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    Polyphase compositions and process for their preparation
    51.
    发明授权
    Polyphase compositions and process for their preparation 失效
    多相组合物及其制备方法

    公开(公告)号：US3689597A

    公开(公告)日：1972-09-05

    申请号：US3689597D

    申请日：1970-06-26

    Applicant: HERCULES INC

    Inventor： MAHLMAN BERT H

    IPC: C08L23/10 ,  C08L45/02 ,  C08L57/02 ,  C09J3/26

    CPC classification number: C08L25/16 ,  C08L23/10 ,  C08L25/04 ,  C08L25/06 ,  C08L45/02 ,  C08L57/02 ,  C08L2207/14 ,  C08L2666/04 ,  C08L2666/06

    Abstract: Unique polyphase compositions are disclosed having, as a continuous phase a propylene polymer and as a second phase a substantially amorphous organic material selected from solid or semi-solid hydrocarbons and hydrocarbon resins. These compositions are prepared by dispersing a propylene polymer of substantially all sub-micron particle size in the second phase and fusing the polymer under controlled conditions which assure the formation of the propylene polymer into a continuous phase.

    Abstract translation: 公开了独特的多相组合物，其具有作为连续相的丙烯聚合物和作为第二相的选自固体或半固体烃和烃树脂的基本上无定形的有机材料。 这些组合物通过将基本上全部亚微米粒度的丙烯聚合物分散在第二相中并在控制条件下使聚合物熔融，从而确保丙烯聚合物形成连续相来制备。

    Azidoformates and their use
    52.
    发明授权
    Azidoformates and their use 失效
    AZIDOFORMATES及其使用

    公开(公告)号：US3686231A

    公开(公告)日：1972-08-22

    申请号：US3686231D

    申请日：1970-11-27

    Applicant: HERCULES INC

    Inventor： HAYNES JAMES N

    IPC: C08G63/91 ,  C08J5/12 ,  C07C117/00

    CPC classification number: C07C247/00 ,  C08G63/916 ,  C08J5/124

    Abstract: WHERE R IS AN ALKYLENE RADICAL CONTAINING 2 TO 10 CARBON ATOMS AND X IS AN INTEGER OF FROM ABOUT 1 TO ABOUT 10. ALSO DISCLOSED IS A PROCESS OF IMPROVING THE ADHESION OF POLYESTER MATERIAL TO VARIOUS OTHER MATERIALS USING THE AZIDOLFORMATE COMPOUNDS. IN PARTICULAR, THERE IS DISCLOSED A PROCESS OF IMPROVING THE ADHESION OF POLYESTER TIRE CORD TO RUBBER TIRE STOCK USING THE SAID AZIDOFORMATE COMPOUNDS.
    DISCLOSED ARE THE AZIDOFORMATES OF OMEGA-HYDROXYALKYL PHTHALATES, THEIR RELATED LOW MOLECULAR WEIGHT CONDENSATION POLYMERS AND THEIR MIXTURES REPRESENTED BY THE GENERAL FORMULA

    N3-CO-(O-R-OOC-C6H4-CO)X-O-R-OOC-N3

    Method of producing fine particle ammonium perchlorate
    53.
    发明授权
    Method of producing fine particle ammonium perchlorate 失效
    生产细颗粒乳酸铵的方法

    公开(公告)号：US3685163A

    公开(公告)日：1972-08-22

    申请号：US3685163D

    申请日：1971-03-16

    Applicant: HERCULES INC

    Inventor： OLT ROBERT L

    IPC: C01B11/18 ,  F26B5/06

    CPC classification number: C01B11/185 ,  Y10S149/113

    Abstract: A process for preparing ultra-fine ammonium perchlorate particles is provided. In this process an aqueous solution of ammonium perchlorate is dispersed in an organic liquid to form a water-in-oil emulsion. The emulsion is frozen and freeze dried to produce the ultra-fine particles.

    Apparatus for removing oil spills from the surface of a body of water
    56.
    发明授权
    Apparatus for removing oil spills from the surface of a body of water 失效
    从水体表面去除油体的装置

    公开(公告)号：US3667608A

    公开(公告)日：1972-06-06

    申请号：US3667608D

    申请日：1970-04-24

    Applicant: HERCULES INC

    Inventor： BURROUGHS RALPH H ,  COX PAUL R JR

    IPC: A47L13/20 ,  E02B15/04 ,  E02B15/10

    CPC classification number: E02B15/10 ,  A47L13/20 ,  Y02A20/204 ,  Y10S210/924

    Abstract: Oil is removed from contaminated water by means of a fibrous structure of low denier polyolefin fibers attached to a pumping system. The polyolefin fiber structure can absorb many times its own weight of oil while absorbing little or no water. The oil is then easily removed from the fibrous structure by pumping.

    Abstract translation: 油通过附着在泵送系统上的低旦尼尔聚烯烃纤维的纤维结构从污染的水中除去。 聚烯烃纤维结构可以吸收很多次自身重量的油，同时吸收很少或没有水。 然后通过泵送容易地从纤维结构中除去油。

    Manufacture of high purity nitric oxide
    59.
    发明授权
    Manufacture of high purity nitric oxide 失效
    高纯氮氧化物的制造

    公开(公告)号：US3663167A

    公开(公告)日：1972-05-16

    申请号：US3663167D

    申请日：1970-09-21

    Applicant: HERCULES INC

    Inventor： VRY FRANK E DE

    IPC: C01B21/26

    CPC classification number: C01B21/26 ,  B01J2219/00078 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00162 ,  B01J2219/00182 ,  C01B21/262

    Abstract: Process, integrated with ammonia air oxidation, for the manufacture of nitric oxide of at least 99 percent purity comprising the steps of (1) effecting the ammonia oxidation, (2) maintaining maximum NO content in the oxidation effluent, and then contacting the effluent with nitric acid to convert the NO to NO2, (3) cooling the NO2 containing gas product to condense the NO2 therefrom as liquid N2O4, (4) passing the liquid N2O4 into a packed converter tower and therein at least partially vaporizing the liquid; passing resulting vaporization product upwardly through the tower packing and passing water or weak nitric acid into the tower and downwardly through the packing in countercurrent flow reaction contact with the vaporization product, and then into the zone of said vaporization and reaction contact with any unvaporized liquid, and vaporization product to convert substantially all of the initially added liquid dinitrogen tetroxide to nitric oxide gas product containing minor contaminant amounts of NO2, HNO3 and water, (5) water-scrubbing the NO2 and HNO3 contaminants from the NO gas product to form resulting water-wet NO gas product containing, on an anhydrous basis, at least 99 percent NO, and (6) dehydrating the water-wet NO gas product to form said NO of at least 99 weight percent purity. Strong nitric acid is formed in the converter tower as by-product.

    Abstract translation: 与氨空气氧化相结合的方法，用于制造纯度至少为99％的一氧化氮，包括以下步骤：（1）进行氨氧化，（2）保持氧化流出物中的最大NO含量，然后使流出物与 硝酸将NO转化为NO2，（3）冷却含NO 2气体产物以将NO 2作为液体N2O4冷凝，（4）将液体N2O4通入填料转炉塔并在其中至少部分蒸发液体; 使所产生的蒸发产物向上通过塔填料并将水或弱硝酸通入塔中，并向下通过填料与逆流反应接触蒸发产物，然后进入与任何未蒸发的液体的蒸发和反应接触的区域， 和蒸发产物 - 将基本上所有初始添加的液体四氧化二氮转化成含有少量NO 2，HNO 3和水的少量污染物的一氧化氮气体产物，（5）从NO气体产物中水洗涤NO 2和HNO 3污染物以形成 水无水气体产物，其以无水方式含有至少99％的NO，和（6）使水湿NO气体产物脱水以形成至少99重量％纯度的所述NO。 在转炉塔中形成强硝酸作为副产物。

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