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    Metal complex and manufacturing method therefor
    3.
    发明授权
    Metal complex and manufacturing method therefor 失效
    金属络合物及其制造方法

    公开(公告)号：US08592626B2

    公开(公告)日：2013-11-26

    申请号：US13059766

    申请日：2009-08-19

    申请人： Yasutaka Inubushi ,  Takashi Hori ,  Hiroyuki Ohgi

    发明人： Yasutaka Inubushi ,  Takashi Hori ,  Hiroyuki Ohgi

    IPC分类号： C07C63/34 ,  C07C63/36 ,  B01J20/26

    CPC分类号： C07F1/005 ,  B01D53/02 ,  B01D2253/204 ,  B01D2257/102 ,  B01D2257/104 ,  B01D2257/108 ,  B01D2257/11 ,  B01D2257/302 ,  B01D2257/304 ,  B01D2257/404 ,  B01D2257/406 ,  B01D2257/502 ,  B01D2257/504 ,  B01D2257/556 ,  B01D2257/702 ,  B01D2257/80 ,  B01D2258/06 ,  B01J20/223 ,  C07C65/105 ,  C07C65/11 ,  Y02C10/08 ,  Y02P20/152

    摘要： Disclosed is a metal complex that can be used as a gas absorption material with superior gas absorbing properties, a gas storage material with a high storage capacity, and a gas separation material with superior gas separation performance and high adsorption capacity. Disclosed is a metal complex, and a manufacturing method therefor, which consists of: a polycyclic aromatic dihydroxy monocarboxylic acid compound, in the structural formula of which hydroxyl groups are at the farthest locations from each other, which has carboxyl groups at the locations adjacent to the hydroxyl groups, and which has 10 or more circularly conjugated π electrons, such as 3,7-dihydorxy-2-naphtoic acid or 4,4′-dihydroxy-3-biphenylcaroxylic acid; at least one metal selected from chromium, molybdenum, tungsten, manganese, iron, ruthenium, cobalt, rhodium, nickel, palladium, copper, zinc, and cadmium; and an organic ligand, such as 4,4′-bipyridyl, capable of bidentate bonding with said metal.

    摘要翻译： 公开了可以用作气体吸收性优异的气体吸收材料的金属络合物，具有高储存能力的储气材料和具有优异的气体分离性能和高吸附能力的气体分离材料。 公开了一种金属络合物及其制造方法，其由以下结构构成：多环芳族二羟基单羧酸化合物，其结构式为羟基在彼此最远的位置，在邻近的位置具有羧基 羟基，并且具有10个或更多个环状共轭π电子，例如3,7-二羟基-2-萘甲酸或4,4'-二羟基-3-联苯基羟基酸; 选自铬，钼，钨，锰，铁，钌，钴，铑，镍，钯，铜，锌和镉中的至少一种金属; 以及能够与所述金属二齿键合的有机配体，例如4,4'-联吡啶。

    Process for production of hydrogenated polymers and hydrogenated polymers
    8.
    发明授权
    Process for production of hydrogenated polymers and hydrogenated polymers 有权
    氢化聚合物和氢化聚合物的生产方法

    公开(公告)号：US08044149B2

    公开(公告)日：2011-10-25

    申请号：US12442305

    申请日：2007-09-20

    申请人： Hideharu Iwasaki ,  Yasutaka Inubushi

    发明人： Hideharu Iwasaki ,  Yasutaka Inubushi

    IPC分类号： C08F8/42

    CPC分类号： C08G61/08

    摘要： Provision of, in a process of producing a hydrogenated polymer, which comprises steps of sequentially performing, in the presence of a ruthenium carbene complex, a ring-opening metathesis polymerization reaction of a cyclic olefin and a hydrogenation reaction of a ring-opening metathesis polymer produced by the polymerization reaction to give a hydrogenated polymer, a simple and economic process of obtaining a hydrogenated polymer having an extremely small content of residual ruthenium derived from the ruthenium carbene complex.A process of producing a hydrogenated polymer, which comprises, in the presence of a ruthenium carbene complex, subjecting a cyclic monoolefin and/or a cyclic diolefin to a ring-opening metathesis polymerization, hydrogenating the resulting ring-opening metathesis polymer to give a hydrogenated polymer, and bringing the hydrogenated polymer in contact with a poor solvent of the hydrogenated polymer in the presence of dissolved hydrogen to allow precipitation. As the poor solvent of the hydrogenated polymer, alcohol having 1 to 6 carbon atoms, ketone having 3 to 6 carbon atoms and the like are preferable.

    摘要翻译： 在生产氢化聚合物的方法中提供了包括以下步骤：在钌卡宾络合物的存在下，环烯烃的开环易位聚合反应和开环易位聚合物的氢化反应 通过聚合反应生成氢化聚合物，获得氢化聚合物的简单且经济的方法，该氢化聚合物的钌卡宾络合物的残余钌含量极少。 一种制备氢化聚合物的方法，其包括在钌卡宾络合物的存在下，使环状单烯烃和/或环状二烯烃进行开环易位聚合，将所得开环易位聚合物氢化，得到氢化 聚合物，并使氢化聚合物与氢化聚合物的不良溶剂在溶解的氢气存在下接触以允许沉淀。 作为氢化聚合物的不良溶剂，优选具有1〜6个碳原子的醇，具有3〜6个碳原子的酮等。

    PROCESS FOR PRODUCTION OF HYDROGENATED POLYMERS AND HYDROGENATED POLYMERS
    10.
    发明申请
    PROCESS FOR PRODUCTION OF HYDROGENATED POLYMERS AND HYDROGENATED POLYMERS 有权
    生产氢化聚合物和加氢聚合物的方法

    公开(公告)号：US20100029874A1

    公开(公告)日：2010-02-04

    申请号：US12442305

    申请日：2007-09-20

    申请人： Hideharu Iwasaki ,  Yasutaka Inubushi

    发明人： Hideharu Iwasaki ,  Yasutaka Inubushi

    IPC分类号： C08F4/80

    CPC分类号： C08G61/08

    摘要： Provision of, in a process of producing a hydrogenated polymer, which comprises steps of sequentially performing, in the presence of a ruthenium carbene complex, a ring-opening metathesis polymerization reaction of a cyclic olefin and a hydrogenation reaction of a ring-opening metathesis polymer produced by the polymerization reaction to give a hydrogenated polymer, a simple and economic process of obtaining a hydrogenated polymer having an extremely small content of residual ruthenium derived from the ruthenium carbene complex.A process of producing a hydrogenated polymer, which comprises, in the presence of a ruthenium carbene complex, subjecting a cyclic monoolefin and/or a cyclic diolefin to a ring-opening metathesis polymerization, hydrogenating the resulting ring-opening metathesis polymer to give a hydrogenated polymer, and bringing the hydrogenated polymer in contact with a poor solvent of the hydrogenated polymer in the presence of dissolved hydrogen to allow precipitation. As the poor solvent of the hydrogenated polymer, alcohol having 1 to 6 carbon atoms, ketone having 3 to 6 carbon atoms and the like are preferable.

    摘要翻译： 在生产氢化聚合物的方法中提供了包括以下步骤：在钌卡宾络合物的存在下，环烯烃的开环易位聚合反应和开环易位聚合物的氢化反应 通过聚合反应生成氢化聚合物，获得氢化聚合物的简单且经济的方法，该氢化聚合物的钌卡宾络合物的残余钌含量极少。 一种制备氢化聚合物的方法，其包括在钌卡宾络合物的存在下，使环状单烯烃和/或环状二烯烃进行开环易位聚合，将所得开环易位聚合物氢化，得到氢化 聚合物，并使氢化聚合物与氢化聚合物的不良溶剂在溶解的氢气存在下接触以允许沉淀。 作为氢化聚合物的不良溶剂，优选具有1〜6个碳原子的醇，具有3〜6个碳原子的酮等。