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    A METHOD FOR PRODUCING CROSS-LINKED RUBBER
    1.
    发明公开
    A METHOD FOR PRODUCING CROSS-LINKED RUBBER 审中-公开

    公开(公告)号：US20240209163A1

    公开(公告)日：2024-06-27

    申请号：US18555864

    申请日：2021-11-16

    Applicant: BRIDGESTONE CORPORATION

    Inventor： Yasuo OHSAWA ,  Norihiko KAGA

    IPC: C08J3/24 ,  B29C35/04 ,  B29C64/147 ,  B29C64/30 ,  B29K7/00 ,  B29K105/24 ,  B29K507/04 ,  B33Y40/20

    CPC classification number: C08J3/247 ,  B29C35/041 ,  B29C64/30 ,  B33Y40/20 ,  C08J3/248 ,  B29C64/147 ,  B29K2007/00 ,  B29K2105/24 ,  B29K2507/04 ,  C08J2307/00

    Abstract: This disclosure provides a method for producing a cross-linked rubber for the additively fabricated object that can be easily produced with good dimensional accuracy and simplicity, even using a general-purpose uncross-linked rubber composition. This producing method is a method for producing a cross-linked rubber, in which an additively fabricated object of uncross-linked rubber is heated in a liquid to produce an additively fabricated object of cross-linked rubber, wherein the method includes, heating the additively fabricated object of uncross-linked rubber within the range not exceeding the saturated vapor pressure by controlling the temperature and pressure of the liquid, obtaining the equivalent cross-linking amounts at regular intervals from the start of heating using the following Formula (1), accumulating them and calculating the cumulative cross-linking degree, and stopping the cross-linking reaction when the cross-linking degree of the additively fabricated object of cross-linked rubber reaches the required cross-linking degree.







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    MEASUREMENT OF CURING
    6.
    发明申请
    MEASUREMENT OF CURING 审中-公开
    测量固化

    公开(公告)号：US20110183422A1

    公开(公告)日：2011-07-28

    申请号：US13003219

    申请日：2009-06-29

    Applicant: Leif Cronvall ,  Jonas Lundberg

    Inventor： Leif Cronvall ,  Jonas Lundberg

    IPC: G01N33/44

    CPC classification number: B29C35/0288 ,  C08J3/248 ,  G01N29/024 ,  G01N2291/0251

    Abstract: A method for increasing productivity and quality in production of cured polymer by a real time measurement of the progress of curing, in a mould cavity, which being filled with a compound to be cured, wherein a signal is generated by a wave at an ultrasonic or equivalent frequency, which is transmitted through the mould cavity, the time for the wave to pass through the compound in the mould and back is detected, and the detected signal being analyzed in a suitable data processing computer , to establish a graph showing a relationship between the time for the wave to pass through the compound in the mould and back, and the time of the curing of the compound. The graph is used to determine a feature of the compound by identifying at least one specific parameter of the graph, and using said parameter to control the production.

    Abstract translation: 一种在固化聚合物的生产中提高生产率和质量的方法，其中通过在待固化的化合物填充的模腔中实时测量固化过程，其中通过超声波产生信号，或 通过模腔传输的等效频率被检测到波通过模具和背面中的化合物的时间，并且检测到的信号在合适的数据处理计算机中进行分析，以建立一个图示出 波浪通过模具中的化合物和反射的时间以及化合物的固化时间。 该图用于通过识别图的至少一个特定参数并使用所述参数来控制生产来确定化合物的特征。

    Apparatus and method for measuring cured state of reaction curable resin
    8.
    发明申请
    Apparatus and method for measuring cured state of reaction curable resin 失效
    用于测量反应固化树脂的固化状态的装置和方法

    公开(公告)号：US20050143483A1

    公开(公告)日：2005-06-30

    申请号：US11013536

    申请日：2004-12-17

    Applicant: Tatsushi Sanuki ,  Naoko Miura

    Inventor： Tatsushi Sanuki ,  Naoko Miura

    IPC: C08G2/00 ,  C08G59/18 ,  C08J3/24 ,  C08J3/28 ,  G01N21/27 ,  G01N21/33

    CPC classification number: C08G59/18 ,  C08J3/248 ,  C08J3/28 ,  G01N21/272 ,  G01N21/33

    Abstract: Ultraviolet light having wavelengths of 250 to 380 nm is irradiated to a reaction curable resin. A screen image of luminance value is recorded which is obtained by extracting only a specific wavelength component of the reflected ultraviolet light, and the cured state of an ultraviolet curable resin is quantified from a captured image and displayed. At the same time, the spectral characteristic of reflected light is measured by an ultraviolet spectroscope and a cured state is quantified in accordance with the change rate of absorbances obtained from a change of spectral characteristics by combining the spectral characteristic with a luminance value image and displayed. Thereby, decrease in defects due to irregular curing and uncured portion of the ultraviolet curable resin can be realized by measuring the temporal change of the cured state of the reaction curable resin as a screen image and optimizing an optimum curing condition of the ultraviolet curable resin.

    Abstract translation: 对反应固化性树脂照射波长为250〜380nm的紫外线。 记录通过仅提取反射紫外线的特定波长成分而获得的亮度值的屏幕图像，并且从拍摄图像中量化紫外线固化树脂的固化状态并进行显示。 同时，通过紫外分光光度计测定反射光的光谱特性，根据通过将光谱特性与亮度值图像组合而得到的光谱特性变化得到的吸光度的变化率来量化固化状态，并显示出 。 由此，可以通过测定作为屏幕图像的反应固化性树脂的固化状态的时间变化，并且优化紫外线硬化树脂的最佳固化条件，来实现紫外线固化树脂的不规则固化和未固化部分的缺陷的减少。

    Method for determining cure in a polycarboxylic acid bindered material
    9.
    发明申请
    Method for determining cure in a polycarboxylic acid bindered material 有权
    确定多羧酸结合材料固化的方法

    公开(公告)号：US20030224527A1

    公开(公告)日：2003-12-04

    申请号：US10160775

    申请日：2002-05-31

    Inventor： Liang Chen

    IPC: G01N021/72

    CPC classification number: C08J3/248 ,  G01N31/22 ,  Y10T436/201666

    Abstract: By utilizing a pH indicator having known color change characteristics, an accurate determination of the pH of a binder surface, and hence the amount of cure of a polycarboxylic acid based binder on the fiberglass fibers, can be easily determined for polycarboxylic binder based fiberglass materials used in insulation and composite applications. Based on these results, the manufacturing line used to make these bindered materials may be adjusted to ensure adequate curing at maximum efficiency while minimizing operating costs and reducing waste.

    Abstract translation: 通过使用具有已知颜色变化特性的pH指示剂，可以容易地确定粘合剂表面的pH的精确测定以及因此在玻璃纤维纤维上聚羧酸基粘合剂的固化量，所使用的聚羧酸粘合剂基玻璃纤维材料 在绝缘和复合应用中。 基于这些结果，可以调节用于制造这些结合材料的生产线，以确保以最大效率充分固化，同时最小化操作成本并减少浪费。

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