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    Method and apparatus for producing a peroxyacid solution
    1.
    发明申请
    Method and apparatus for producing a peroxyacid solution 审中-公开
    用于制备过氧酸溶液的方法和装置

    公开(公告)号：US20050031530A1

    公开(公告)日：2005-02-10

    申请号：US10878176

    申请日：2004-06-28

    Applicant: Perry Martin

    Inventor： Perry Martin

    IPC: C01B15/06

    CPC classification number: C01B15/06

    Abstract: A method and apparatus for production of a high-concentration H2SO5 solution is presented. This high-concentration H2SO5 solution is useful for producing a stable, non-hygroscopic triple salt. The invention includes a single-stage reactor that includes a reservoir for holding an oxyacid solution and an inlet to the reservoir for receiving a peroxide solution. The peroxide solution is added such that a gradient of peroxide concentration forms in the oxyacid solution as a function of distance from the inlet, and less than all of the oxyacid solution reacts with the peroxide solution at a given time. A stirring mechanism slowly dissipates the gradient, so that any H2SO5 formed as a result of reaction between the peroxide and the oxyacid is stirred away from the high-peroxide concentration zone, thereby preventing the decomposition of H2SO5 by an equilibrium reaction. The temperature of the reservoir is maintained at less than or equal to 20 ° C.

    Abstract translation: 提出了一种生产高浓度H2SO4溶液的方法和装置。 该高浓度H2SO5溶液可用于生产稳定的非吸湿性三重盐。 本发明包括单级反应器，其包括用于保持含氧酸溶液的储存器和用于接收过氧化物溶液的储存器的入口。 添加过氧化物溶液，使得在含氧酸溶液中形成过氧化物浓度的梯度作为与入口的距离的函数，并且少于全部含氧酸溶液在给定时间与过氧化物溶液反应。 搅拌机构缓慢地消散梯度，使得由于过氧化物和含氧酸之间的反应而形成的任何H 2 SO 5被从高过氧化物浓度区域搅拌离开，从而通过平衡反应阻止H2SO4的分解。 储存器的温度保持在小于或等于20℃

    Hydrogen peroxide complexes of inorganic salts and synthesis thereof
    3.
    发明授权
    Hydrogen peroxide complexes of inorganic salts and synthesis thereof 失效
    无机盐的过氧化氢配合物及其合成

    公开(公告)号：US5820841A

    公开(公告)日：1998-10-13

    申请号：US716055

    申请日：1996-09-19

    Applicant: Xiaolan Chen ,  Paul Taylor Jacobs ,  Szu-Min Lin

    Inventor： Xiaolan Chen ,  Paul Taylor Jacobs ,  Szu-Min Lin

    IPC: A61L2/16 ,  A01N59/00 ,  A61L2/20 ,  C01B15/04 ,  C01B15/055 ,  C01B15/06 ,  C01B15/14 ,  C01B15/16 ,  C01B15/08

    CPC classification number: A61L2/208 ,  A01N59/00 ,  C01B15/06 ,  C01B15/14 ,  C01B15/16 ,  A61L2202/24

    Abstract: A method of making an inorganic salt-hydrogen peroxide complex includes the following steps: (a) mixing the inorganic salt with sufficient water for a time sufficient to form a soft paste, (b) mixing the paste with an aqueous hydrogen peroxide solution to form a hydrogen peroxide-containing paste, and (c) drying the hydrogen peroxide-containing paste. A hydrate method of making Na.sub.4 P.sub.2 O.sub.7.3H.sub.2 O.sub.2 includes the steps of: mixing sodium pyrophosphate decahydrate solid with an aqueous solution of hydrogen peroxide having a concentration of less than 30%, and drying the mixture. Compositions of matter include K.sub.2 HPO.sub.4.3H.sub.2 O.sub.2, KH.sub.2 PO.sub.4.H.sub.2 O.sub.2 Ca.sub.2 P.sub.2 O.sub.7.nH.sub.2 O.sub.2, Ca.sub.2 P.sub.2 O.sub.4.nH.sub.2 O.sub.2, Na.sub.2 SO.sub.4.nH.sub.2 O.sub.2, K.sub.2 SO.sub.4.nH.sub.2 O.sub.2, Na.sub.2 SiO.sub.3.nH.sub.2 O.sub.2 and Na.sub.2 SiO.sub.7.nH.sub.2 O.sub.2.

    Abstract translation: 制备无机盐 - 过氧化氢络合物的方法包括以下步骤：（a）将无机盐与足够的水混合足以形成软糊剂的时间，（b）将糊料与过氧化氢水溶液混合以形成 含有过氧化氢的糊剂，（c）干燥含过氧化氢的糊剂。 制备Na4P2O7.3H2O2的水合物方法包括以下步骤：将焦磷酸十水合物固体与浓度小于30％的过氧化氢水溶液混合，并干燥该混合物。 物质组成包括K2HPO4.3H2O2，KH2PO4H2O2 Ca2P2O7.nH2O2，Ca2P2O4.nH2O2，Na2SO4·nH2O2，K2SO4·nH2O2，Na2SiO3·nH2O2和Na2SiO7·nH2O2。

    Manufacture of peroxidic compositions
    7.
    发明授权
    Manufacture of peroxidic compositions 失效
    过氧化物组合物的制造

    公开(公告)号：US5429812A

    公开(公告)日：1995-07-04

    申请号：US70376

    申请日：1993-06-08

    Applicant: Colin F. McDonogh ,  Neil J. Sanders

    Inventor： Colin F. McDonogh ,  Neil J. Sanders

    IPC: C01B15/06 ,  C01B20060101 ,  C01B17/98

    CPC classification number: C01B15/06

    Abstract: Production of peroxomonosulphuric acid (Caro's acid) by reaction between concentrated hydrogen peroxide and sulphuric acid solutions can be impaired substantially when substoichiometric amounts of sulphuric acid are employed.The problem is ameliorated or removed by first forming a body of sulphuric acid-rich fluid (usually the smaller volume) and thereafter introducing into that body of fluid the hydrogen peroxide solution (usually the larger volume). The reaction mixture progressively becomes sulphuric acid-lean. The body of fluid is advantageously either concentrated sulphuric acid itself, or a premix formed by reaction between hydrogen peroxide and at least an equimolar amount of sulphuric acid. The process is particularly suitable for making Caro's acid when from 0.02 to 0.5 moles of sulphuric acid is employed per mole of hydrogen peroxide.

    Abstract translation: PCT No.PCT / GB91 / 02138 Sec。 371日期：1993年6月8日 102（e）日期1993年6月8日PCT 1991年12月3日PCT PCT。 公开号WO92 / 11200 日期：1992年7月9日。当使用亚化学计量的硫酸时，通过浓缩的过氧化氢和硫酸溶液之间的反应生产过氧硫酸（卡罗酸）。 通过首先形成一个富含硫酸的流体（通常较小的体积），然后将该过氧化氢溶液（通常较大的体积）引入该体内的流体来改善或去除该问题。 反应混合物逐渐变成贫硫酸。 流体本身有利地是浓硫酸本身或由过氧化氢和至少等摩尔量的硫酸之间的反应形成的预混合物。 当每摩尔过氧化氢使用0.02至0.5摩尔硫酸时，该方法特别适用于制备Caro酸。

    Process for generating an oxidizing reagent for the treatment of polluted water
    8.
    发明授权
    Process for generating an oxidizing reagent for the treatment of polluted water 失效
    用于生产用于处理污染水的氧化试剂的方法

    公开(公告)号：US3900555A

    公开(公告)日：1975-08-19

    申请号：US38081573

    申请日：1973-07-19

    Applicant: AIR LIQUIDE

    Inventor： JOURDAN-LAFORTE ERIC

    IPC: C01B15/08 ,  B01J4/02 ,  C01B15/06 ,  C02F1/72 ,  C02F1/78 ,  C25D21/18 ,  C02B1/34 ,  C01B21/12

    CPC classification number: C02F1/72 ,  C01B15/06 ,  C02F1/722

    Abstract: A process for obtaining monopersulphuric acid from hydrogen peroxide and sulphuric acid is disclosed. Hydrogen peroxide in the form of an aqueous solution with a concentration ranging from 35 to 100% and either concentrated sulphuric acid or fuming sulphuric acid are added simultaneously to a reaction vessel. The temperature of the reaction is maintained in the range -10*C to +80*C and the supply of the hydrogen peroxide and sulphuric acid to the reaction vessel is controlled so that the generation of the monoperoxysulphuric acid occurs when required and the quantity thereof produced is adjusted according to the quantity thereof required for reaction with another reactant, for example a pollutant, the concentration of the monoperoxysulphuric acid being substantially constant.

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