Abstract:
A method of analysing a foodstuff sample using laser-induced breakdown spectroscopy, comprises: ashing the foodstuff sample to generate an ash residue; and forming the ash residue into a layered pellet based on: loading at least the portion of the ash residue into a die, loading a support material into the die as a layer covering a second surface of the portion of the ash residue subsequently to loading at least the portion of the ash residue into the die, and compressing the portion of the ash residue and the support material in the die to form the layered pellet, such that a first surface of the portion of the ash residue at least partially defines the first surface of the layered pellet and the portion of the ash residue is undiluted by the support material at least at the first surface of the portion of the ash residue.
Abstract:
A method for preparing a sample of organic material for laser induced breakdown spectroscopy (LIBS) may include obtaining granular organic material, forming a portion of the granular organic material into a sample pellet, and searing the organic material. The searing may include searing only an exposed end surface of the sample pellet on which LIBS analysis is to be performed. The method may include pressing the seared sample pellet to consolidate the material comprising the seared end surface.
Abstract:
A filtration system for a liquid comprising a container (2) having an internal container volume (11), a particulate filter portion (10) for allowing passage of the liquid into the internal container volume (11) to forma liquid sample aliquot and a first opening (14) providing access to the internal container volume (11); the filtration system further comprising a non-porous housing (4) configured to provide an internal space (28) for receiving the container (2), the internal space (28) being dimensioned to provide a volume such that the amount left unoccupied by the received container (2) is less than the internal container volume (11).
Abstract:
A spectrometer system comprises a scanning interferometer; a drive system mechanically coupled to a movable reflector element of the scanning interferometer and operable to effect reciprocation of the movable reflector element at a plurality, preferably more than two, for example three, different scan speeds; a detector arrangement configured to sample at equidistant time intervals an interferogram formed by the scanning interferometer to generate a sampled interferogram; and a data processor is adapted to acquire a sampled interferogram at each of the plurality of different scan speeds and to perform a relative comparison of the content of the so acquired plurality of sampled interferograms.
Abstract:
A method for preparing a sample of organic material for laser induced breakdown spectroscopy (LIBS) may include obtaining granular organic material, forming a portion of the granular organic material into a sample pellet, and searing the organic material. The searing may include searing only an exposed end surface of the sample pellet on which LIBS analysis is to be performed. The method may include pressing the seared sample pellet to consolidate the material comprising the seared end surface.
Abstract:
A non-intrusive method for determining an indication of wholesomeness of an unopened item of packaged aliment comprising the steps of illuminating an unopened item of packaged aliment with electromagnetic energy at a plurality of different wavelengths through a suitably transparent region of the packaging so as to interact with the packaged aliment; obtaining spectral information regarding the interaction of the plurality of different wavelengths with the packaged aliment as subsequent spectral information; interrogating the packaging to access original spectral information regarding a previous interaction of the plurality of wavelengths with the same unopened item of packaged aliment and associated with the packaging; comparing some or all of the subsequent spectral information with some or all of the original spectral information to obtain a measure of their spectral deviation; and determining an indication of wholesomeness of the unopened item of packaged aliment in dependence of the obtained measure of spectral deviation.
Abstract:
Determination of Analytes in a Sample Matrix by Solvent Extraction A method for the assay of one or more analytes in a sample matrix comprising the steps of: performing analyte extraction on the sample matrix, said analyte extraction comprising combining the sample matrix with a solvent for an extraction period which is less than that required for reaching equilibrium; and separating the analyte containing solvent from the sample matrix; next measuring a level of analyte present in the separated solvent; and then applying in a computer a calibration by which is established a mathematical relationship between levels of analyte extracted from each of a plurality of reference samples by means of the process employed above in the extraction for the sample matrix and a reference value of the levels of analyte for each reference sample to thereby derive a measure of the level of analyte in the sample matrix. Specifically a method to determine the amount of mycotoxins in cereal grain, especially OTA (ochratoxin A) and DON (deoxynivalenol) by mixing with a solvent comprising water alcohol mixture, with 20-40% ethanol by volume.
Abstract:
A method of determining a pathlength deviation of a sample (610), the method comprising: exposing the sample (610) to electromagnetic radiation at a plurality of wavenumbers, determining electromagnetic absorption in the sample (610) at the plurality of wavenumbers, determining a first wavenumber associated with a first absorption level of an absorption band and a second wavenumber associated with a second absorption level of the absorption band, wherein the second wavenumber is different from the first wavenumber, determining a difference between the first wavenumber and the second wavenumber, and determining the pathlength deviation based on the difference.
Abstract:
A system (102) for determining properties of a sample (114) comprises a LIBS detector (104,106) and an infra-red absorption detector (108,110) for interrogating a sample (114) to generate LIBS spectral data and infra-red absorption spectral data respectively; and a data processor (112) adapted to apply at least one chemometric prediction model, each constructed to link, preferably quantitatively link, features of both LIBS and absorption spectral data to a different specific property of the sample, to a combined dataset derived from at least portions of both the LIBS and the absorption data to generate therefrom a determination, preferably a quantitative determination, of the specific property linked by that model.
Abstract:
A device for determining one or more of multiple analytes in a sample liquid includes a detection surface having thereon a microarray of elements, comprising: a plurality of binding elements immobilized by insoluble binding at discrete locations on the detection surface and a plurality of dissolvable elements immobilized by soluble binding at other discrete locations on the detection surface. The elements being arranged in the microarray such that at least a portion of the dissolvable elements is located closer to the center of the microarray and/or at least a portion of the dissolvable elements is located closer to the periphery of the microarray than each of the binding elements. Alternatively, the dissolvable and immovable elements may be provided similarly or mirrored in areas which may be duplicated.