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14 条记录 (耗时 0.012 秒)

    Method for the production of sulphamic acid halogenides
    1.
    发明授权
    Method for the production of sulphamic acid halogenides 有权
    制备氨基磺酸卤化物的方法

    公开(公告)号：US07232926B2

    公开(公告)日：2007-06-19

    申请号：US10513668

    申请日：2003-05-15

    申请人： Gerhard Hamprecht ,  Michael Puhl ,  Robert Reinhard ,  Ingo Sagasser ,  Thomas Schmidt ,  Norbert Götz ,  Thomas Zierke

    发明人： Gerhard Hamprecht ,  Michael Puhl ,  Robert Reinhard ,  Ingo Sagasser ,  Thomas Schmidt ,  Norbert Götz ,  Thomas Zierke

    IPC分类号： C07C19/00 ,  C07D239/02

    CPC分类号： C07D295/26 ,  C07C303/34 ,  C07C307/00 ,  C07C2601/14 ,  C07D207/48 ,  C07D211/96 ,  C07D239/46

    摘要： The present invention relates to a process for preparing sulfamoyl halides of primary or secondary amines, comprising the following steps: i) reacting a primary or secondary amine A1 with at least equimolar amounts of SO3 or an SO3 source in the presence of at least equimolar amounts of a tertiary amine A2, based in each case on the amine A1, and ii) reacting the reaction mixture obtained in step i) with at least the amount of a phosphorus halide required by the stoichiometry; The invention further relates to a process for preparing sulfonic diamides, comprising the preparation of sulfamoyl halides by means of carrying out steps i) and ii) and subsequently reacting the sulfamoyl halide obtained with ammonia. The invention further relates to the use of this process for preparing active herbicidal ingredients having a sulfuric diamide structure. The invention further relates to novel sulfamoyl chlorides.

    摘要翻译： 本发明涉及一种制备伯胺或仲胺的氨磺酰卤的方法，包括以下步骤：i）使伯胺或仲胺A1与至少等摩尔量的SO 3或SO 3反应， 在至少等摩尔量的叔胺A2的存在下，基于胺A1，基于每种情况，并且ii）使步骤i）中获得的反应混合物与至少一定量的 化学计量所需的卤化磷; 本发明还涉及制备磺酰二酰胺的方法，其包括通过进行步骤i）和ii）制备氨磺酰卤，随后使所得氨磺酰卤与氨反应。 本发明还涉及该方法用于制备具有硫酸二酰胺结构的活性除草成分的用途。 本发明还涉及新的氨磺酰氯。

    Ionic conducting material having good anticorrosive properties
    3.
    发明申请
    Ionic conducting material having good anticorrosive properties 失效
    离子导电材料具有良好的防腐蚀性能

    公开(公告)号：US20010025943A1

    公开(公告)日：2001-10-04

    申请号：US09837274

    申请日：2001-04-19

    申请人： CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIC

    发明人： Christophe Michot ,  Michel Armand ,  Jean-Yves Sanchez ,  Yves Choquette ,  Michel Gauthier

    IPC分类号： H01M006/16 ,  H01M006/18

    CPC分类号： H01G9/038 ,  C01B21/0935 ,  C07C307/00 ,  H01B1/122 ,  H01G11/20 ,  H01G11/56 ,  H01M6/181 ,  H01M10/052 ,  H01M10/0525 ,  H01M10/0565 ,  H01M10/0567 ,  H01M10/0568 ,  H01M10/0569 ,  Y02E60/13

    摘要： The invention relates to an tonically conductive material, to its preparation and to its uses. The material includes at least one ionic compound in solution in an aprotic solvent, chosen from the compounds (1/mM)nullnull(ZY)2Nnullnull, (1/mM)nullnull(ZY)3Cnullnull and (1/mM)nullnull(ZY)2CQnullnull, in which Y denotes SO2 or POZ, Q denotes nullH, nullCOZ or Z, each substituent Z independently denotes a fluorine atom or an optionally perfluorinated organic group which optionally contains at least one polymerizable functional group, at least one of the substituents Z denoting a fluorine atom, and M denotes a cation. Application to electrochemical generators, supercapacities, to the doping of polymers and to electrochromic devices.

    摘要翻译： 本发明涉及一种导电材料，其制备及其用途。 选自化合物（1 / mM）+ [（ZY）2 N] - ，（1 / mM）+ [（ZY）3 C] - 和（1））的非质子溶剂中的至少一种离子化合物 mM）+ [（ZY）2CQ] - ，其中Y表示SO2或POZ，Q表示-H，-COZ或Z，各取代基Z独立地表示氟原子或任选含有至少一个可聚合的 官能团，至少一个取代基Z表示氟原子，M表示阳离子。 应用于电化学发生器，超电容，掺杂聚合物和电致变色器件。

    Post-treated sulfurized salt of an alkyl-substituted hydroxyaromatic composition
    5.
    发明授权
    Post-treated sulfurized salt of an alkyl-substituted hydroxyaromatic composition 有权
    经后处理的烷基取代的羟基芳族组合物的硫化盐

    公开(公告)号：US09249091B2

    公开(公告)日：2016-02-02

    申请号：US13727892

    申请日：2012-12-27

    申请人： Andrew R. Gibbs ,  Curtis Campbell

    发明人： Andrew R. Gibbs ,  Curtis Campbell

    IPC分类号： C07C307/00 ,  C10M159/16 ,  C07G99/00

    CPC分类号： C07C307/00 ,  C07G17/00 ,  C10M159/16 ,  C10M2217/043 ,  C10N2230/64 ,  C10N2240/04 ,  C10N2240/08 ,  C10N2240/10 ,  C10N2240/102 ,  C10N2240/30 ,  C10N2250/10 ,  C10N2260/10 ,  C10N2210/02

    摘要： Disclosed herein is a post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition which is a reaction product of (a) a salt of a sulfurized alkyl-substituted hydroxyaromatic composition, wherein the alkyl-substituted hydroxyaromatic compound is derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof, (b) a source of an aldehyde and (c) a primary and/or secondary monoamine compound having at least one active hydrogen. The post-treated salt of a sulfurized alkylhydroxyaromatic composition disclosed herein has a reduced content of unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt as compared to the content, by combined mass, of the unsulfurized alkyl-substituted hydroxyaromatic compound and its unsulfurized metal salt present in the non-post-treated salt of a sulfurized alkyl-substituted hydroxyaromatic composition.

    摘要翻译： 本文公开了硫化烷基取代的羟基芳族组合物的后处理盐，其是（a）硫化烷基取代的羟基芳族组合物的盐的反应产物，其中烷基取代的羟基芳族化合物衍生自羟基芳族化合物的烷基化 包含选自丙烯，丁烯或其混合物的单体的C 9至C 18低聚物的一种或多种烯烃的化合物，（b）醛源和（c）具有至少一个活性氢的伯和/或仲单胺化合物。 本文公开的硫化烷基羟基芳族化合物的后处理盐与未硫化的烷基取代的羟基芳族化合物及其未硫化金属的组合质量相比，未硫化的烷基取代的羟基芳族化合物及其未硫化金属盐的含量降低 存在于硫化烷基取代的羟基芳族组合物的非后处理盐中的盐。

    LITHIUM SALTS OF PENTAFLUOROPHENYLAMIDE ANIONS, PREPARATION THEREOF AND USE THEREOF
    6.
    发明申请
    LITHIUM SALTS OF PENTAFLUOROPHENYLAMIDE ANIONS, PREPARATION THEREOF AND USE THEREOF 审中-公开
    二芳基酰胺阴离子的锂盐，其制备及其用途

    公开(公告)号：US20120245387A1

    公开(公告)日：2012-09-27

    申请号：US13502894

    申请日：2010-10-20

    申请人： Jorg Sundermeyer ,  Thomas Linder ,  Bernhard Roling ,  Benedikt Huber ,  Till Fromling

    发明人： Jorg Sundermeyer ,  Thomas Linder ,  Bernhard Roling ,  Benedikt Huber ,  Till Fromling

    IPC分类号： C07C311/13 ,  C07C303/40

    CPC分类号： C07C307/00 ,  C07C311/09 ,  H01M10/0525 ,  H01M10/0568

    摘要： The present invention provides new lithium salts comprising pentafluorophenylamide anions following the general formula Li+[N(SO2—R)(C6F5)]−, which are optionally present as solvent-free complexes. R is hereby selected from fluorine, linear or branched acyclic or cyclic alkyl groups with 1 to 20 carbon atoms which are not fluorinated, partially fluorinated or fully fluorinated; or not fluorinated, partially fluorinated or fully fluorinated aryl or benzyl groups with 1 to 20 carbon atoms. The lithium salts according to the present invention are produced by reacting the corresponding NH acid of the pentafluorophenylamide with one equivalent of lithium bis(trimethylsilyl)amide or lithium organyl, wherein the reaction is carried out advantageously in the presence of apolar aprotic solvents. In this way, lithium salts in the form of solvent-free complexes are obtained. These solvent-free lithium complexes are thermally, electrochemically and against oxidation stable and comprise a high ionic conductivity. The lithium salts according to the present invention are suitable to be used as ion-conducting materials, electrically conductive materials, dyes and in chemical catalysis. They are preferably used as ion-conducting electrolytes in lithium ion accumulators.

    摘要翻译： 本发明提供新的锂盐，其包含以通式Li + [N（SO 2 -R）（C 6 F 5）] - 的五氟苯基酰胺阴离子，它们任选作为无溶剂络合物存在。 R选自具有1至20个碳原子的氟，直链或支链无环或环状烷基，其不是氟化的，部分氟化的或完全氟化的; 或不含氟化，部分氟化或完全氟化的具有1至20个碳原子的芳基或苄基。 根据本发明的锂盐通过使五氟苯基酰胺的相应NH酸与一当量的双（三甲基甲硅烷基）氨基锂或有机锂的锂反应制备，其中该反应有利地在非极性非质子溶剂的存在下进行。 以这种方式获得无溶剂络合物形式的锂盐。 这些无溶剂的锂络合物是热的，电化学的和抗氧化稳定的并且包含高离子电导率。 根据本发明的锂盐适合用作离子导电材料，导电材料，染料和化学催化剂。 它们优选用作锂离子蓄电池中的离子传导电解质。

    Method for producing chlorosulfonyl isocyanate
    7.
    发明授权
    Method for producing chlorosulfonyl isocyanate 有权
    氯磺酰基异氰酸酯的制备方法

    公开(公告)号：US07468174B2

    公开(公告)日：2008-12-23

    申请号：US10583194

    申请日：2004-12-15

    申请人： Mutsumi Sugawara ,  Tsutomu Imagawa ,  Fumitaka Masui

    发明人： Mutsumi Sugawara ,  Tsutomu Imagawa ,  Fumitaka Masui

    IPC分类号： C01B21/084 ,  C01B21/086

    CPC分类号： C01C3/145 ,  C07C303/34 ,  C07C307/00

    摘要： A method for producing chlorosulfonyl isocyanate by reaction of sulfur trioxide with cyanogen chloride, wherein chlorosulfonyl isocyanate or a solution including chlorosulfonyl isocyanate is used as a reaction solvent, sulfur trioxide and cyanogen chloride which are respectively diluted with the chlorosulfonyl isocyanate or the solution including chlorosulfonyl isocyanate are added at the same time to a reaction system in an almost equimolar amount under reflux. By the production method of present invention, chlorosulfonyl isocyanate can be produced from sulfur trioxide and cyanogen chloride in which the yield of the chlorosulfonyl isocyanate is high, the method has excellent operability, number of equipments is reduced, and time for controlling the temperature is saved.

    摘要翻译： 使用三氧化硫与氯化氰反应制备氯代磺酰基异氰酸酯的方法，其中使用氯磺酰基异氰酸酯或包含氯代磺酰基异氰酸酯的溶液作为反应溶剂，分别用氯磺酰基异氰酸酯或包括氯磺酰基异氰酸酯的溶液稀释的三氧化硫和氯化氰 同时加入反应体系中几乎等摩尔量的回流。 通过本发明的制造方法，氯代磺酰基异氰酸酯可以由三氧化硫和氯代磺酰基异氰酸酯的产率高的氯化氰制备，该方法具有优异的可操作性，减少了设备数量，节省了控制温度的时间 。