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公开(公告)号:US20240355515A1
公开(公告)日:2024-10-24
申请号:US18548206
申请日:2022-01-17
发明人: Weiguo Mou , Jiaying Huang
IPC分类号: H01F1/057 , B22F3/16 , B22F3/24 , B22F9/02 , B22F9/04 , C21D1/84 , C21D6/00 , C22C33/04 , C22C38/00 , C22C38/10 , C22C38/12 , C22C38/14 , C22C38/16 , H01F41/02
CPC分类号: H01F1/0577 , B22F3/16 , B22F3/24 , B22F9/023 , B22F9/04 , C21D1/84 , C21D6/007 , C22C33/04 , C22C38/002 , C22C38/005 , C22C38/10 , C22C38/12 , C22C38/14 , C22C38/16 , H01F41/0293 , B22F2003/248 , B22F2009/044 , B22F2202/05 , B22F2301/355 , B22F2998/10 , B22F2999/00 , C22C2202/02
摘要: Disclosed are an R-T-B magnet and a preparation method therefor. The R-T-B magnet comprises the following components: R≥29 wt. %, R being a rare earth element and containing Nd, wherein Nd is ≥22 wt. %; 0.2-0.75 wt. % of Ti+Nb; 0.05-0.45 wt. % of Cu; 0.955-1.15 wt. % of B; and 58-69 wt. % of Fe, wherein wt. % is the ratio of the mass of each component to the total mass of the components; and the mass ratio of Ti to Nb is (1-5):1. According to the present invention, the matching relationship among the added elements in the R-T-B magnet is further optimized, and an R-T-B magnet with better magnetic properties such as relatively high residual magnetization, coercivity, and squareness can be prepared by using the formula.
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2.
公开(公告)号:US20240274333A1
公开(公告)日:2024-08-15
申请号:US18568831
申请日:2022-06-13
发明人: Bingqiang SHI , Zhongxin AN , Chubo DENG , Lei LIU , Yanmei JIN
IPC分类号: H01F1/057 , B22F3/16 , B22F3/24 , B22F9/02 , B22F9/04 , C22C33/02 , C22C35/00 , C22C38/00 , C22C38/06 , C22C38/14 , C22C38/16 , H01F41/02
CPC分类号: H01F1/0577 , B22F3/16 , B22F3/24 , B22F9/023 , B22F9/04 , C22C33/0207 , C22C33/0278 , C22C35/005 , C22C38/002 , C22C38/005 , C22C38/06 , C22C38/14 , C22C38/16 , H01F41/0266 , H01F41/0293 , B22F2003/248 , B22F2009/044 , B22F2201/20 , B22F2202/05 , B22F2301/355 , B22F2304/10 , B22F2998/10 , B22F2999/00 , C22C2202/02
摘要: A low-cost high-coercivity LaCe-rich neodymium-iron-boron permanent magnet, and a preparation method therefor and the use thereof are provided. The permanent magnet is prepared by mixing and sintering an LaCe-free and HRE-free neodymium-iron-boron main phase alloy and an LaCe-M alloy. An LaCe-free main phase alloy and an LaCe-M auxiliary phase alloy are respectively smelted at first, and then, the same are subjected to powder preparation, mixing, pressing, and sintering, thereby avoiding LaCe entering main phase crystal grains. The depth and concentration of HRE diffused into the magnet are effectively improved by using the characteristics of a low melting point and high flowability of an LaCe-rich crystal boundary phase, thereby improving the uniformity of components and structure distribution in the magnet.
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公开(公告)号:US11869690B2
公开(公告)日:2024-01-09
申请号:US17578856
申请日:2022-01-19
发明人: Noritsugu Sakuma , Tetsuya Shoji , Akihito Kinoshita , Akira Kato
CPC分类号: H01F1/0577 , C22C38/005 , C22C38/10 , H01F41/0293 , C22C2202/02 , H01F41/0266
摘要: A rare earth magnet in which the amount used of a heavy rare earth element is more reduced while maintaining enhancement of the coercive force, and a producing method thereof are provided. The rare earth magnet of the present disclosure has a main phase 10 and a grain boundary phase 20. The main phase 10 has a composition represented by R12T14B. The main phase 10 has a core part 12 and a shell part 14. Denoting the abundances of R2 and Ce (R2 is heavy rare earth element) occupying 4f site of the shell part 14 as R24f and Ce4f, respectively, and denoting the abundances of R2 and Ce occupying 4g site of the shell part 14 as R24g and Ce4g, respectively, the rare earth magnet satisfies 0.44≤R24g/(R24f+R24g)≤0.70 and 0.04≤(Ce4f+Ce4g)/(R24f+R24g). The rare earth magnet-producing method of the present disclosure uses a modifier containing at least R2 and Ce.
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公开(公告)号:US11810698B2
公开(公告)日:2023-11-07
申请号:US15742460
申请日:2016-06-29
发明人: Tuncay Celik
CPC分类号: H01F1/0577 , H01F41/0293
摘要: Magnets and systems, methods, and techniques for manufacturing magnets are provided. In some embodiments, methods of manufacturing magnets comprise providing a rare earth magnetic body, depositing a bead of dysprosium or terbium metal onto a part of the magnetic body to form a magnet; and heat-treating the magnet. In some embodiments, a magnet is provided comprising a magnetic body and a bead of dysprosium or terbium metal. In some embodiments, the magnetic body contains grains of rare earth magnet alloy, and the bead of dysprosium or terbium metal is deposited onto a part only of a surface of the magnetic body.
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公开(公告)号:US20230144451A1
公开(公告)日:2023-05-11
申请号:US17906446
申请日:2021-03-18
发明人: Tadao NOMURA , Kazuki OTSUKA , Masayuki KAMATA
CPC分类号: H01F1/0593 , B22F3/12 , B22F3/24 , H01F41/0293 , H01F41/0266 , C22C38/10 , C22C2202/02
摘要: An anisotropic rare earth sintered magnet represented by the formula (R1-aZra)x(Fe1-b COb)100-x-y(M11-cM2c)y where R is at least one element selected from rare earth elements and Sm is essential; M1 is at least one of V, Cr, Mn, Ni, Cu, Zn, Ga, Al, and Si; M2 is at least one of Ti, Nb, Mo, Hf, Ta, and W; and x, y, a, b, and c each satisfy certain conditions. The anisotropic rare earth sintered magnet includes 80% by volume or more of a main phase composed of a compound of a ThMn12 type crystal, the main phase having an average crystal grain size of 1 μm or more, and containing an R-rich phase and an R(Fe,Co)2 phase in a grain boundary portion. A method for producing the anisotropic rare earth sintered magnet is also described.
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公开(公告)号:US20180286545A1
公开(公告)日:2018-10-04
申请号:US15939778
申请日:2018-03-29
申请人: TDK CORPORATION
发明人: Yoshinori FUJIKAWA , Masashi MIWA
CPC分类号: H01F1/0577 , C22C38/005 , H01F41/0293
摘要: An R-T-B based sintered magnet including a plural number of main phase particles having an R2T14B type crystal structure. R is at least one rare earth element essentially including heavy rare earth elements RH, T is at least one transition metal element essentially including Fe or Fe and Co, and B is boron. At least one of the main phase particles is a reverse core-shell main phase particle including a core part and a shell part, in which CRC/CRS>1.0 is satisfied when a total RH concentration (at %) in the core part is defined as CRC and a total RH concentration (at %) in the shell part is defined as CRS. An existence ratio of the reverse core-shell main phase particles is larger in a surface layer part of the magnet than in a central part of the magnet.
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公开(公告)号:US20180247743A1
公开(公告)日:2018-08-30
申请号:US14534758
申请日:2014-11-06
发明人: Wanfeng LI
CPC分类号: H01F41/0293 , C22C1/02 , H01F1/0577
摘要: Magnets and methods of making the magnets are disclosed. The magnets may have high coercivity and may be suitable for high temperature applications. The magnet may include a plurality of grains of a Nd—Fe—B alloy having a mean grain size of 100 to 500 nm. The magnet may also comprise a non-magnetic low melting point (LMP) alloy, which may include a rare earth element and one or more of Cu, Ga, and Al. The magnets may be formed from a Nd—Fe—B alloy powder produced using HDDR and jet milling, or other pulverization process. The powder may have a refined grain size and a small particle size and particle size distribution. The LMP alloy may be mixed with a powder of the Nd—Fe—B alloy or it may be diffused into a consolidated Nd—Fe—B bulk magnet. The LMP alloy may be concentrated at the grain boundaries of the bulk magnet.
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8.
公开(公告)号:US20180236554A1
公开(公告)日:2018-08-23
申请号:US15754647
申请日:2016-08-19
申请人: HITACHI METALS, LTD.
发明人: Futoshi KUNIYOSHI
CPC分类号: B22F3/24 , B22F2999/00 , C22C19/07 , C22C28/00 , C22C33/02 , C22C38/00 , C22C38/005 , C22C38/10 , C22C38/32 , F27D3/12 , H01F1/0536 , H01F1/057 , H01F1/0577 , H01F1/08 , H01F41/02 , H01F41/0293 , C22C2202/02 , B22F2003/248 , B22F3/003
摘要: A diffusion treatment device includes: a treatment container including a cylindrical main body and first and second lids, the cylindrical main body having a treatment space which is capable of receiving sintered magnet pieces and RH diffusion sources, the first and second lids being capable of hermetically sealing first and second openings, respectively, at opposite ends of the cylindrical main body; a conveyor for conveying the treatment container by a predetermined distance in an x-axis direction while a longitudinal direction of the treatment container is located in a y-axis direction in a rectangular coordinate system xyz; a heating unit including a lower heating section provided under the treatment container and an upper heating section provided above the treatment container, and a first rotating unit for rotating the treatment container around a y-axis while the longitudinal direction of the treatment container is located in the y-axis direction.
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公开(公告)号:US20180226189A1
公开(公告)日:2018-08-09
申请号:US15842039
申请日:2017-12-14
发明人: Shujie Wu , Yi Dong , Shulin Diao , Shuai Zhang , Yi Yuan , Ya Chen , Wenjie Yuan
CPC分类号: H01F41/0266 , C25D3/665 , C25D5/18 , C25D5/50 , C25D7/001 , H01F1/0536 , H01F1/0577 , H01F41/0293
摘要: The disclosure discloses a method for preparing a permanent magnet material. In this method, an ionic liquid electroplating process is used to electroplate a heavy rare earth metal onto a surface of a sintered magnet to form a magnet with a coating, wherein the sintered magnet has a thickness of 10 mm or less in at least one direction; in the ionic liquid electroplating process, an electroplating solution comprises an ionic liquid, a heavy rare earth salt, a group VIII metal salt, an alkali metal salt and an additive, an anode is a heavy rare earth metal or a heavy rare earth alloy, a cathode is the sintered magnet, an electroplating temperature is 20-50° C., an electroplating time is 15-80 min. The preparation method of the disclosure can improve an intrinsic coercive force of the magnet with low cost and high production efficiency. A utilization rate of heavy rare earth is high.
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公开(公告)号:US10017871B2
公开(公告)日:2018-07-10
申请号:US14625277
申请日:2015-02-18
CPC分类号: C25D7/001 , C25D13/02 , C25D13/22 , C25D13/24 , C25D17/00 , C25D17/02 , C25D17/06 , C25D17/12 , C25D21/12 , H01F41/0293
摘要: An electrodepositing apparatus is provided comprising an inner tank (1) filled with an electrodepositing solution, an outer tank (3), a feedback means (4), a rectifying member (5) disposed in the inner tank (1), a means (8) for holding an article (p), a counter electrode (6), and a power supply (9). The electrodepositing solution is circulated in such a way that it overflows the inner tank and is fed back from the outer tank to the inner tank by the feedback means, the flow of the solution is rectified by the rectifying member to keep flat the solution surface in the inner tank, a selected portion of the article is immersed in the solution, and the coating agent is electrodeposited on the selected portion of the article.
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