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    Alkoxylation of 6-membered alkylene carbonates
    4.
    发明授权
    Alkoxylation of 6-membered alkylene carbonates 失效
    6元碳酸亚烷基酯的烷氧基化

    公开(公告)号：US06498278B1

    公开(公告)日：2002-12-24

    申请号：US09946312

    申请日：2001-09-05

    Applicant: John H. Clements ,  Howard P. Klein ,  Edward T. Marquis

    Inventor： John H. Clements ,  Howard P. Klein ,  Edward T. Marquis

    IPC: C07C4100

    CPC classification number: C07C43/23 ,  C07C41/16

    Abstract: A method for the preparation of &ggr;-hydroxy ethers from cyclic organic carbonates and active-hydrogen-containing compounds in one form includes the steps of contacting an active-hydrogen-containing compound and a cyclic organic carbonate compound containing a six-membered ring, and a catalyst, running the reaction at a suitable temperature, and isolating the &ggr;-hydroxy ether as a mixture that can be purified or used directly as produced in the reaction.

    Abstract translation: 一种形式的环状有机碳酸酯和含活性氢化合物的γ-羟基醚的制备方法包括使含活性氢的化合物与含有六元环的环状有机碳酸酯化合物接触的步骤，以及 催化剂，在合适的温度下运行反应，并将γ-羟基醚作为可以如反应产生的直接纯化或直接使用的混合物分离。

    Polyurethane foams based on amino polyols
    5.
    发明授权
    Polyurethane foams based on amino polyols 失效
    基于氨基多元醇的聚氨酯泡沫

    公开(公告)号：US4654376A

    公开(公告)日：1987-03-31

    申请号：US791015

    申请日：1985-10-24

    Applicant: Michael E. Brennan ,  Kenneth G. McDaniel ,  Howard P. Klein

    Inventor： Michael E. Brennan ,  Kenneth G. McDaniel ,  Howard P. Klein

    IPC: C08G18/50 ,  C08G18/54 ,  C08G18/14 ,  C08G18/32

    CPC classification number: C08G18/5033 ,  C08G18/546 ,  C08G2101/0025 ,  C08G2101/005 ,  C08G2105/02 ,  Y10S521/902

    Abstract: An improved method for preparing amino polyols is disclosed. The method is the Mannich condensation of phenol, formaldehyde and diethanolamine in a molar ratio of (1:1:1), and then alkoxylation with a mixture of ethylene oxide and propylene oxide in a weight ratio of about 5:95 to 20:80 to form an amino polyol of hydroxyl number 440 to 515.The method gives higher yields of aromatic amino polyols of lower viscosity than those of the comparative example.

    Abstract translation: 公开了改进的制备氨基多元醇的方法。 该方法是苯酚，甲醛和二乙醇胺的摩尔比为（1:1:1）的曼尼希缩合，然后用环氧乙烷和环氧丙烷的混合物以约5:95至20:80的重量比进行烷氧基化 以形成羟基数为440至515的氨基多元醇。该方法提供比比较例的更低的粘度的芳族氨基多元醇的较高产率。

    Accelerated cure of epoxy resins
    8.
    发明授权
    Accelerated cure of epoxy resins 失效
    加速固化环氧树脂

    公开(公告)号：US4164520A

    公开(公告)日：1979-08-14

    申请号：US927260

    申请日：1978-07-24

    Applicant: Harold G. Waddill ,  Howard P. Klein

    Inventor： Harold G. Waddill ,  Howard P. Klein

    IPC: C08G14/06 ,  C08G14/14 ,  C08G59/62 ,  C08L63/00

    CPC classification number: C08G59/623 ,  C08G14/06 ,  C08G14/14 ,  C08L63/00

    Abstract: A process for the accelerated cure of an epoxy resin is disclosed. The resulting epoxy resin may be used in protective coatings, adhesives, seamless and terrazo flooring and caulking and sealing compositions. The resulting resin system is also useful, for example, in casting, potting, in escapulating, grouting and patching. The process involves mixing an epoxy resin of the polyhydric phenol, polyglycidyl ether type with a novel accelerator-hardener which is a condensation product of phenol, formaldehyde and an aminoalkylene derivative of a polyoxyalkylenepolyamine.

    Abstract translation: 公开了一种加速固化环氧树脂的方法。 所得到的环氧树脂可用于保护涂料，粘合剂，无缝和地层和填缝和密封组合物中。 所得的树脂体系也可用于例如浇铸，灌封，脱水，灌浆和修补。 该方法包括将多元酚的环氧树脂，聚缩水甘油醚型与作为苯酚，甲醛和聚氧亚烷基多胺的氨基亚烷基衍生物的缩合产物的新型促进剂 - 硬化剂混合。

    Isocyanurate foam catalyst
    9.
    发明授权
    Isocyanurate foam catalyst 失效
    异氰脲酸酯泡沫催化剂

    公开(公告)号：US4026836A

    公开(公告)日：1977-05-31

    申请号：US644494

    申请日：1975-12-29

    Applicant: Robert L. Zimmerman ,  Edward E. McEntire ,  Howard P. Klein

    Inventor： Robert L. Zimmerman ,  Edward E. McEntire ,  Howard P. Klein

    IPC: C08G18/18 ,  C08G18/20 ,  C08G18/22 ,  C08J9/00

    CPC classification number: C08G18/2009 ,  C08G18/1866 ,  C08G18/225 ,  C08G2101/0008 ,  C08G2101/0016 ,  C08G2101/0025 ,  C08G2105/02 ,  Y10S521/902

    Abstract: New catalysts for isocyanurate foams are those comprising aminomethacrylate salts. The foams are obtained by the polymerization of an aromatic polyisocyanate, and a polyether or polyester polyol in the presence of a blowing agent and said amino methacrylate salts falling within the following structural formula: ##STR1## where the radicals represented by R when taken singly are lower alkyl, and hydroxy lower alkyl, and when taken together with the adjacent nitrogen atom are selected from the group consisting of morpholino, C-substituted morpholino, N-alkylpiperazino and C-substituted N-alkylpiperazino, and M is selected from the group consisting of sodium, potassium, cesium, lithium and rubidium. The novel foams are useful in preparing rigid, flexible, semi-rigid, or semi-flexible materials such as panels, slabs or sprayed foam surfaces.

    Abstract translation: 用于异氰脲酸酯泡沫的新催化剂是包含氨基甲基丙烯酸盐的那些。 通过在发泡剂存在下聚合芳族多异氰酸酯和聚醚或聚酯多元醇而获得泡沫，所述氨基甲基丙烯酸盐属于以下结构式：其中由单独表示的基团由R表示的基团为 低级烷基和羟基低级烷基，当与相邻的氮原子一起选自吗啉代，C取代的吗啉代，N-烷基哌嗪基和C-取代的N-烷基哌嗪基，M选自 的钠，钾，铯，锂和铷。 新型泡沫可用于制备刚性，柔性，半刚性或半柔性材料，例如面板，板坯或喷涂的泡沫表面。

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