公开(公告)号：US20040132147A1

公开(公告)日：2004-07-08

申请号：US10614833

申请日：2003-07-09

申请人： KAO CORPORATION

发明人： Minoru Kase ,  Keiji Shibata ,  Eizo Maruyama

IPC分类号： C12P007/64 ,  C07C051/43

CPC分类号： C12P7/6472 ,  C11C1/005 ,  C11C1/08 ,  C11C3/02

摘要： The present invention provides a method for producing a saturated fatty acid and an unsaturated fatty acid, which comprises adding and mixing a polyglycerol ester of a fatty acid to a raw fatty acids mixture, cooling the resultant mixture to deposit crystals, and fractionating the saturated fatty acid and the unsaturated fatty acid, wherein a cooling procedure is performed at a cooling rate of 4null C./h or less when a supersaturation ratio is 60% or more and said cooling rate is varied during the cooling, and a glycerides mixture obtained from the fractionated unsaturated fatty acids. According to the present invention, a saturated fatty acid and an unsaturated fatty acid in a raw fatty acids mixture can be separated easily and efficiently by a dry fractionation process.

摘要翻译： 本发明提供饱和脂肪酸和不饱和脂肪酸的制造方法，其包括将脂肪酸的聚甘油酯与生脂肪酸混合物混合，冷却所得混合物以沉淀晶体，并将饱和脂肪酸 酸和不饱和脂肪酸，其中当过饱和比为60％以上并且所述冷却速度在冷却期间变化时，以4℃/小时以下的冷却速度进行冷却过程，得到甘油酯混合物 来自分级的不饱和脂肪酸。 根据本发明，原料脂肪酸混合物中的饱和脂肪酸和不饱和脂肪酸可以通过干馏分离方法容易且有效地分离。

公开(公告)号：US20040024233A1

公开(公告)日：2004-02-05

申请号：US10621202

申请日：2003-07-15

发明人： Toshio Endo

IPC分类号： C07C051/43

CPC分类号： A61Q19/00 ,  A61K8/39 ,  A61Q5/02 ,  A61Q11/00 ,  A61Q19/10 ,  C07C67/26 ,  C07C69/33 ,  C08K5/103 ,  C11D1/04 ,  C11D1/667

摘要： Disclosed are a fatty acid esters composition of a polyglycerine containing more than 70% of a fatty acid monoester which is defined by a specified analysis method, a process for the preparation thereof, a process for the preparation of a highly purified fatty esters composition of a polyglycerine, and a highly-purified fatty acid esters composition of a polyglycerine having an oxirane oxygen concentration of below 100 ppm which is defined by a specified analysis method. The fatty acid esters compositions of a polyglycerine are useful as additives for a variety of food-stuffs, additives for a variety of thermoplastic resins, and as additives for a variety of cosmetics or detergents.

摘要翻译： 公开了含有超过70％的脂肪酸​​单酯的聚甘油的脂肪酸酯组合物，其通过指定的分析方法定义，其制备方法，制备高纯度脂肪酸酯组合物的方法 聚甘油和通过特定分析方法定义的环氧乙烷氧浓度低于100ppm的聚甘油的高度纯化的脂肪酸酯组合物。 聚甘油的脂肪酸酯组合物可用作各种食品的添加剂，各种热塑性树脂的添加剂以及用于各种化妆品或洗涤剂的添加剂。

公开(公告)号：US20030083511A1

公开(公告)日：2003-05-01

申请号：US10194312

申请日：2002-07-15

发明人： Richard Neil Cawthorne ,  Robert William Humble ,  David Andrew Parker

IPC分类号： C07C051/43

CPC分类号： C07C51/487 ,  C07C53/126 ,  C07C59/01

摘要： A process for recovering 18-methyl eicosanoic acid (18-MEA) and/or alpha hydroxy acids (AHAs) from woolwax acids or derivatives thereof comprises the steps of heating the woolwax acids or derivatives thereof to 100null to 230null C. to form estolides and polymeric species; distilling to obtain a distillate (D1) and a residue (R1); and recovering 18-MEA from the distillate and/or recovering AHAs from the residue.

摘要翻译： 从羊蜡酸或其衍生物中回收18-甲基二十烷酸（18-MEA）和/或α-羟基酸（AHAs）的方法包括将羊毛酸或其衍生物加热至100℃至230℃以形成 耳tol体和聚合物种; 蒸馏得到馏出物（D1）和残余物（R1）; 并从馏出物中回收18-MEA和/或从残余物中回收AHAs。

公开(公告)号：US20030050492A1

公开(公告)日：2003-03-13

申请号：US10190263

申请日：2002-07-03

申请人： IP Holdings, L.L.C.

发明人： Dick Copeland ,  W. Maurice Belcher

IPC分类号： C11B003/00 ,  C07C051/43

CPC分类号： C11B3/14 ,  A23D9/00 ,  A23J7/00 ,  C07F9/103 ,  C11B3/00 ,  C11B3/001 ,  C11B3/006 ,  C11B3/04 ,  C11B3/10 ,  C11B3/12

摘要： The present invention relates to improved methods for refining vegetable oils. Vegetable oil is combined with organic acid and subjected to high shear to finely disperse the acid solution in the oil. The resulting acid-and-oil mixture is mixed at low shear for a time sufficient to sequester contaminants into a hydrated impurities phase, producing a purified vegetable oil phase.

摘要翻译： 本发明涉及精制植物油的改进方法。 植物油与有机酸结合，经高剪切力将酸溶液精细分散于油中。 将所得酸和油混合物在低剪切下混合足以将污染物螯合到水合杂质相中的时间，产生纯化的植物油相。

公开(公告)号：US20020198393A1

公开(公告)日：2002-12-26

申请号：US09992553

申请日：2001-11-06

发明人： Ralph S. Daniels ,  Monoj K. Gupta ,  Phillip L. McKinney

IPC分类号： C11B003/00 ,  C07C051/43

CPC分类号： C11B3/06

摘要： In refining crude vegetable oils, there are certain economic and quality advantages to refining the oils with potassium hydroxide. Lower overall cost is achieved from reduced levels of soap and trace impurities in the oil, improved refining yield for the oils refined with potassium hydroxide, higher retention of recoverable tocopherols in the oil, gentler reaction with triglyceride, lower mono and diglyceride in the potassium hydroxide soapstock, the option to convert a by-product of soapstock acidulation, into a profitable co-product and eliminate acid-water discharge from the soapstock acidulation process.

摘要翻译： 在精炼粗植物油时，用氢氧化钾精炼油具有一定的经济和质量优势。 较低的总体成本可以通过降低油中的皂和微量杂质水平来实现，提高用氢氧化钾精炼的油的精炼产率，油中可回收的生育酚的保留率更高，甘油三酯的温和反应，氢氧化钾中的较低的单酸甘油酯和甘油二酯 肥皂块，将肥皂片酸化的副产物转化为有利可图的副产品，并消除肥皂排放过程中的酸水排放。

公开(公告)号：US20040186307A1

公开(公告)日：2004-09-23

申请号：US10775996

申请日：2004-02-09

申请人： GMK-GESELLSCHAFT FUR MOTOREN

发明人： Aldo Piacentini ,  Rene Niesner

IPC分类号： C07C051/43

CPC分类号： C10L1/026 ,  B01J23/06 ,  B01J35/04 ,  B01J38/62 ,  C11C3/003 ,  F02F2007/0097 ,  Y02E50/13

摘要： The present invention is directed to a method of producing fuel from vegetable or animal fat having a free fatty acid content by means of catalytic esterification reactions. The method includes esterification of free fatty acids at a higher temperature in a vacuum with one or more multivalent alcohols accompanied by solid neutral catalysts, which are present in a packing bed inside a reactor, whereby the fat travels from top to bottom in the reactor with the alcohol(s) running counter current and a mixture containing alcohol and water being removed from an upper part of the reactor by means of a vacuum effect. The present invention is also directed to the apparatus for implementing the methods disclosed.

摘要翻译： 本发明涉及通过催化酯化反应从具有游离脂肪酸含量的植物或动物脂肪生产燃料的方法。 该方法包括在真空中较高温度下使用一种或多种伴随固体中性催化剂的多元醇酯化游离脂肪酸，所述多元醇存在于反应器内的填料床中，由此脂肪在反应器中从顶部向底部移动， 通过真空效应从反应器的上部除去运行逆流的醇和含有醇和水的混合物。 本发明还涉及用于实现所公开方法的装置。

公开(公告)号：US20040170658A1

公开(公告)日：2004-09-02

申请号：US10481890

申请日：2004-01-02

发明人： Pierre Charlier De Chily ,  Mikaele Raynard

IPC分类号： A61K007/00 ,  C07C051/43

CPC分类号： C07C57/02 ,  A61K8/31 ,  A61K8/922 ,  A61K9/0014 ,  A61K9/107 ,  A61K47/44 ,  A61Q1/06 ,  A61Q19/00 ,  C09D11/00 ,  C09G1/14 ,  C10M159/12 ,  C11C3/00 ,  C11C3/003 ,  C11C3/02 ,  C14C9/02

摘要： This invention proposes a lanolin substitute, capable of absorbing up to at least twice its weight of water or aqueous solution or aqueous suspension. It forms true emulsions, stable over time with a capacity for water absorption superior to that of lanolin. It also possesses the known emollient, moisturizing and occlusive properties of lanolin. This substitute is usable in all the present and future areas of application of lanolin: in the cosmetics industry, dermatology, and in industrial applications (polishes, lubricants . . . ). It is obtained by hemi-synthesis from a mixture of unsaturated fatty acids, esters of unsaturated fatty acids, unsaturated hydrocarbons or unsaturated derivatives of the latter and compounds comprising or generating hydroxyl functions, such as glycerol, preferably without a catalyst and in an atmosphere devoid of oxygen. Classical thermal treatment or preferably treatment by dielectric heating.

摘要翻译： 本发明提出一种羊毛脂替代物，其能够吸收至多两倍于其重量的水或水溶液或水悬浮液。 它形成真正的乳液，随着时间的推移具有稳定的吸水能力，优于羊毛脂。 它还具有羊毛脂已知的润肤剂，保湿和闭塞性质。 该替代物可用于羊毛脂的所有当前和未来应用领域：化妆品工业，皮肤病学和工业应用（抛光剂，润滑剂...）。 它是通过从不饱和脂肪酸，不饱和脂肪酸的酯，不饱和烃或后者的不饱和衍生物的混合物和包含或产生羟基官能团的化合物如甘油，优选不含催化剂和在无空气中的混合物中进行半合成而获得的 的氧气。 经典热处理或优选通过介电加热处理。

公开(公告)号：US20040122246A1

公开(公告)日：2004-06-24

申请号：US10699201

申请日：2003-10-31

发明人： Flemming Vang Sparso ,  Ulrik Engelrud

IPC分类号： C07C051/43

CPC分类号： C11B7/00 ,  A23D9/00 ,  C07C67/54 ,  C11B3/12 ,  C11B3/14 ,  C07C69/30

摘要： The present invention relates to a process for controlling the fatty acid chain composition of triglycerides wherein a feed stream comprises a mixture of triglycerides containing at least one long chain. Said mixture is substantially free of trishort chain triglycerides and it is treated in at least two fractionation steps to fractionate between long chain triglycerides at temperatures above 200null C. and pressures between 0.01 and 10 Pa, wherein one of said steps fractionates between trilong chain triglycerides and mono- and dilong chain triglycerides and the other one of said steps fractionates between monolong chain triglycerides and dilong chain triglycerides. The process can be used for the providing of target triglycerides having a controlled fatty acid chain distribution.

摘要翻译： 本发明涉及一种控制甘油三酯的脂肪酸链组成的方法，其中进料流包含含有至少一个长链的甘油三酯的混合物。 所述混合物基本上不含三链段甘油三酸酯，并且在至少两个分馏步骤中进行处理，以在高于200℃的温度和0.01至10Pa的压力下在长链甘油三酯之间分馏，其中所述步骤之一在三龙链甘油三酯之间分级 和单链和双链甘油三酸酯，并且所述步骤中的另一个步骤在单链甘油三酯和二链甘油三酯之间分级。 该方法可用于提供具有受控脂肪酸链分布的目标甘油三酯。

公开(公告)号：US20030236422A1

公开(公告)日：2003-12-25

申请号：US10382065

申请日：2003-03-05

发明人： Ralph S. Daniels

IPC分类号： C11B001/00 ,  C07C051/43

CPC分类号： C05G3/0064 ,  C05D9/02 ,  C05F5/006 ,  C05F7/00 ,  Y02A40/211 ,  Y02A40/213 ,  C05F11/00

摘要： A method of processing agricultural oil in which non-toxic reagents are used, so that a waste stream is evolved suitable for use as a nutrient source and wherein the non-toxic reagents include nutrient source and wherein the non-toxic reagents include nutrient components whereby the nutrient value of the waste stream is enhanced. A variation of convention refining is detailed in which potassium hydroxide is used as refining caustic instead of conventional sodium hydroxide. The resulting process exhibits improvements in waste wash characteristics, more complete oil recovery, less oil in the soapstock, reduced interlayer formation, more soap removed from the refined oil into the soapstock stream, and a less viscous soapstock.

摘要翻译： 一种处理农用油的方法，其中使用无毒试剂，使得废物流放出适合用作营养源，其中无毒试剂包括营养源，其中无毒试剂包括营养成分，由此 废物流的营养价值得到提高。 详细说明了常规精炼的变化，其中氢氧化钾用作澄清碱而不是常规的氢氧化钠。 所得到的方法表现出废水洗涤特性，更完全的油回收，较少的油渣，减少夹层形成，更多的皂从精制油进入皂液料流中的皂以及较不粘稠的皂屑。

公开(公告)号：US20030225304A1

公开(公告)日：2003-12-04

申请号：US10384596

申请日：2003-03-11

申请人： KAO CORPORATION

发明人： Taku Mumura ,  Hidetoshi Kadowaki ,  Futoshi Nishigaki

IPC分类号： C07C051/43 ,  C07C029/136

CPC分类号： C11C3/003 ,  C07C29/149 ,  C07C67/56 ,  C11C1/08 ,  C07C69/24 ,  C07C69/52 ,  C07C31/125

摘要： There is provided a process wherein a lower alkyl ester of a fatty acid derived from natural fats and oils and a lower alcohol containing 1 to 4 carbon atoms is produced in a lower sulfur content at lower costs without causing a reduction in yield and a deterioration in selectivity, as well as a process for producing an alcohol without reducing the activity of a catalyst. The process comprises the step of adsorption treatment of an ester with at least one adsorbent selected from clay and activated carbon. Further are provided a process for producing an ester which further comprises adsorption treatment with a hydrogenating decomposition-type adsorbent containing Ni and/or Cu, in hydrogen or a mixed gas atmosphere of hydrogen and an inert gas, and a process for producing an alcohol which comprises hydrogenation reaction with an ester produced by any one of these processes as the starting material.

摘要翻译： 提供了一种方法，其中以较低的成本生产来自天然脂肪和油的脂肪酸的低级烷基酯和含有1至4个碳原子的低级醇，而不会导致产率的降低和劣化 选择性，以及在不降低催化剂活性的情况下生产醇的方法。 该方法包括用选自粘土和活性炭的至少一种吸附剂吸附处理酯的步骤。 还提供了一种制备酯的方法，其还包括在氢气或惰性气体的氢气或混合气体气氛中用含有Ni和/或Cu的氢化分解型吸附剂进行吸附处理，以及制备醇的方法 包括与由这些方法中的任一种制备的酯作为起始原料的氢化反应。