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    Method for preparing carbonylic perfluoropolyethers
    1.
    发明授权
    Method for preparing carbonylic perfluoropolyethers 有权
    制备羰基全氟聚醚的方法

    公开(公告)号：US09249260B2

    公开(公告)日：2016-02-02

    申请号：US12595037

    申请日：2008-04-08

    Applicant: Ugo De Patto ,  Giuseppe Marchionni ,  Pier Antonio Guarda

    Inventor： Ugo De Patto ,  Giuseppe Marchionni ,  Pier Antonio Guarda

    IPC: C07C43/30 ,  C07C53/46 ,  C08G65/00 ,  C08G65/322

    CPC classification number: C08G65/007 ,  C08G65/322

    Abstract: A process for preparing perfluoropolyethers of formula T-O—(RF)z-T′  (I) wherein: T, T' are end groups, z=0 or 1; RF is a perfluoro(poly)oxyalkylene chain containing one or more fluorooxyalkylene repeating units selected from the group consisting of (CF2O), —(CF(CF3)O)—, —(CF2CF2O)—, —(CF2CF(CF3)O)—, —(CF(CF3)CF2O)—, —(CF2CF2CF2O)—, —(CF2CF2CF2CF2O)—, and —(CF2)j—CFZ—O— wherein j is an integer from 0 to 3, and Z is a fluorooxyalkylene chain comprising from 1 to 20 repeating units selected from the above reported fluorooxyalkylene units; comprising the reduction of peroxidic perfluoropolyethers comprising one or more of the above defined repeating units by using gaseous hydrogen in the presence of a catalyst comprising one or more metals of the VIII group supported on graphitic materials.

    Abstract translation: 制备式T-O-（RF）z-T'（I）的全氟聚醚的方法，其中：T，T'是端基，z = 0或1; RF是包含选自（CF 2 O）， - （CF（CF 3）O） - ， - （CF 2 CF 2 O） - ， - （CF 2 CF（CF 3）O）中的一种或多种氧代烯烃重复单元的全氟（聚）氧化烯链， - （CF（CF 3）CF 2 O） - ， - （CF 2 CF 2 CF 2 O） - ， - （CF 2 CF 2 CF 2 CF 2 O） - 和 - （CF 2）j-CFZ-O-其中j为0至3的整数，Z为氟氧化烯 链，其包含1至20个选自上述氟氧化烯单元的重复单元; 包括通过在包含一种或多种负载在石墨材料上的VIII族的金属的催化剂存在下使用气态氢来还原包含一个或多个上述定义的重复单元的过氧化全氟聚醚。

    Immobilized heteropoly acids and the use of the same for electrode stabilization and enhancement
    3.
    发明授权
    Immobilized heteropoly acids and the use of the same for electrode stabilization and enhancement 有权
    固定化的杂多酸和使用它们用于电极稳定和增强

    公开(公告)号：US08753997B2

    公开(公告)日：2014-06-17

    申请号：US12122529

    申请日：2008-05-16

    Applicant: Ronald Justin Stanis ,  Andrew Michael Herring ,  Mei-Chen Kuo ,  Jack Richard Ferrell, III

    Inventor： Ronald Justin Stanis ,  Andrew Michael Herring ,  Mei-Chen Kuo ,  Jack Richard Ferrell, III

    IPC: B01J21/00 ,  C07C319/00 ,  C07C43/30

    CPC classification number: H01G11/30 ,  H01M4/8657 ,  H01M4/8892 ,  H01M4/9008 ,  H01M4/9016 ,  H01M4/9075 ,  H01M8/1004 ,  H01M2008/1095 ,  Y02E60/13 ,  Y02E60/523

    Abstract: The use of fuel cells to produce electricity are known as an environmentally clean and reliable source of energy, and show promise as an automotive power source if the polymer electrolyte membrane fuel cell can be made less expensive, more durable, reduce or eliminate humidification of the reactive gases, and operate at temperatures encountered during automotive operating conditions. The use of an electro-catalyst formed from heteropoly acids immobilized by a conductive material, such as carbon or platinum black, and stabilizing a metallic black with the immobilized conductive material addressed these automotive fuel cell needs. Coating the fuel cell electrode, polymer electrolyte assembly with a nano-particle catalyst derived from a heteropoly acid provided anodic carbon monoxide tolerance at anodic overpotentials and an active cathodic oxygen reduction. The heteropoly acids can also function as supercapacitor electrode films.

    Abstract translation: 将燃料电池用于生产电力被称为环境清洁和可靠的能源，并且如果聚合物电解质膜燃料电池可以制造成更便宜，更耐用，减少或消除加湿 反应气体，并在汽车操作条件下遇到的温度下运行。 使用由诸如碳或铂黑等导电材料固定的杂多酸形成的电催化剂和用固定的导电材料稳定金属黑以满足这些汽车燃料电池的需要。 用衍生自杂多酸的纳米颗粒催化剂涂覆燃料电池电极，聚合物电解质组件，在阳极超电势下提供阳极一氧化碳耐受性和活性阴极氧还原。 杂多酸也可以用作超级电容器电极膜。

    Process for production of benzaldehyde compound
    5.
    发明授权
    Process for production of benzaldehyde compound 有权
    苯甲醛化合物生产工艺

    公开(公告)号：US08258349B2

    公开(公告)日：2012-09-04

    申请号：US12863759

    申请日：2009-01-30

    Applicant: Koichi Nakazawa

    Inventor： Koichi Nakazawa

    IPC: C07C45/00 ,  C07C43/30

    CPC classification number: C07C45/515 ,  C07C41/16 ,  C07C41/52 ,  C07C43/225 ,  C07C43/315 ,  C07C47/575

    Abstract: A benzaldehyde acetal compound of formula (3): (wherein Q represents a hydrogen atom or a halogen atom, Ar represents a phenyl group optionally substituted with at least one selected from the group consisting of alkyl groups having 1 to 4 carbon atoms and halogen atoms, and R represents an alkyl group having 1 to 4 carbon atoms).

    Abstract translation: 式（3）的苯甲醛缩醛化合物：（其中Q表示氢原子或卤素原子，Ar表示任选被至少一个选自具有1至4个碳原子的烷基和卤素原子取代的苯基） ，R表示碳原子数为1〜4的烷基）。

    METHOD FOR PREPARING (E3,Z5)-3,5-ALKADIENYL ACETATE
    6.
    发明申请
    METHOD FOR PREPARING (E3,Z5)-3,5-ALKADIENYL ACETATE 有权
    制备（E3，Z5）-3,5-亚氨基乙酸酯的方法

    公开(公告)号：US20100069664A1

    公开(公告)日：2010-03-18

    申请号：US12620981

    申请日：2009-11-18

    Applicant: Miyoshi Yamashita ,  Takehiko Fukumoto

    Inventor： Miyoshi Yamashita ,  Takehiko Fukumoto

    IPC: C07C43/30 ,  C07C41/48 ,  C07C67/24

    CPC classification number: C07C41/48 ,  C07C29/10 ,  C07C41/50 ,  C07C67/08 ,  C07C69/007 ,  C07C69/145 ,  C07C33/02 ,  C07C43/30

    Abstract: Provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate and (E3,Z5)-3,5-dodecadienyl acetate which is a sex pheromone of Brazilian apple leafminer. Specifically, provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate, comprising steps of hydrolyzing 5,5-diethoxy-(Z3)-3-pentenyl methoxymethyl ether in the presence of an acid to obtain 4-formyl-(E3)-butenyl methoxymethyl ether; reacting the 4-formyl-(E3)-butenyl methoxymethyl ether with alkylidene triphenylphosphorane in accordance with the Wittig reaction to obtain (E3,Z5)-3,5-alkadienyl methoxymethyl ether; and obtaining (E3,Z5)-3,5-alkadienyl acetate using the (E3,Z5)-3,5-alkadienyl methoxymethyl ether as a starting substance.

    Abstract translation: 提供一种制备（E3，Z5）-3,5-链二烯酸乙酸酯和（E3，Z5）-3,5-十二烷基乙酸酯的方法，其是巴西苹果叶片的性信息素。 具体地说，提供了制备（E3，Z5）-3,5-链二烯基乙酸酯的方法，包括在酸存在下水解5,5-二乙氧基 - （Z 3）-3-戊烯基甲基甲基醚的步骤，得到4- 甲酰基 - （E3） - 丁烯基甲氧基甲基醚; 根据Wittig反应使4-甲酰基 - （E3） - 丁烯基甲氧基甲基醚与亚烷基三苯基正膦反应，得到（E3，Z5）-3,5-二甲氧基甲基醚; 并使用（E3，Z5）-3,5-链二烯基甲氧基甲基醚作为起始物质获得（E3，Z5）-3,5-链二烯酸乙酯。

    Method for preparing polymethoxymethylal
    7.
    发明授权
    Method for preparing polymethoxymethylal 有权
    制备聚甲氧基甲基的方法

    公开(公告)号：US07560599B2

    公开(公告)日：2009-07-14

    申请号：US12180594

    申请日：2008-07-28

    Applicant: Jing Chen ,  Zhonghua Tang ,  Chungu Xia ,  Xinzhi Zhang ,  Zhen Li

    Inventor： Jing Chen ,  Zhonghua Tang ,  Chungu Xia ,  Xinzhi Zhang ,  Zhen Li

    IPC: C07C43/30 ,  C07C43/303

    CPC classification number: C08G2/10 ,  C07C41/56 ,  C07C43/30

    Abstract: This invention describes a method for preparing polymethoxymethylal. By this method, polymethoxymethylal is prepared by a catalytic reaction using methanol and trioxymethylene as reactants and using an ionic liquid as catalyst under a relatively moderate reaction condition. The catalyst of this invention has a high catalytic activity and a high conversion; the reaction process is simple, easy to be operated and has a strong controllability; the distribution of the products after reaction is superior and the utilization ratio of the raw materials is high.

    Abstract translation: 本发明描述了制备聚甲氧基甲基的方法。 通过该方法，通过使用甲醇和三氧化甲烯作为反应物的催化反应制备聚甲氧基甲基，并在相对适中的反应条件下使用离子液体作为催化剂。 本发明的催化剂具有高催化活性和高转化率; 反应过程简单，操作方便，可控性强; 反应后产物的分布优越，原料利用率高。

    Molecules to Enhance Percutaneous Delivery and Methods for Discovery Therefor
    8.
    发明申请
    Molecules to Enhance Percutaneous Delivery and Methods for Discovery Therefor 审中-公开
    分子增强经皮递送及其发现方法

    公开(公告)号：US20090105260A1

    公开(公告)日：2009-04-23

    申请号：US11883606

    申请日：2006-01-17

    Applicant: Samir Mitragotri ,  Pankaj Karande ,  Amit K. Jain

    Inventor： Samir Mitragotri ,  Pankaj Karande ,  Amit K. Jain

    IPC: A61K31/53 ,  C07D251/26 ,  C07C43/30 ,  C07D211/06 ,  A61K31/445 ,  A61K31/03 ,  G06F19/00 ,  G01N21/25 ,  A61K31/495 ,  A61K31/075 ,  C07D241/04 ,  C07C17/00

    CPC classification number: A61B5/411 ,  A61B5/0075 ,  A61B5/445 ,  G01N21/35 ,  G16C20/30

    Abstract: An IR spectroscopic technique provides methods for measuring the irritation potential of a formulation and to assess the ability of molecules to enhance the permeability of substances into and through skin using samples comprising stratum corneum. Molecules are screened for their performance as chemical penetration enhancers using a unique in silico procedure that may be applied iteratively in an attempt to generate molecules showing successively higher performance. Both the irritation potential and the ability of the molecule to enhance penetration are considered in the in silico approach. The invention provides specific molecules that may be used in topical or transdermal formulations to improve the delivery of actives. The structures of compounds of the invention include: Formulas (I), (II), (III), (IV), (V), (IV) and analogs thereof.

    Abstract translation: IR光谱技术提供了用于测量制剂的刺激电位的方法，并评估分子通过包含角质层的样品增强物质进入皮肤和通过皮肤的渗透性的能力。 使用独特的计算机程序筛选分子作为化学渗透增强剂的性能，其可以迭代地施用以试图产生显示连续更高性能的分子。 在计算机方法中考虑了刺激潜能和分子增强渗透能力。 本发明提供可用于局部或透皮制剂以改善活性物质递送的特定分子。 本发明化合物的结构包括：式（I），（II），（III），（IV），（V），（IV）及其类似物。

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