/32

    CPC分类号： C01D3/20 ,  C01F5/32

    摘要： Substantially anhydrous magnesium chloride is prepared through the chlorination of a hydrated magnesium chloride by melting the hydrated chloride, feeding that molten material to a bed of carbonaceous material so that it flows downwardly therethrough and simultaneously feeding a mixture of chlorine and air to the bed of carbonaceous material so that it flows upwardly therethrough countercurrent to the molten material, until magnesium chloride of the desired state of purity is obtained, and the purified magnesium chloride is then recovered.

    摘要翻译： 通过熔化水合氯化物将水合氯化镁熔化，将熔融材料送入碳质材料床，使其向下流过并同时将氯和空气的混合物送入碳质床层中制备基本上无水的氯化镁 材料，使得其与熔融材料逆流向上流动，直到获得所需纯度的氯化镁，然后回收纯化的氯化镁。

    Ultra-pure metal halide particles
    6.
    发明授权
    Ultra-pure metal halide particles 失效
    超纯金属卤化物颗粒

    公开(公告)号：US3948793A

    公开(公告)日：1976-04-06

    申请号：US259858

    申请日：1972-06-05

    申请人： Scott Anderson

    发明人： Scott Anderson

    IPC分类号： C01D3/20 ,  C01F17/00 ,  C01G1/06 ,  C01G13/04 ,  H01J61/12 ,  H01J7/18 ,  H01J35/20 ,  H01K1/56

    CPC分类号： H01J61/125 ,  C01D3/20 ,  C01F17/0031 ,  C01G1/06 ,  C01G13/04 ,  C01P2004/61 ,  C01P2006/40 ,  C01P2006/80

    摘要： Compositions are described including free-flowing particles of controlled size of purified metal halides such as sodium iodide and mixtures of sodium iodide with scandium iodide. These ultra-pure metal halide particles are particularly useful as a vaporizable fill disposed within an arc tube of a high pressure electric discharge device. The preparation and identification of the coordination entity Na.sup.+ScI.sub.4 .sup.- (III) is also described. The apparatus for producing purified metal halides of accurately controlled particle size includes means for evaporating volatiles from the solid impure metal halide, melting the impure halide, passing hydrogen, hydrogen halide, hydrogen and halogen, or mixtures thereof through the halide, and then passing the molten halide through a vibrating discharge conduit or nozzle into an inert quenching atmosphere to form the particles of purified halide.

    摘要翻译： 描述了包含自由流动的精制金属卤化物如碘化钠和碘化钠与碘化钪的混合物的自由流动颗粒的组合物。 这些超纯金属卤化物颗粒特别可用作设置在高压放电装置的电弧管内的可蒸发填充物。 还描述了配位体Na + ScI4 - （III）的制备和鉴定。 用于制备精确控制粒度的精制金属卤化物的装置包括用于从固体不纯的金属卤化物蒸发挥发物，熔化不纯的卤化物，使氢，卤化氢，氢和卤素或其混合物通过卤化物，然后通过 熔融卤化物通过振动排放导管或喷嘴进入惰性淬火气氛中以形成纯化的卤化物颗粒。

    PROCESS FOR RECOVERING SULFATE AND CHLORIDE SALTS FROM WASTEWATER, MIXED SALTS, AND BRINES
    8.
    发明申请
    PROCESS FOR RECOVERING SULFATE AND CHLORIDE SALTS FROM WASTEWATER, MIXED SALTS, AND BRINES 有权
    从废水，混合物和盐水中回收硫酸盐和氯化物废水的方法

    公开(公告)号：US20160280571A1

    公开(公告)日：2016-09-29

    申请号：US15079174

    申请日：2016-03-24

    申请人： VEOLIA WATER TECHNOLOGIES, INC.

    发明人： Benjamin S. Mack ,  Timothy J. Rittof

    IPC分类号： C02F1/52 ,  C02F1/04 ,  C01D3/20 ,  C02F1/44 ,  C01D5/16 ,  C01D3/16

    CPC分类号： C02F1/52 ,  B01D9/0004 ,  B01D9/0031 ,  B01D9/0059 ,  C01B17/96 ,  C01D3/08 ,  C01D3/16 ,  C01D3/20 ,  C01D5/16 ,  C02F1/04 ,  C02F1/048 ,  C02F1/283 ,  C02F1/441 ,  C02F2001/5218 ,  C02F2101/101 ,  C02F2101/12 ,  C02F2101/30 ,  C02F2103/10 ,  C02F2103/18 ,  C02F2103/365 ,  C02F2209/02

    摘要： A process is described for recovering alkali-chloride and alkali-sulfate salts from a salt solution. The salt solution comprises alkali metal, chloride and sulfate ions and is directed to a hydrous salt crystallization unit which crystallizes hydrated sulfate salts that comprise sulfate and at least one alkali metal. A purged solution from the hydrous salt crystallization unit is directed to a chloride salt crystallization unit while the hydrated sulfate salt crystals are melted to form an aqueous sulfate solution which is directed to a sulfate crystallization unit. Anhydrous sulfate salts are crystallized from the aqueous sulfate solution to form sulfate salt crystals comprising sulfate and at least one alkali metal. In the chloride salt crystallization unit, chloride salt is crystallized to form chloride salt crystals. A purge from the chloride salt crystallization unit is directed to the hydrous salt crystallization unit.

    摘要翻译： 描述了从盐溶液中回收碱金属氯化物和碱金属硫酸盐的方法。 盐溶液包含碱金属，氯化物和硫酸根离子，并被引导到水合盐结晶单元，其结晶含硫酸盐和至少一种碱金属的水合硫酸盐。 来自含水盐结晶单元的清洗溶液被引导至氯化物盐结晶单元，同时将水合硫酸盐晶体熔化以形成硫酸盐结晶单元的硫酸盐水溶液。 无水硫酸盐从硫酸水溶液中结晶形成硫酸盐晶体，其包含硫酸盐和至少一种碱金属。 在氯化物盐结晶单元中，氯化物盐结晶形成氯化物盐晶体。 来自氯化物盐结晶单元的吹扫被引导到含水盐结晶单元。

    High pressure light emitting electric discharge device
    9.
    发明授权
    High pressure light emitting electric discharge device 失效
    高压发光放电装置

    公开(公告)号：US4023059A

    公开(公告)日：1977-05-10

    申请号：US570778

    申请日：1975-04-23

    申请人： Scott Anderson

    发明人： Scott Anderson

    IPC分类号： C01D3/20 ,  C01F17/00 ,  C01G1/06 ,  C01G13/04 ,  H01J61/12 ,  H01J61/18

    CPC分类号： C01D3/20 ,  C01F17/0031 ,  C01G1/06 ,  C01G13/04 ,  H01J61/125 ,  C01P2004/61 ,  C01P2006/40 ,  C01P2006/80

    摘要： Compositions are described including free-flowing particles of controlled size of purified metal halides such as sodium iodide and mixtures of sodium iodide with scandium iodide. These ultra-pure metal halide particles are particularly useful as a vaporizable fill disposed within an arc tube of a high pressure electric discharge device. The preparation and identification of the coordination entity Na.sup.+ScI.sub.4.sup.- (III) is also described. The apparatus for producing purified metal halides of accurately controlled particle size includes means for evaporating volatiles from the solid impure metal halide, melting the impure halide, passing hydrogen, hydrogen halide, hydrogen and halogen, or mixtures thereof through the halide, and then passing the molten halide through a vibrating discharge conduit or nozzle into an inert quenching atmosphere to form the particles of purified halide.

    摘要翻译： 描述了包含自由流动的精制金属卤化物如碘化钠和碘化钠与碘化钪的混合物的自由流动颗粒的组合物。 这些超纯金属卤化物颗粒特别可用作设置在高压放电装置的电弧管内的可蒸发填充物。 还描述了配位体Na + ScI4 - （III）的制备和鉴定。 用于制备精确控制粒度的精制金属卤化物的装置包括用于从固体不纯的金属卤化物蒸发挥发物，熔化不纯的卤化物，使氢，卤化氢，氢和卤素或其混合物通过卤化物，然后通过 熔融卤化物通过振动排放导管或喷嘴进入惰性淬火气氛中以形成纯化的卤化物颗粒。

    Sodium chloride melt refining process
    10.
    发明授权
    Sodium chloride melt refining process 失效
    氯化钠熔炼精制工艺

    公开(公告)号：US3840651A

    公开(公告)日：1974-10-08

    申请号：US28667272

    申请日：1972-09-06

    申请人： CARGILL INC

    发明人： IRELAND D

    IPC分类号： C01D3/20 ,  C01D3/14 ,  C01D3/16

    CPC分类号： C01D3/20 ,  Y10S423/12

    摘要： 1. A PROCESS FOR MELT REFINING SODIUM CHLORIDE TO PROVIDE A HIGH PURITY SALT PRODUCT WHICH IS SUBSTANTIALLY FREE OF CALCIUM, MAGNESIUM, AND SULFATE IMPURITIES, COMPRISING CARRYING OUT IN COMBINATION THE STEPS OF (A) HEATING THE SODIUM CHLORIDE ABOVE ITS MELTING TEMPERATURE TO PROVIDE A SALT MELT, (B) INTRODUCING INTO SAID MELT A SUFFICIENT QUANTITY OF AN ALKALI PRECIPITATION AGENT SELECTED FROM THE GROUP CONSISTING OF ALKALI HYDROXIDES, CARBONATES, SILICATES AND PHOSPHARES, TO PRECIPITATE CALCIUM AND MAGNESIUM NESIUM IMPURITIES IN SAID MELT, (C) REMOVING PRECIPITATED CALCIUM AND MAGNESIUM IMPURITIES FROM SAID MELT, (D) CONTACTING SAID MELT WITH ELEMENTAL CARBON TO REMOVE SULFATE IMPURITY FROM SAID MELT, (E) MAINTAINING SAID SALT MELT IN CONTACT WITH SAID CARBON FOR A PREDETERMINED TIME OF EFFECT THE DESIRED LEVEL OF SULFATE REMOVAL, (F) REMOVING ANY REMAINING CARBON FROM THE SALT MELT AFTER TH DESIRED LEVEL OF SULFATE REMOVAL HAS BEEN OBTAINED, AND (G) SUBSEQUENTLY COOLING AND SOLIDIFYING THE SALT MELT TO PROVIDE A HIGH PURITY, SOLID SALT PRODUCT.