Process for preparing microporous sheet materials
    32.
    发明授权
    Process for preparing microporous sheet materials 失效
    制备微孔材料的方法

    公开(公告)号:US3565668A

    公开(公告)日:1971-02-23

    申请号:US3565668D

    申请日:1968-05-27

    Applicant: DU PONT

    Abstract: A PROCESS FOR PREPARING MICROPOROUS SHEET MATERIALS IS DISCLOSED WHEREIN A LAYER OF A POLYMER SOLUTION CONTAINING THE REQUIRED AMOUNT OF INERT LIQUID IS APPLIED AT A SUITABLE TEMPERATURE TO A SUBSTRATE (E.G., A FABRIC), AND THEN THE LAYER OF SOLUTION IS SUBJECTED TO COOLING AND BATHING CONDITIONS SUCH THAT (1) THE LAYER IS COOLED BY AT LEAST 5*C., (2) THE SOLUTION IS CONVERTED TO A SUBSTANTIALLY COLLOIDAL POLYMERIC DISPERSION AND (3) THE LAYER IS BATHED WITH A SUITABLE BATHING LIQUID ADAPTED TO EXTRACT SAID SOLVENT UNTIL SUBSTANTIALLY ALL THE SOLVENT IS EXTRACTED.

    METHOD FOR PREPARING MICROPOROUS POLYOLEFIN FILM BY THERMALLY-INDUCED PHASE SEPARATION METHOD
    34.
    发明申请
    METHOD FOR PREPARING MICROPOROUS POLYOLEFIN FILM BY THERMALLY-INDUCED PHASE SEPARATION METHOD 有权
    通过热诱导相分离方法制备微孔聚烯烃薄膜的方法

    公开(公告)号:US20150031780A1

    公开(公告)日:2015-01-29

    申请号:US14444419

    申请日:2014-07-28

    Applicant: LG CHEM, LTD.

    Abstract: The present invention discloses a method for preparing a microporous polyolefin film comprising: a step of injecting a composition comprising polyolefin 30 to 60 wt % and a diluent, which can make liquid-liquid phase separation with the polyolefin thermodynamically 40 to 70 wt %, into an extruding machine, and melting and kneading thereof to prepare a single phase melt; and a step of extruding the melt while conducting liquid-liquid phase separation by passing through a section having the temperature below the liquid-liquid phase separation temperature and forming thereof in the form of a sheet, and a microporous polyolefin film prepared according to the method.

    Abstract translation: 本发明公开了一种微孔聚烯烃薄膜的制造方法,其特征在于,包括以下步骤:将含有聚烯烃30〜60重量%的组合物和稀释剂进行注入,所述稀释剂能够将聚烯烃与动力学上的液 - 液相分离为40〜70重量% 挤出机,并将其熔融和捏合以制备单相熔体; 以及通过使液体 - 液相分离温度低于液 - 液相分离温度的部分进行液 - 液相分离而挤出熔融物的步骤,并将其形成为片状,以及根据该方法制备的微孔聚烯烃膜 。

    POLYSACCHARIDE MONOLITHIC STRUCTURE AND MANUFACTURING METHOD THEREFOR
    35.
    发明申请
    POLYSACCHARIDE MONOLITHIC STRUCTURE AND MANUFACTURING METHOD THEREFOR 审中-公开
    多晶体单晶结构及其制造方法

    公开(公告)号:US20140311984A1

    公开(公告)日:2014-10-23

    申请号:US14258456

    申请日:2014-04-22

    Abstract: A problem is to provide a monolithic structure that is a porous body formed of a polysaccharide being a naturally-occurring polymer, and has continuous pores having an average pore diameter suitable for biomolecule separation to allow formation into an arbitrary shape, and a manufacturing method therefor. A solution is to manufacture the polysaccharide monolithic structure by a method including a first step for dissolving a polysaccharide into a mixed solvent including a solvent into which the polysaccharide is soluble and a solvent into which the polysaccharide is insoluble, at a temperature lower than a boiling point of the mixed solvent, to give a polysaccharide solution, and a second step for cooling the polysaccharide solution to give the polysaccharide monolithic structure. The polysaccharide monolithic structure obtained is a porous body having continuous pores having an average pore diameter of 0.01 to 20 micrometers and a thickness of 100 micrometers or more.

    Abstract translation: 问题在于提供作为天然存在的聚合物的多糖形成的多孔体的整体结构,并且具有适于生物分子分离以使形成任意形状的平均孔径的连续孔及其制造方法 。 解决方案是通过包括第一步骤的方法来制造多糖整体结构,该方法包括将多糖溶解在包含多糖可溶性的溶剂的混合溶剂中,以及多糖不溶于其中的溶剂,在低于沸点 的混合溶剂,得到多糖溶液,第二步是冷却多糖溶液,得到多糖整体结构。 获得的多糖整体结构是具有平均孔径为0.01〜20微米,厚度为100微米以上的连续孔的多孔体。

    PROCESS FOR PRODUCTION OF POROUS BODY AND USES THEREOF
    36.
    发明申请
    PROCESS FOR PRODUCTION OF POROUS BODY AND USES THEREOF 失效
    生产多孔体的方法及其用途

    公开(公告)号:US20090319016A1

    公开(公告)日:2009-12-24

    申请号:US12518386

    申请日:2008-03-24

    Abstract: A process for producing a porous body with different physical properties in desired regions is provided by pore forming treatment, not by bonding two or more materials made porous beforehand, with, for example, an adhesive. Raw materials are prepared, each of which contains a polymer and a raw material preparation solvent. At least two types of the raw materials having different compositions are prepared. Thereafter, the respective raw materials are frozen into desired shapes to form frozen bodies thereof. The frozen bodies thus formed are brought into contact with each other to form an assembly thereof, the assembly is exposed to a condition under which the frozen bodies begin to melt, and the assembly is then freeze-dried. Thus, a porous body having regions different in physical properties can be obtained. Such a porous body can be used as, for example, an adhesion inhibitory material or a scaffold for a cell culture.

    Abstract translation: 通过成孔处理提供了在所需区域中生产具有不同物理性质的多孔体的方法,而不是通过使用例如粘合剂将两种或更多种预先多孔的材料接合。 制备原料,每种原料含有聚合物和原料制备溶剂。 制备至少两种具有不同组成的原料。 然后将各原料冷冻成所需形状,形成冷冻体。 如此形成的冷冻体彼此接触以形成其组件,该组件暴露于冷冻体开始融化的状态下,然后将组件冷冻干燥。 因此,可以获得具有物理性质不同的区域的多孔体。 这样的多孔体可以用作例如粘附抑制物质或细胞培养用支架。

    Use of synthetic granulate or powder for the removal of liquid, gaseous
and/or dissolved constituents from a process stream
    40.
    发明授权
    Use of synthetic granulate or powder for the removal of liquid, gaseous and/or dissolved constituents from a process stream 失效
    使用合成颗粒或粉末从工艺流中除去液体,气态和/或溶解成分

    公开(公告)号:US5750030A

    公开(公告)日:1998-05-12

    申请号:US699003

    申请日:1996-08-16

    Abstract: It is proposed to use a synthetic granulate or powder with a particle size of 0.1 to 10 mm as packing material for the removal of liquid, gaseous and/or dissolved constituents from a process stream, which packing material is made up of a porous, preferably dimensionally stable polymer having an overall porosity of 50 to 95% by volume, which when used as an extracting medium has pores of a diameter of 0.01 to 50 .mu.m, with an extracting liquid immobilised therein, or when used as a coalescence medium has a cellular body/window structure with the diameter of more than 50% by volume of the bodies being in the range of 100 to 700 .mu.m, which materials can be obtained by dissolving a polymer in one or more liquid and miscible compounds at a temperature above the upper critical phase separation temperature Tc, followed by a lowering of the temperature and mechanical diminution of the polymer filled with the liquid compounds, optionally followed by removal of the liquid therefrom and, optionally, refilling of at least 10% of the pore volume with an extracting liquid, characterised in that the polymer solution incorporates 5 to 60% by volume of filler, calculated on the overall solids content. The granulate or powder preferably is subjected to an aftertreatment by being coated with a powder or fibrous material having a softening temperature or melting temperature higher than that of the material to be coated.

    Abstract translation: 建议使用粒径为0.1〜10毫米的合成颗粒或粉末作为包装材料,用于从工艺流中除去液体,气体和/或溶解成分,该填料由多孔,优选 尺寸稳定的总体孔隙率为50〜95体积%的聚合物,当用作提取介质时,其直径为0.01至50μm的孔,其中固定有提取液,或当用作聚结介质时具有 体积大于体积的50体积%的细胞体/窗体结构在100至700微米的范围内,这些材料可以通过将聚合物溶解在一种或多种液体和混溶性化合物中而获得,其温度高于 上临界相分离温度Tc,然后降低填充有液体化合物的聚合物的温度和机械减小,任选地随后从其中除去液体,并且可选 用提取液重新填充至少10%的孔体积,其特征在于聚合物溶液包含5至60体积%的填料,根据总固体含量计算。 优选通过涂覆软化温度或熔融温度高于被涂覆材料的粉末或纤维材料来对颗粒或粉末进行后处理。

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