公开(公告)号：US07029503B2

公开(公告)日：2006-04-18

申请号：US10476471

申请日：2002-05-08

Applicant: Junji Odani ,  Eiichi Ogawa ,  Yasuo Shirasaki

Inventor： Junji Odani ,  Eiichi Ogawa ,  Yasuo Shirasaki

IPC: C09B62/09 ,  C09B62/085 ,  C09B67/22 ,  D06P3/82 ,  D06P3/66

CPC classification number: C09B67/0048 ,  C09B62/09 ,  C09B67/0045 ,  Y10S8/918

Abstract: The present invention provides a disazo compound which in a free acid form is represented by the formula (1) and which has high ability to dye cellulosic fibers and attains efficient dyeing with satisfactory reproducibility; and a method of dyeing cellulosic fibers with the compound. Also provided are: a reactive dye composition comprising a compound represented by the formula (1) and a specific red reactive dye and/or a specific blue reactive dye; and a method of dyeing cellulosic fibers with the composition. In the formula, R1 and R3 each represents hydrogen atom or methoxy group; R2 and R4 each represents hydrogen atom, methyl group, acetylamino group, ureido group, etc.; and m is 2 or 3.

Abstract translation: 本发明提供一种游离酸形式的双偶氮化合物，其由式（1）表示，并且具有高的染色纤维素纤维的能力，并以令人满意的重现性得到有效的染色; 以及用该化合物染色纤维素纤维的方法。 还提供了：包含由式（1）表示的化合物和特定的红色活性染料和/或特定的蓝色活性染料的活性染料组合物; 以及用该组合物染色纤维素纤维的方法。 在该式中，R 1和R 3各自表示氢原子或甲氧基; R 2和R 4各自表示氢原子，甲基，乙酰基氨基，脲基等; m为2或3。

公开(公告)号：US5942011A

公开(公告)日：1999-08-24

申请号：US11146

申请日：1998-02-02

Applicant: Yasuo Shirasaki ,  Eiichi Ogawa ,  Yoshikazu Aizawa ,  Shigemitsu Yabe

Inventor： Yasuo Shirasaki ,  Eiichi Ogawa ,  Yoshikazu Aizawa ,  Shigemitsu Yabe

IPC: D06P1/16 ,  D06P1/62 ,  D06P3/54 ,  D06P3/82

CPC classification number: D06P1/628 ,  D06P3/54 ,  D06P3/8238 ,  Y10S8/922

Abstract: This invention relates to a method of dyeing fibers containing polyester fibers characterized by their exhaustion dyeing in an alkaline aqueous medium, and a dyeing assistant for fibers containing polyester fibers which is effective for carrying out the dyeing method, and which is characterized by containing a compound represented by formula (I) ##STR1## (where R is H or CH3, n is 1 to 3, and X is H, an alkali metal, or an organic base).Moreover, this invention relates to a dyed product of fibers containing polyester fibers as dyed by the method mentioned above.

Abstract translation: PCT No.PCT / JP97 / 01961 Sec。 371日期1998年2月2日 102（e）1998年2月2日PCT 1997年6月9日PCT公布。 第WO97 / 46752号公报 日期1997年12月11日本发明涉及一种染色含有聚酯纤维的纤维的方法，其特征在于其在碱性水性介质中的染色染色，以及对于进行染色方法有效的含有聚酯纤维的纤维的染色助剂， 其特征在于含有由式（I）表示的化合物（其中R为H或CH 3，n为1至3，X为H，碱金属或有机碱）。 此外，本发明涉及通过上述方法染色的含有聚酯纤维的纤维的染色产品。

公开(公告)号：US06653454B1

公开(公告)日：2003-11-25

申请号：US09889189

申请日：2002-10-01

Applicant: Mariko Umeda ,  Hideshiro Nomura ,  Yasuo Shirasaki ,  Eiichi Ogawa

Inventor： Mariko Umeda ,  Hideshiro Nomura ,  Yasuo Shirasaki ,  Eiichi Ogawa

IPC: C09B5610

CPC classification number: C09B50/06

Abstract: The present invention relates to a novel blue dye compound represented by Formula (1) as shown below, which can be synthesized without a dianisidine compound used for a raw material and can dye a cellulosic high molecular material to provide the blue dyed product that has a high color value, a good build-up and various kinds of good fastness; a method for dyeing a cellulosic high molecular material by using the same; and a cellulosic high molecular material dyed with the same. A formazan compound represented by (In Formula (1), R1 is hydrogen, sulfo, hydroxy, chloro, methoxy, carboxyl or alkyl; either of R2 and R3 is hydrogen and the other is sulfo; X is morpholino, 2-hydroxyethylamino or bis(2-hydroxyethyl)amino; and Y is a phenylene diimino represented by Formula (2) as shown below (In Formula (2), R4 is sulfo or carboxyl)) or the salt thereof.

Abstract translation: 本发明涉及如下所示的由式（1）表示的新型蓝色染料化合物，其可以不用用于原料的二叠氮化合物合成，并且可以染色纤维素高分子材料以提供具有 高色值，良好的贴合性和各种良好的牢度; 通过使用该方法染色纤维素高分子材料的方法; 由式（1）表示的甲az化合物，R 1为氢，磺基，羟基，氯，甲氧基，羧基或烷基; R2和R3中的任一个为氢，另一个为 磺酰基; X是吗啉代，2-羟乙基氨基或双（2-羟乙基）氨基; Y是如下所示的由式（2）表示的亚苯基二亚氨基（在式（2）中，R 4是磺基或羧基））或盐 其中。

公开(公告)号：US6086640A

公开(公告)日：2000-07-11

申请号：US367156

申请日：1999-08-09

Applicant: Toru Tabei ,  Eiichi Ogawa ,  Shin-ichi Namba

Inventor： Toru Tabei ,  Eiichi Ogawa ,  Shin-ichi Namba

IPC: C09B50/00 ,  B05D7/14 ,  C08B13/00 ,  C08L1/00 ,  C08L1/26 ,  C09B62/04 ,  C09B67/00 ,  C09B69/10 ,  C09D5/29 ,  C09D5/36 ,  C09D5/38 ,  C09D101/00 ,  C09D101/32 ,  C09K19/00 ,  C09K19/38 ,  D06P3/40 ,  C09B45/00

CPC classification number: C09B62/046 ,  C08B13/00 ,  C09B67/0098 ,  C09D5/36 ,  C09K19/00 ,  C09K19/3819 ,  Y10S8/918

Abstract: For dyeing (printing, for example) cellulose fibers with a reactive dye, a blue compound is greatly desired, the blue compound being capable of generating a product dyed in blue at excellent dyeing reproducibility and with good light fastness and superior fastness against chlorine water, involving less staining of white area. The invention relates to a formazan compound in a free acid form as represented by the following formula I, a dyeing method of cellulose fibers using the same and a final dyed product prepared by the method, characterized in that the compound, the method and the product are suitable so as to overcome the problem.Formula I ##STR1## (wherein R represents hydrogen, sulfo group, hydroxyl group, halogen, a C1-C4 alkyl group, a C1-C4 alkoxyl group or carboxyl group; and M represents copper or nickel.)

Abstract translation: PCT No.PCT / JP98 / 00748 Sec。 371日期1999年8月9日 102（e）日期1999年8月9日PCT提交1998年2月25日PCT公布。 公开号WO98 / 38252 日期1998年9月3日对于用活性染料染色（例如印刷）纤维素纤维，蓝色化合物是非常需要的，蓝色化合物能够以优异的染色重现性和良好的耐光性和优异的颜色产生蓝色染色的产品 耐氯水牢度，涉及染色较少的白色区域。 本发明涉及以下式I表示的游离酸形式的甲an化合物，使用其的纤维素纤维的染色方法和通过该方法制备的最终染色产物，其特征在于，化合物，方法和产物 是适合的，以克服这个问题。 式I（其中R表示氢，磺基，羟基，卤素，C1-C4烷基，C1-C4烷氧基或羧基; M表示铜或镍。

公开(公告)号：US5545281A

公开(公告)日：1996-08-13

申请号：US217973

申请日：1994-03-25

Applicant: Koji Matsui ,  Mitsuru Kimura ,  Kazuaki Utsumi ,  Eiichi Ogawa ,  Hiroshi Komano ,  Toshimi Aoyama

Inventor： Koji Matsui ,  Mitsuru Kimura ,  Kazuaki Utsumi ,  Eiichi Ogawa ,  Hiroshi Komano ,  Toshimi Aoyama

IPC: H01L21/60 ,  H01L21/603 ,  H01L21/98 ,  H05K3/00 ,  H05K3/28 ,  H05K3/32 ,  H05K3/46 ,  B32B31/12 ,  B32B31/20 ,  B32B31/28 ,  H05K3/30

CPC classification number: H05K3/4617 ,  H01L24/81 ,  H01L25/50 ,  H01L2224/13111 ,  H01L2224/13144 ,  H01L2224/16 ,  H01L2224/2929 ,  H01L2224/293 ,  H01L2224/81193 ,  H01L2224/81801 ,  H01L2224/83101 ,  H01L2224/83851 ,  H01L2924/01005 ,  H01L2924/01006 ,  H01L2924/01013 ,  H01L2924/01019 ,  H01L2924/0102 ,  H01L2924/01024 ,  H01L2924/01029 ,  H01L2924/01033 ,  H01L2924/01042 ,  H01L2924/01049 ,  H01L2924/0105 ,  H01L2924/01073 ,  H01L2924/01079 ,  H01L2924/01082 ,  H01L2924/014 ,  H01L2924/07811 ,  H01L2924/09701 ,  H01L2924/14 ,  H01L2924/3025 ,  H05K2203/0278 ,  H05K3/0023 ,  H05K3/28 ,  H05K3/328 ,  Y10T29/49126 ,  Y10T29/4913 ,  Y10T29/49144

Abstract: An integrated circuit connecting method that includes connecting electrode pads on an integrated circuit device to electrode terminals on a base with metal bumps interposed, the electrode terminals being formed in registry with the electrode pads. The method includes the steps of forming metal bumps on a surface of at least one of the electrode pads and the electrode terminals; covering the surface on at least one of the integrated circuit device side and the base side with a resin that cures upon exposure to active energy rays; patterning the resin to strip selectively the coating of the resin over one of the electrode pads and the electrode terminals; bringing the electrode pads and the electrode terminals into a face-to-face relationship, allowing the metal bumps to contact one of the opposing electrode pads and electrode terminals, performing thermocompressing so that the resin coating will adhere closely to one of the integrated circuit device and the base while, at the same time, the electrode pads are connected to the electrode terminals with the metal bumps interposed; and performing at least one of heat treatment and exposure to active energy rays.

Abstract translation: 一种集成电路连接方法，其包括将集成电路器件上的电极焊盘连接到基底上的电极端子，并插入金属凸块，所述电极端子与电极焊盘对准形成。 该方法包括在至少一个电极焊盘和电极端子的表面上形成金属凸块的步骤; 在集成电路器件侧和基底侧的至少一个上覆盖表面，该树脂在暴露于活性能量射线时固化; 图案化树脂以在电极焊盘和电极端子之一上选择性地剥离树脂涂层; 使电极焊盘和电极端子成为面对面的关系，允许金属凸块接触相对的电极焊盘和电极端子之一，进行热压缩，使得树脂涂层将紧密地粘附到集成电路器件 并且同时将电极焊盘连接到电极端子，同时插入金属凸块; 并进行热处理和暴露于活性能量射线中的至少一种。

公开(公告)号：US5318651A

公开(公告)日：1994-06-07

申请号：US978720

申请日：1992-11-19

Applicant: Koji Matsui ,  Mitsuru Kimura ,  Kazuaki Utsumi ,  Eiichi Ogawa ,  Hiroshi Komano ,  Toshimi Aoyama

Inventor： Koji Matsui ,  Mitsuru Kimura ,  Kazuaki Utsumi ,  Eiichi Ogawa ,  Hiroshi Komano ,  Toshimi Aoyama

IPC: H01L21/60 ,  H01L21/603 ,  H01L21/98 ,  H05K3/00 ,  H05K3/28 ,  H05K3/32 ,  H05K3/46 ,  B32B31/00

CPC classification number: H05K3/4617 ,  H01L24/81 ,  H01L25/50 ,  H01L2224/13111 ,  H01L2224/13144 ,  H01L2224/16 ,  H01L2224/2929 ,  H01L2224/293 ,  H01L2224/81193 ,  H01L2224/81801 ,  H01L2224/83101 ,  H01L2224/83851 ,  H01L2924/01005 ,  H01L2924/01006 ,  H01L2924/01013 ,  H01L2924/01019 ,  H01L2924/0102 ,  H01L2924/01024 ,  H01L2924/01029 ,  H01L2924/01033 ,  H01L2924/01042 ,  H01L2924/01049 ,  H01L2924/0105 ,  H01L2924/01073 ,  H01L2924/01079 ,  H01L2924/01082 ,  H01L2924/014 ,  H01L2924/07811 ,  H01L2924/09701 ,  H01L2924/14 ,  H01L2924/3025 ,  H05K2203/0278 ,  H05K3/0023 ,  H05K3/28 ,  H05K3/328 ,  Y10T29/49126 ,  Y10T29/4913 ,  Y10T29/49144

Abstract: A method of bonding first and second circuit boards includes applying a light-sensitive adhesive over the first electrodes on a first circuit board and the areas where the first electrodes are not formed, and drying the applied adhesive to form a light-sensitive adhesive layer having the light-sensitive adhesive layer exposed selectively to active rays of light and performing development to remove only the light-sensitive adhesive layer on the first electrodes, and then performing a heat treatment to impart bonding quality to the light-sensitive adhesive layer remaining between adjacent first electrodes, placing the first and second circuit boards one on top of the other and thermocompressing the two circuit boards to have the first electrodes connected electrically to the second electrodes to form a single circuit board; and performing a heat treatment and/or exposure to active rays of light on the formed single circuit board.

Abstract translation: 接合第一和第二电路板的方法包括在第一电路板上的第一电极上和不形成第一电极的区域上施加光敏粘合剂，并干燥所施加的粘合剂以形成具有 光敏粘合剂层选择性地暴露于活性光线并进行显影以除去第一电极上的光敏粘合剂层，然后进行热处理以赋予残留在相邻的粘合剂层之间的粘合剂层的粘合质量 第一电极，将第一和第二电路板放置在另一个之上，并且热压两个电路板，以使第一电极与第二电极电连接以形成单个电路板; 并且对所形成的单电路板进行热处理和/或对活性光线的曝光。

公开(公告)号：US4667021A

公开(公告)日：1987-05-19

申请号：US654665

申请日：1984-09-26

Applicant: Junji Toda ,  Eiichi Ogawa

Inventor： Junji Toda ,  Eiichi Ogawa

IPC: C09B45/14 ,  C09B62/095 ,  D06P1/382 ,  C09B45/26 ,  D06P1/10

CPC classification number: C09B62/095 ,  D06P1/382

Abstract: A chromium complex compound represented as the free acid form by the formula (I): ##STR1## wherein X.sup.1 represents a hydrogen atom, a methyl group, a methoxy group or a sulfonic acid group; X.sup.2, X.sup.3 and X.sup.4 represent independently a hydrogen atom, a chlorine atom, a methyl gorup, a methoxy group, a carboxyl group or a sulfonic acid group; Y represents a hydrogen atom or a sulfonic acid group; Z represents a chlorine atom, a fluorine atom or --N.sup.30 (R).sub.3 (R represents a C.sub.1 to C.sub.4 -alkyl group), ##STR2## and M represents a hydrogen atom or an alkali metal, a process for producing the chromium complex compound (I) and a method for dyeing cellulosic fibers with the same. The chromium complex compound represented by formula (I) is excellent in affinity to cellulosic fibers and in color-yield, build-up properties and fastness properties. These compounds are dyes for cellulosic fibers.

Abstract translation: 由式（I）表示为游离酸形式的铬配位化合物：其中X1表示氢原子，甲基，甲氧基或磺酸基; X2，X3和X4独立地表示氢原子，氯原子，甲基，甲氧基，羧基或磺酸基; Y表示氢原子或磺酸基; Z表示氯原子，氟原子或-N30（R）3（R表示C1〜C4烷基），＆lt; IMAGE＆gt; M表示氢原子或碱金属，铬配位化合物的制造方法 （I）和用其染色纤维素纤维的方法。 由式（I）表示的铬配位化合物对纤维素纤维的亲和性和色产率，增加性能和牢度性质优异。 这些化合物是纤维素纤维的染料。

公开(公告)号：US06485551B1

公开(公告)日：2002-11-26

申请号：US09643332

申请日：2000-08-22

Applicant: Takahiro Kohsaka ,  Eiichi Ogawa

Inventor： Takahiro Kohsaka ,  Eiichi Ogawa

IPC: C09D1100

CPC classification number: D06P5/30 ,  D06P3/06 ,  D06P3/10 ,  D06P3/148 ,  D06P3/16 ,  D06P3/241 ,  D06P3/248

Abstract: A method of printing a polyamide structure using two or more of water-soluble dye with an inorganicity/organicity value of 1 to 7 selected so that the ones with the largest and smallest inorganicity/organicity values show a difference of 2 or below between their two such values, to allow the polyamide structure to be printed with no uneven color, high color reproducibility and excellent ink bleeding prevention.

Abstract translation: 使用两种或更多种无机/有机质值为1至7的水溶性染料印刷聚酰胺结构的方法，使得具有最大和最小无机性/有机性值的那些具有2或更低的差异 这样的值可以使聚酰胺结构印刷没有不均匀的颜色，高的颜色再现性和出色的防止油墨渗出。

公开(公告)号：US5032140A

公开(公告)日：1991-07-16

申请号：US426746

申请日：1989-10-24

Applicant: Nobuyuki Yamanaka ,  Kazuo Hanawa ,  Eiichi Ogawa

Inventor： Nobuyuki Yamanaka ,  Kazuo Hanawa ,  Eiichi Ogawa

IPC: C09B69/02

CPC classification number: C09B69/02 ,  Y10S8/917 ,  Y10S8/918 ,  Y10S8/924 ,  Y10S8/937

Abstract: A reactive dye represented by the formula (I), ##STR1## wherein R represents --NH.sub.2 or --NHC.sub.2 H.sub.4 SO.sub.3 M, and M's independently represent Li.sup..sym., Na.sup..sym., K.sup..sym. or .sup..sym. NH(C.sub.2 H.sub.4 OH).sub.3, provided that at least one of M's represents Li.sup..sym. or .sup..sym. NH(C.sub.2 H.sub.4 OH).sub.3. This reactive dye easily gives a stable liquid composition and is useful to dye cellulosic or polyamide fibers.

Abstract translation: 由式（I）表示的活性染料，其中R表示-NH 2或-NHC 2 H 4 SO 3 M，M独立地表示Li（+），Na（+），K（+）或（+）NH（ C2H4OH）3，条件是M中的至少一个表示Li（+）或（+）NH（C 2 H 4 OH）3。 该活性染料容易得到稳定的液体组合物，可用于染色纤维素或聚酰胺纤维。