公开(公告)号：US20130194670A1

公开(公告)日：2013-08-01

申请号：US13713990

申请日：2012-12-13

Applicant: Guardian Industries Corp.

Inventor： Liang LIANG ,  Chris LOVELL ,  Richard BLACKER ,  Mark A. LEWIS

IPC: B05D5/06 ,  G02B1/11

CPC classification number: B05D5/063 ,  B82Y30/00 ,  C03C1/008 ,  C03C17/007 ,  C03C17/3417 ,  C03C2217/213 ,  C03C2217/73 ,  C03C2217/732 ,  C03C2217/91 ,  C03C2218/113 ,  C03C2218/116 ,  C23C18/1212 ,  C23C18/1225 ,  C23C18/1245 ,  C23C18/1254 ,  C23C18/127 ,  C23C18/1283 ,  G02B1/11 ,  G02B2207/107 ,  G02B2207/109

Abstract: Certain examples relate to a method of making an antireflective (AR) coating supported by a glass substrate. The anti-reflection coating may include porous metal oxide(s) and/or silica, and may be produced using a sol-gel process. The pores may be formed and/or tuned in each layer respectively in such a manner that the coating ultimately may comprise a porous matrix, graded with respect to porosity. The gradient in porosity may be achieved by forming first and second layers using one or more of (a) nanoparticles of different shapes and/or sizes, (b) porous nanoparticles having varying pore sizes, and/or (c) compounds/materials of various types, sizes, and shapes that may ultimately be removed from the coating post-deposition (e.g., carbon structures, micelles, etc., removed through combustion, calcination, ozonolysis, solvent-extraction, etc.), leaving spaces where the removed materials were previously located.

Abstract translation: 某些实例涉及制​​备由玻璃基底支撑的抗反射（AR）涂层的方法。 防反射涂层可以包括多孔金属氧化物和/或二氧化硅，并且可以使用溶胶 - 凝胶法制备。 可以以这样的方式分别在各层中形成和/或调整孔，使得涂层最终可以包括相对于多孔性分级的多孔基质。 孔隙度的梯度可以通过使用一种或多种（a）不同形状和/或尺寸的纳米颗粒形成第一层和第二层来实现，（b）具有不同孔径的多孔纳米颗粒和/或（c） 可能最终从涂层后沉积（例如，通过燃烧，煅烧，臭氧分解，溶剂萃取等除去的碳结构，胶束等）中除去的各种类型，尺寸和形状，留下被移除的空间 材料以前位于。

公开(公告)号：US20130194668A1

公开(公告)日：2013-08-01

申请号：US13713811

申请日：2012-12-13

Applicant: GUARDIAN INDUSTRIES CORP.

Inventor： Liang LIANG ,  Richard BLACKER ,  Mark A. LEWIS ,  Nikhil KALYANKAR ,  Minh Huu LE

IPC: C03C17/22 ,  G02B1/11

CPC classification number: C03C17/22 ,  B82Y20/00 ,  B82Y40/00 ,  C03C1/008 ,  C03C17/3417 ,  C03C2217/213 ,  C03C2217/425 ,  C03C2217/452 ,  C03C2217/465 ,  C03C2217/478 ,  C03C2217/73 ,  C03C2217/732 ,  C03C2217/91 ,  C03C2218/113 ,  C03C2218/116 ,  G02B1/115 ,  G02B2207/107 ,  Y10S977/773

Abstract: Certain examples relate to a method of making an antireflective (AR) coating supported by a glass substrate. The anti-reflection coating may include porous metal oxide(s) and/or silica, and may be produced using a sol-gel process. The pores may be formed and/or tuned in each layer respectively in such a manner that the coating ultimately may comprise a porous matrix, graded with respect to porosity. The gradient in porosity may be achieved by forming first and second layers using one or more of (a) nanoparticles of different shapes and/or sizes, (b) porous nanoparticles having varying pore sizes, and/or (c) compounds/materials of various types, sizes, and shapes that may ultimately be removed from the coating post-deposition (e.g., carbon structures, micelles, etc., removed through combustion, calcination, ozonolysis, solvent-extraction, etc.), leaving spaces where the removed materials were previously located.

Abstract translation: 某些实例涉及制​​备由玻璃基底支撑的抗反射（AR）涂层的方法。 抗反射涂层可以包括多孔金属氧化物和/或二氧化硅，并且可以使用溶胶 - 凝胶法制备。 可以以这样的方式分别在各层中形成和/或调整孔，使得涂层最终可以包括相对于多孔性分级的多孔基质。 孔隙度的梯度可以通过使用一种或多种（a）不同形状和/或尺寸的纳米颗粒形成第一层和第二层来实现，（b）具有不同孔径的多孔纳米颗粒和/或（c） 可能最终从涂层后沉积中除去的各种类型，尺寸和形状（例如，通过燃烧，煅烧，臭氧分解，溶剂萃取等除去的碳结构，胶束等），留下被除去的空间 材料以前位于。

公开(公告)号：US20130108858A1

公开(公告)日：2013-05-02

申请号：US12278130

申请日：2007-01-31

Applicant: John Biteau ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Muriel Matheron ,  Lorraine Raboin

Inventor： John Biteau ,  Jean-Pierre Boilot ,  Thierry Gacoin ,  Muriel Matheron ,  Lorraine Raboin

IPC: B32B3/26 ,  B05D3/06 ,  B05D3/02 ,  B05D3/10

CPC classification number: G02B5/23 ,  C03C1/008 ,  C03C17/007 ,  C03C2217/425 ,  C03C2218/113 ,  C08J7/047 ,  C08J2483/00 ,  C09K9/02 ,  C09K2211/1029 ,  C09K2211/1033 ,  C09K2211/1088 ,  G03C1/73 ,  Y10T428/249953

Abstract: The present invention relates to a method for making a substrate coated with a mesoporous photochromic film, comprising: a) preparing a precursor sol of a mesoporous film comprising an inorganic precursor agent, at least one organic solvent, water, at least one pore-forming agent and one hydrophobic precursor agent bearing at least one hydrophobic group; b) depositing a film of the precursor sol onto a main surface of a substrate; c) removing the pore-forming agent from the film resulting from the previous step at a temperature ≦150° C.; d) impregnating the mesoporous film resulting from step c) with a solution comprising at least one photochromic agent. In an alternative embodiment, the photochromic agent is directly introduced into the precursor sol. In an alternative embodiment of the previous alternative embodiment, the precursor sol does not comprise any hydrophobic precursor agent but the photochromic film is made hydrophobic by a treatment subsequent to its preparation.

Abstract translation: 本发明涉及一种制备涂覆有介孔光致变色膜的基材的方法，包括：a）制备介孔膜的前体溶胶，所述介孔膜包含无机前体试剂，至少一种有机溶剂，水，至少一个成孔 剂和一种具有至少一个疏水基团的疏水性前体剂; b）将前体溶胶的膜沉积到基底的主表面上; c）在150℃的温度下从上一步骤得到的膜中除去造孔剂; d）用包含至少一种光致变色剂的溶液浸渍由步骤c）得到的介孔膜。 在替代实施方案中，将光致变色剂直接引入前体溶胶中。 在先前替代实施方案的替代实施方案中，前体溶胶不包含任何疏水性前体试剂，但是通过在其制备之后的处理使光致变色膜成为疏水性的。

公开(公告)号：US20130004762A1

公开(公告)日：2013-01-03

申请号：US13544904

申请日：2012-07-09

Applicant: SALAH BOUSSAAD ,  DAMIEN FRANCIS REARDON

Inventor： SALAH BOUSSAAD ,  DAMIEN FRANCIS REARDON

IPC: B32B15/04 ,  B32B17/06

CPC classification number: C23D5/02 ,  C03C1/008 ,  H01L31/03926 ,  H01L31/03928 ,  Y02E10/541 ,  Y02P70/521 ,  Y10T428/26

Abstract: The present disclosure relates to a method of manufacturing of a glass coated metal product. This invention also relates to a coated metallic substrate material that is suitable for manufacturing flexible solar cells and other articles in which a passivated stainless steel surface is desirable.

Abstract translation: 本公开涉及一种制造玻璃涂覆的金属产品的方法。 本发明还涉及一种适用于制造柔性太阳能电池的涂覆金属基底材料和其中需要钝化的不锈钢表面的其它制品。

公开(公告)号：US08329299B2

公开(公告)日：2012-12-11

申请号：US12059948

申请日：2008-03-31

Applicant: Sudipta Seal ,  Erik R. Brinley ,  Suresh Babu Krishna Moorthy ,  Abhilash Vincent ,  David Reid ,  Clara Rivero

Inventor： Sudipta Seal ,  Erik R. Brinley ,  Suresh Babu Krishna Moorthy ,  Abhilash Vincent ,  David Reid ,  Clara Rivero

IPC: B32B27/32 ,  B32B17/10 ,  B32B17/06 ,  B05D3/00 ,  B29C71/02

CPC classification number: C03C17/02 ,  C03C1/008 ,  C03C2203/26 ,  C03C2218/113 ,  G02B2207/109 ,  Y10T428/26 ,  Y10T428/265 ,  Y10T428/269 ,  Y10T428/31504

Abstract: A method for depositing sol-gel derived coatings on substrates to form coated substrates includes the steps of providing a first solution including at least one sol precursor and at least one solvent. A water comprising solution is added to the first solution to form a sol-gel. The sol-gel is deposited on a substrate. The sol-gel layer on the substrate is dried/cured at a temperature ≦100° C. for at least 10 minutes to form a solid layer, wherein the solid layer has a thickness from 50 nm to 110 nm. The depositing and curing steps are repeated at least once until combined thickness of the solid layers forms a coating of a predetermined thickness. The resulting solid layers are low water content layers that can be evidenced by transmission measurements. The coated substrate can be an IR transmissive substrate having a recrystallization temperature

Abstract translation: 用于在基底上沉积溶胶凝胶衍生的涂层以形成涂覆的基底的方法包括提供包括至少一种溶胶前体和至少一种溶剂的第一溶液的步骤。 向第一溶液中加入包含水的溶液以形成溶胶 - 凝胶。 溶胶 - 凝胶沉积在基底上。 将衬底上的溶胶 - 凝胶层在温度为100℃，100℃下干燥/固化至少10分钟以形成固体层，其中固体层具有50nm至110nm的厚度。 沉积和固化步骤重复至少一次，直到固体层的组合厚度形成预定厚度的涂层。 所得固体层是低含水层，可以通过透射测量来证明。 涂覆的基板可以是具有重结晶温度<130℃的IR透射基板，并且每个固体层在λ= 2950nm处提供透射，如果放置在≥99％的IR透射基底上则为法向入射和1mW功率， 的传输直接通过IR透射基板。

公开(公告)号：US20120282415A1

公开(公告)日：2012-11-08

申请号：US13286634

申请日：2011-11-01

Applicant: Raymond Nicholas Vrtis ,  Mark Leonard O'Neill ,  Jean Louise Vincent ,  Aaron Scott Lukas ,  Mary Kathryn Haas

Inventor： Raymond Nicholas Vrtis ,  Mark Leonard O'Neill ,  Jean Louise Vincent ,  Aaron Scott Lukas ,  Mary Kathryn Haas

IPC: C23C16/56 ,  C08K5/5425

CPC classification number: C23C16/401 ,  C03C1/008 ,  C09D7/63 ,  C23C16/30 ,  C23C16/402 ,  C23C16/56 ,  C23C30/00 ,  H01L21/02126 ,  H01L21/02203 ,  H01L21/02208 ,  H01L21/02214 ,  H01L21/02216 ,  H01L21/02274 ,  H01L21/02348 ,  H01L21/31695

Abstract: A chemical vapor deposition method for producing a porous organosilica glass film comprising: introducing into a vacuum chamber gaseous reagents including at least one precursor selected from the group consisting of an organosilane and an organosiloxane, and a porogen that is distinct from the precursor; applying energy to the gaseous reagents in the vacuum chamber to induce reaction of the gaseous reagents to deposit a preliminary film on the substrate, wherein the preliminary film contains the porogen; and removing from the preliminary film substantially all of the porogen to provide the porous film with pores and a dielectric constant less than 2.6.

Abstract translation: 一种用于生产多孔有机硅玻璃膜的化学气相沉积方法，包括：向真空室中引入包含至少一种选自有机硅烷和有机硅氧烷的前体的气态试剂和与前体不同的致孔剂; 向真空室中的气态试剂施加能量以诱导气态试剂在衬底上沉积初步膜的反应，其中预备膜含有致孔剂; 并且从基本上所有的致孔剂的初步膜上除去，以提供具有小于2.6的孔隙和介电常数的多孔膜。

公开(公告)号：US08262936B2

公开(公告)日：2012-09-11

申请号：US12883712

申请日：2010-09-16

Applicant: Kyung Nam Kim ,  Tomizo Matsuoka ,  Mi Youn Chang

Inventor： Kyung Nam Kim ,  Tomizo Matsuoka ,  Mi Youn Chang

IPC: C09K11/70

CPC classification number: C09K11/025 ,  C03C1/008 ,  C03C17/007 ,  C09K11/0883 ,  C09K11/642 ,  C09K11/7731 ,  C09K11/7734 ,  C09K11/7774 ,  C09K11/883 ,  H01L33/502 ,  H01L2224/48091 ,  H01L2224/48247 ,  H01L2924/181 ,  H01L2924/00014 ,  H01L2924/00012

Abstract: A phosphor is formed with a glass coating layer on a surface of a phosphor grain to have improved moisture and/or thermal stability. A method for manufacturing the phosphor comprises preparing phosphor gains excitable by light, and forming a glass coating layer on a surface of each phosphor grain. The glass coating layer may be formed by mixing the phosphor grains with a glass composition; heat-treating a mixture of the phosphor grains and the glass composition to make the glass composition melt and surround the phosphor grains; and cooling and breaking the heat-treated mixture to provide phosphors, each comprising the phosphor grain having the glass coating layer formed on a surface of the phosphor grain.

公开(公告)号：US08084123B2

公开(公告)日：2011-12-27

申请号：US11885328

申请日：2006-03-01

Applicant: Laurence Beaurain ,  Philippe Prene ,  Yves Montouillout ,  Philippe Belleville

Inventor： Laurence Beaurain ,  Philippe Prene ,  Yves Montouillout ,  Philippe Belleville

IPC: C09K3/10 ,  B01J13/00 ,  C08J3/03 ,  C08J3/09

CPC classification number: C23C18/00 ,  C03C1/008 ,  C03C2203/27 ,  C03C2203/30 ,  C23C18/04 ,  C23C18/1208 ,  C23C18/1241 ,  C23C18/1254 ,  C23C18/14 ,  F24S23/82 ,  Y10T428/26 ,  Y10T428/265 ,  Y10T428/31678

Abstract: The invention relates to a process for preparing a stable sol-gel solution. The solution may be used to form coating materials for metallic substrates, such as silver-based substrates for use in mirrors. The process includes the steps of preparing a sol-gel solution by bringing one or more molecular metal and/or metalloid precursors into contact with a medium comprising an organic solvent, adding at least one mercaptoorganosilane compound to the solution, hydrolyzing the solution obtained, and then adding one or more complexing agents to the solution.

Abstract translation: 本发明涉及制备稳定的溶胶 - 凝胶溶液的方法。 该溶液可用于形成用于金属基材的涂料，例如用于反射镜的银基底材。 该方法包括通过使一种或多种分子金属和/或准金属前体与包含有机溶剂的介质接触来制备溶胶 - 凝胶溶液的步骤，向溶液中加入至少一种巯基有机硅烷化合物，水解所获得的溶液，和 然后在溶液中加入一种或多种络合剂。

公开(公告)号：US20110183838A1

公开(公告)日：2011-07-28

申请号：US13078473

申请日：2011-04-01

Applicant: GUOYI FU ,  BillieJo M. Monk ,  Robert McIntyre

Inventor： GUOYI FU ,  BillieJo M. Monk ,  Robert McIntyre

IPC: B01J31/38 ,  B01J37/04 ,  B01J37/03

CPC classification number: C04B41/65 ,  B01J21/063 ,  B01J35/0013 ,  B01J35/004 ,  B01J37/0219 ,  B01J37/031 ,  C01G23/053 ,  C01P2004/64 ,  C01P2006/22 ,  C03C1/008 ,  C03C17/02 ,  C03C2203/32 ,  C03C2218/113 ,  C04B41/009 ,  C04B41/5041 ,  C04B2111/00827 ,  Y10S516/922 ,  C04B41/4537 ,  C04B41/4549 ,  C04B28/02

Abstract: A method of preparing stable, transparent photocatalytic titanium dioxide sots is disclosed which involves thermal treatment of a suspension of amorphous titanium dioxide in the presence of certain alpha-hydroxy acids. The sots comprise titanium dioxide particles in the anatase form having a crystallite size less than about 10 nm and exhibit excellent stability and transparency at basic, neutral, and acid pH.

Abstract translation: 公开了一种制备稳定，透明的光催化二氧化钛沉淀物的方法，其涉及在某些α-羟基酸存在下热处理无定形二氧化钛的悬浮液。 所述沉淀物包含具有小于约10nm的微晶尺寸的锐钛矿形式的二氧化钛颗粒，并且在碱性，中性和酸性pH下表现出优异的稳定性和透明度。

公开(公告)号：US07937968B2

公开(公告)日：2011-05-10

申请号：US11038789

申请日：2005-01-18

Applicant: Armin Maul ,  Thorsten Herbert ,  Jürgen Weber ,  Waltraud Werdecker ,  Rolf Gerhardt

Inventor： Armin Maul ,  Thorsten Herbert ,  Jürgen Weber ,  Waltraud Werdecker ,  Rolf Gerhardt

IPC: C03B19/01 ,  C03B19/06 ,  C03C17/02 ,  C03C27/00

CPC classification number: C03C1/008 ,  C03B19/06 ,  C03B37/0126 ,  C03C27/06 ,  C03C27/10

Abstract: In a known method for bonding components made of material with a high silicic acid content by means of a substance to substance bond, a SiO2-containing bonding mass is formed between connecting surfaces of the components. In order to provide for cost-efficient manufacture of a thermally stable composite, the invention proposes to generate a SiO2-containing bonding mass that is generic with regard to the material with a high silicic acid content, comprising the following procedural steps: provision of a slurry containing amorphous SiO2 particles; formation of a slurry mass between the connecting surfaces which are fixed in position with regard to each other; drying of the slurry mass; and solidification of the slurry mass by heating under formation of the SiO2-containing bonding mass. A component assembly manufactured according to the method of the invention shows high temperature resistance and thermal fatigue resistance and can also be used in contamination-sensitive applications. The component assembly is characterized by an amorphous SiO2-containing bonding mass, whose chemical composition is generic with regard to the material with the high silicic acid content of the basic material of the components, whereby the specific density of the SiO2-containing bonding mass is at least 2.0 g/cm3.

Abstract translation: 在通过物质与物质接合的用于将由高硅酸含量的材料制成的部件的已知方法中，在部件的连接表面之间形成含SiO 2的粘结物质。 为了提供热稳定复合材料的成本有效的制造，本发明提出产生相对于具有高硅酸含量的材料而言通用的含SiO 2的粘结物质，包括以下程序步骤：提供 含有无定形SiO 2颗粒的浆料; 在连接表面之间形成相对于彼此固定的位置的浆料; 干燥浆料; 并在形成含SiO 2的结合物质的同时通过加热固化浆料。 根据本发明的方法制造的组件组件显示出耐高温性和耐热疲劳性，并且还可以用于污染敏感的应用中。 组分组合物的特征在于含有非晶态SiO 2的结合物质，其化学组成对于组分的碱性材料的高硅酸含量的材料而言是通用的，由此含SiO 2的粘合物质的比密度为 至少2.0g / cm 3。