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公开(公告)号：US07749299B2
公开(公告)日：2010-07-06
申请号：US11331230
申请日：2006-01-13
申请人： Karel Vanheusden , Klaus Kunze , Hyungrak Kiim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
发明人： Karel Vanheusden , Klaus Kunze , Hyungrak Kiim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
IPC分类号： B22F9/24
CPC分类号： B22F1/0018 , B22F1/0022 , B22F9/24 , B22F2998/10 , B82Y30/00 , C09D11/101 , C09D11/30 , C09D11/38 , C22B3/20 , C22B11/04 , C22B23/0453 , H01B1/22 , H01L21/288 , H05K1/097 , H05K3/125 , H05K2203/013 , Y02P10/234 , Y10S977/777 , Y10S977/896
摘要： A process for the production of metal nanoparticles. The process comprises a rapid mixing of a solution of at least about 0.1 mole of a metal compound that is capable of being reduced to a metal by a polyol with a heated solution of a polyol and a substance that is capable of being adsorbed on the nanoparticles.
摘要翻译： 一种生产金属纳米粒子的方法。 该方法包括将至少约0.1摩尔能够被多元醇还原成金属的金属化合物与多元醇的加热溶液和能够吸附在纳米颗粒上的物质快速混合 。
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公开(公告)号：US07732002B2
公开(公告)日：2010-06-08
申请号：US10274495
申请日：2002-10-18
申请人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
发明人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
摘要： Precursor compositions in the form of a tape that can be transferred to a substrate and converted to an electronic feature at a relatively low temperature, such as not greater than about 200° C. The tape composition can be disposed on a carrier to form a ribbon structure that is flexible and can be handled in a variety of industrial processes.
摘要翻译： 胶带形式的前体组合物可以转移到基底并在相对低的温度例如不大于约200℃下转化成电子特征。胶带组合物可以设置在载体上以形成带状物 结构灵活，可以在各种工业过程中处理。
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公开(公告)号：US07691664B2
公开(公告)日：2010-04-06
申请号：US11642664
申请日：2006-12-21
申请人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
发明人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
IPC分类号： H01L21/00
CPC分类号： H05K3/105 , C23C18/06 , C23C18/08 , H01B1/026 , H01L24/03 , H01L24/05 , H01L2224/05294 , H01L2224/053 , H01L2924/12042 , H01L2924/12044 , H01L2924/14 , H05K1/097 , H05K2201/0154 , H05K2203/1131 , H01L2924/00
摘要： A precursor composition for the deposition and formation of an electrical feature such as a conductive feature. The precursor composition advantageously has a low viscosity enabling deposition using direct-write tools. The precursor composition also has a low conversion temperature, enabling the deposition and conversion to an electrical feature on low temperature substrates. A particularly preferred precursor composition includes silver metal for the formation of highly conductive silver features.
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公开(公告)号：US20080108218A1
公开(公告)日：2008-05-08
申请号：US11642664
申请日：2006-12-21
申请人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
发明人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
IPC分类号： H01L21/44
CPC分类号： H05K3/105 , C23C18/06 , C23C18/08 , H01B1/026 , H01L24/03 , H01L24/05 , H01L2224/05294 , H01L2224/053 , H01L2924/12042 , H01L2924/12044 , H01L2924/14 , H05K1/097 , H05K2201/0154 , H05K2203/1131 , H01L2924/00
摘要： A precursor composition for the deposition and formation of an electrical feature such as a conductive feature. The precursor composition advantageously has a low viscosity enabling deposition using direct-write tools. The precursor composition also has a low conversion temperature, enabling the deposition and conversion to an electrical feature on low temperature substrates. A particularly preferred precursor composition includes silver metal for the formation of highly conductive silver features.
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公开(公告)号：US07824466B2
公开(公告)日：2010-11-02
申请号：US11755720
申请日：2007-05-30
申请人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott T. Haubrich , Mark H. Kowalski , Nathan E. Stott
发明人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott T. Haubrich , Mark H. Kowalski , Nathan E. Stott
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , B22F1/0022 , B22F2998/10 , B82Y30/00 , C09D11/03 , C09D11/30 , C09D11/52 , Y10S977/896 , B22F1/0018
摘要： Processes for the production of metal nanoparticles. In one aspect, the invention is to a process comprising the steps of mixing a heated first solution comprising a base and/or a reducing agent (e.g., a non-polyol reducing agent), a polyol, and a polymer of vinyl pyrrolidone with a second solution comprising a metal precursor that is capable of being reduced to a metal by the polyol. In another aspect, the invention is to a process that includes the steps of heating a powder of a polymer of vinyl pyrrolidone; forming a first solution comprising the powder and a polyol; and mixing the first solution with a second solution comprising a metal precursor capable of being reduced to a metal by the polyol.
摘要翻译： 制备金属纳米粒子的方法。 一方面，本发明涉及一种方法，包括以下步骤：将包含碱和/或还原剂（例如非多元醇还原剂）的加热的第一溶液，多元醇和乙烯基吡咯烷酮的聚合物与 第二溶液包含能够被多元醇还原成金属的金属前体。 另一方面，本发明涉及一种方法，其包括加热乙烯基吡咯烷酮聚合物粉末的步骤; 形成包含所述粉末和多元醇的第一溶液; 并将第一溶液与包含能够被多元醇还原成金属的金属前体的第二溶液混合。
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公开(公告)号：US20100269635A1
公开(公告)日：2010-10-28
申请号：US12829934
申请日：2010-07-02
申请人： Karel VANHEUSDEN , Klaus KUNZE , Hyungrak KIM , Aaron D. STUMP , Allen B. Schult , Mark J. Hampden-Smith , Chuck EDWARDS , Anthony R. JAMES , James CARUSO , Toivo T. KODAS , Scott T. HAUBRICH , Mark H. KOWALSKI , Nathan E. STOTT
发明人： Karel VANHEUSDEN , Klaus KUNZE , Hyungrak KIM , Aaron D. STUMP , Allen B. Schult , Mark J. Hampden-Smith , Chuck EDWARDS , Anthony R. JAMES , James CARUSO , Toivo T. KODAS , Scott T. HAUBRICH , Mark H. KOWALSKI , Nathan E. STOTT
IPC分类号： B22F9/18
CPC分类号： B22F9/24 , B22F1/0022 , B22F2998/10 , B82Y30/00 , C09D11/03 , C09D11/30 , C09D11/52 , Y10S977/896 , B22F1/0018
摘要： Processes for the production of metal nanoparticles. In one aspect, the invention is to a process comprising the steps of mixing a heated first solution comprising a base and/or a reducing agent (e.g., a non-polyol reducing agent), a polyol, and a polymer of vinyl pyrrolidone with a second solution comprising a metal precursor that is capable of being reduced to a metal by the polyol. In another aspect, the invention is to a process that includes the steps of heating a powder of a polymer of vinyl pyrrolidone; forming a first solution comprising the powder and a polyol; and mixing the first solution with a second solution comprising a metal precursor capable of being reduced to a metal by the polyol.
摘要翻译： 制备金属纳米粒子的方法。 一方面，本发明涉及一种方法，包括以下步骤：将包含碱和/或还原剂（例如非多元醇还原剂）的加热的第一溶液，多元醇和乙烯基吡咯烷酮的聚合物与 第二溶液包含能够被多元醇还原成金属的金属前体。 另一方面，本发明涉及一种方法，其包括加热乙烯基吡咯烷酮聚合物粉末的步骤; 形成包含所述粉末和多元醇的第一溶液; 并将第一溶液与包含能够被多元醇还原成金属的金属前体的第二溶液混合。
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公开(公告)号：US20100269634A1
公开(公告)日：2010-10-28
申请号：US12829658
申请日：2010-07-02
申请人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
发明人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
IPC分类号： B22F1/00
CPC分类号： B22F1/0018 , B22F1/0022 , B22F9/24 , B22F2998/10 , B82Y30/00 , C09D11/101 , C09D11/30 , C09D11/38 , C22B3/20 , C22B11/04 , C22B23/0453 , H01B1/22 , H01L21/288 , H05K1/097 , H05K3/125 , H05K2203/013 , Y02P10/234 , Y10S977/777 , Y10S977/896
摘要： A process for the production of metal nanoparticles. The process comprises a rapid mixing of a solution of at least about 0.1 mole of a metal compound that is capable of being reduced to a metal by a polyol with a heated solution of a polyol and a substance that is capable of being adsorbed on the nanoparticles.
摘要翻译： 一种生产金属纳米粒子的方法。 该方法包括将至少约0.1摩尔能够被多元醇还原成金属的金属化合物与多元醇的加热溶液和能够吸附在纳米颗粒上的物质快速混合 。
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公开(公告)号：US20100112195A1
公开(公告)日：2010-05-06
申请号：US10274495
申请日：2002-10-18
申请人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
发明人： Toivo T. Kodas , Mark J. Hampden-Smith , Karel Vanheusden , Hugh Denham , Aaron D. Stump , Allen B. Schult , Paolina Atanassova , Klaus Kunze
摘要： Precursor compositions in the form of a tape that can be transferred to a substrate and converted to an electronic feature at a relatively low temperature, such as not greater than about 200° C. The tape composition can be disposed on a carrier to form a ribbon structure that is flexible and can be handled in a variety of industrial processes.
摘要翻译： 胶带形式的前体组合物可以转移到基底并在相对低的温度例如不大于约200℃下转化成电子特征。胶带组合物可以设置在载体上以形成带状物 结构灵活，可以在各种工业过程中处理。
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公开(公告)号：US07575621B2
公开(公告)日：2009-08-18
申请号：US11331238
申请日：2006-01-13
申请人： Karel Vanheusden , Hyungrak Kiim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
发明人： Karel Vanheusden , Hyungrak Kiim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
IPC分类号： B22F9/24
CPC分类号： B22F1/0018 , B22F1/0022 , B22F9/24 , B22F2998/10 , B82Y30/00 , C09D11/101 , C09D11/30 , C09D11/38 , C22B3/20 , C22B11/04 , C22B23/0453 , H01B1/22 , H01L21/288 , H05K1/097 , H05K3/125 , H05K2203/013 , Y02P10/234 , Y10S977/777 , Y10S977/896
摘要： A process for the production of metal nanoparticles. Nanoparticles are formed by combining a metal compound with a solution that comprises a polyol and a substance that is capable of being adsorbed on the nanoparticles. The nanoparticles are precipitated by adding a nanoparticle-precipitating liquid in a sufficient amount to precipitate at least a substantial portion of the nanoparticles and of a protic solvent in a sufficient amount to improve the separation of the nanoparticles from the liquid phase.
摘要翻译： 一种生产金属纳米粒子的方法。 通过将金属化合物与包含多元醇的溶液和能够吸附在纳米颗粒上的物质组合来形成纳米颗粒。 通过添加足够量的纳米颗粒沉淀液体来沉淀纳米颗粒，以使至少大部分的纳米颗粒和质量溶剂足够的量沉淀以改善纳米颗粒与液相的分离。
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公开(公告)号：US08383014B2
公开(公告)日：2013-02-26
申请号：US12816210
申请日：2010-06-15
申请人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
发明人： Karel Vanheusden , Klaus Kunze , Hyungrak Kim , Aaron D. Stump , Allen B. Schult , Mark J. Hampden-Smith , Chuck Edwards , Anthony R. James , James Caruso , Toivo T. Kodas , Scott Thomas Haubrich , Mark H. Kowalski
IPC分类号： H01B1/02
CPC分类号： H01B1/02 , B82Y30/00 , H01B1/22 , Y10S977/773 , Y10S977/81
摘要： A metal nanoparticle composition for the fabrication of conductive features. The metal nanoparticle composition advantageously has a low viscosity permitting deposition of the composition by direct-write tools. The metal nanoparticle composition advantageously also has a low conversion temperature, permitting its deposition and conversion to an electrical feature on polymeric substrates.
摘要翻译： 用于制造导电特征的金属纳米颗粒组合物。 金属纳米颗粒组合物有利地具有低粘度，允许通过直写工具沉积组合物。 金属纳米颗粒组合物有利地还具有低转化温度，允许其沉积并转化成聚合物基底上的电特征。
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