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    SULFONE COMPOUND AND METHOD FOR PRODUCING THE SAME
    1.
    发明申请
    SULFONE COMPOUND AND METHOD FOR PRODUCING THE SAME 审中-公开
    磺化合物及其制造方法

    公开(公告)号：US20110015442A1

    公开(公告)日：2011-01-20

    申请号：US12933014

    申请日：2009-03-16

    申请人： Toshiya Takahashi ,  Tetsuya Shintaku ,  Orhan Ozturk ,  Yohei Fujii

    发明人： Toshiya Takahashi ,  Tetsuya Shintaku ,  Orhan Ozturk ,  Yohei Fujii

    IPC分类号： C07C315/04

    CPC分类号： C07C403/22 ,  C07C315/04 ,  C07C317/24 ,  C07C2601/16

    摘要： The present invention relates to a process for producing a sulfone compound represented by formula (1), which comprising a step of obtaining a compound represented by formula (4) by reacting a compound represented by formula (3) with a chlorate or a bromate, and then resulting reaction solution with HX or X2; a step of obtaining a compound represented by formula (5) or formula (6) by reacting a compound represented by formula (4) with a halogenating agent or M(OCOR)n; or a step of obtaining a compound represented by formula (7) by reacting a compound represented by formula (5) or formula (6) with an inorganic base.

    摘要翻译： 本发明涉及一种由式（1）表示的砜化合物的制备方法，其包括通过使由式（3）表示的化合物与氯酸盐或溴酸盐反应获得式（4）表示的化合物的步骤， 然后用HX或X2得到反应溶液; 通过使式（4）表示的化合物与卤化剂或M（OCOR）n反应，得到式（5）或式（6）所示的化合物的步骤; 或者通过使式（5）或式（6）表示的化合物与无机碱反应来获得由式（7）表示的化合物的步骤。

    SULFONE COMPOUND AND PROCESS FOR PRODUCING CAROTENOID USING THE SAME COMPOUND
    2.
    发明申请
    SULFONE COMPOUND AND PROCESS FOR PRODUCING CAROTENOID USING THE SAME COMPOUND 审中-公开
    SULFONE化合物和使用该化合物生产卡波溶液的方法

    公开(公告)号：US20110015441A1

    公开(公告)日：2011-01-20

    申请号：US12920953

    申请日：2009-03-03

    申请人： Toshiya Takahashi ,  Orhan Ozturk

    发明人： Toshiya Takahashi ,  Orhan Ozturk

    IPC分类号： C07C315/04 ,  C07C317/24 ,  C07C317/10 ,  C07C45/72 ,  C07C5/367

    CPC分类号： C07C403/24 ,  B01J31/0212 ,  B01J31/0239 ,  C07C403/22 ,  C07C2601/16

    摘要： The present invention relates to a process for producing a sulfone compound of the following formula (3), characterized in that an allyl sulfone compound of the formula (1) and an allyl halide compound of the formula (2) are reacted in an organic solvent in the presence of an alkali metal hydroxide and a phase-transfer catalyst: wherein A is CH2 or C═O; Ar is an aryl group optionally having 1 to 3 substitutents; and the wavy line means that the steric relation to the double bond which the wavy line is bound to is of E-form, Z-form or a mixture of E/Z; wherein X is a halogen atom; and the wavy line means the same as defined above; and wherein A, Ar and the wavy line mean the same as defined above. The present invention also relates to a process for producing a carotenoid from the same sulfone compound.

    摘要翻译： 本发明涉及下述式（3）的砜化合物的制造方法，其特征在于，将式（1）的烯丙基砜化合物和式（2）的烯丙基卤化合物在有机溶剂 在碱金属氢氧化物和相转移催化剂存在下，其中A是CH 2或C = O; Ar是任选具有1至3个取代基的芳基; 波浪线意味着与波浪线所绑定的双键的立体关系为E型，Z型或E / Z的混合物; 其中X是卤素原子; 波浪线与上述相同; 并且其中A，Ar和波浪线表示与上述相同的含义。 本发明还涉及由相同的砜化合物生产类胡萝卜素的方法。

    Rubber composition
    3.
    发明授权
    Rubber composition 有权
    橡胶组成

    公开(公告)号：US09068055B2

    公开(公告)日：2015-06-30

    申请号：US14110043

    申请日：2012-04-24

    申请人： Yosuke Watanabe ,  Orhan Ozturk ,  Yasuo Uekita

    发明人： Yosuke Watanabe ,  Orhan Ozturk ,  Yasuo Uekita

    IPC分类号： C08K5/20 ,  B60C1/00 ,  C08K5/17 ,  C08L21/00

    CPC分类号： C07C235/68 ,  B29B7/7495 ,  B60C1/00 ,  B60C1/0008 ,  B60C1/0016 ,  B60C1/0025 ,  B60C1/0041 ,  C08K3/013 ,  C08K5/17 ,  C08K5/20 ,  Y10T152/10495 ,  Y10T152/1081 ,  C08L21/00 ,  C08K3/0033

    摘要： A rubber composition obtained by kneading at least one selected from the group consisting of (A1), (B1), (C1) and (D1), a rubber component and a filler, and a method of improving the viscoelastic property of vulcanized rubber, comprising a first step of kneading at least one selected from the group consisting of (A1), (B1), (C1) and (D1), a rubber component, a filler and a sulfur component and a second step of thermally treating the kneaded material obtained in the previous step. (A1): a compound represented by formula (I) (B1): a salt of a compound represented by formula (I) (C1): a solvate of a compound represented by formula (I) (D1): a solvate of a salt of a compound represented by formula (I).

    摘要翻译： 通过捏合从（A1），（B1），（C1）和（D1）组成的组中选择的至少一种橡胶组分和填料获得的橡胶组合物和改进硫化橡胶的粘弹性的方法， 包括：捏合从（A1），（B1），（C1）和（D1）组成的组中选出的至少一种的橡胶组分，填料和硫组分的第一步骤，以及第二步， 在上一步中获得的材料。 （A1）：由式（I）表示的化合物（B1）：由式（I）表示的化合物的盐（C1）：由式（I）（D1）表示的化合物的溶剂合物： 由式（I）表示的化合物的盐。

    Process for producing aminoalkylthiosulfuric acid compound
    5.
    发明授权
    Process for producing aminoalkylthiosulfuric acid compound 有权
    氨基烷基硫代硫酸化合物的制备方法

    公开(公告)号：US08772537B2

    公开(公告)日：2014-07-08

    申请号：US13808945

    申请日：2011-07-22

    申请人： Orhan Ozturk

    发明人： Orhan Ozturk

    IPC分类号： C07C309/00

    CPC分类号： C07C381/04 ,  C07C381/02

    摘要： An aminoalkylthiosulfuric acid compound represented by formula (1): is produced. In step (A1), a hydrochloride of a chloroalkylamine compound represented by formula (2): is reacted with an alkali metal salt of thiosulfuric acid in the presence of 2 to 6 parts by weight of water with respect to 1 part by weight of the hydrochloride between 50° C. and 100° C. R1 and R2 each represents a hydrogen atom and the like, and n represents an integer of 2 to 9. In step (B1), a mixture of a solid containing the aminoalkylthiosulfuric acid compound and a liquid containing an alkali metal chloride is obtained by adjusting the temperature of the mixture of step (A1) to between −15° C. and 50° C. In step (C1), the aminoalkylthiosulfuric acid compound is obtained as solid by separating the solid containing the aminoalkylthiosulfuric acid compound and the liquid containing the alkali metal chloride from the mixture of (B1).

    摘要翻译： 制备由式（1）表示的氨基烷基硫代硫酸化合物。 在步骤（A1）中，将式（2）表示的氯代烷基胺化合物的盐酸盐与硫代硫酸的碱金属盐在2至6重量份水的存在下相对于1重量份的 盐酸盐在50℃至100℃之间.R 1和R 2各自表示氢原子等，n表示2至9的整数。在步骤（B1）中，将含有氨基烷基硫代酸化合物的固体和 通过将步骤（A1）的混合物的温度调节至-15℃和50℃之间来获得含有碱金属氯化物的液体。在步骤（C1）中，通过将步骤（A1）的混合物的温度分离，得到氨基烷基硫代硫酸化合物 从（B1）的混合物中含有氨基烷基硫代酸化合物和含有碱金属氯化物的液体的固体。

    RUBBER COMPOSITION
    6.
    发明申请
    RUBBER COMPOSITION 有权
    橡胶组合物

    公开(公告)号：US20140020808A1

    公开(公告)日：2014-01-23

    申请号：US14110043

    申请日：2012-04-24

    申请人： Yosuke Watanabe ,  Orhan Ozturk ,  Yasuo Uekita

    发明人： Yosuke Watanabe ,  Orhan Ozturk ,  Yasuo Uekita

    IPC分类号： C08K5/20 ,  B60C1/00

    CPC分类号： C07C235/68 ,  B29B7/7495 ,  B60C1/00 ,  B60C1/0008 ,  B60C1/0016 ,  B60C1/0025 ,  B60C1/0041 ,  C08K3/013 ,  C08K5/17 ,  C08K5/20 ,  Y10T152/10495 ,  Y10T152/1081 ,  C08L21/00 ,  C08K3/0033

    摘要： A rubber composition obtained by kneading at least one selected from the group consisting of (A1), (B1), (C1) and (D1), a rubber component and a filler, and a method of improving the viscoelastic property of vulcanized rubber, comprising a first step of kneading at least one selected from the group consisting of (A1), (B1), (C1) and (D1), a rubber component, a filler and a sulfur component and a second step of thermally treating the kneaded material obtained in the previous step. (A1): a compound represented by formula (I) (B1): a salt of a compound represented by formula (I) (C1): a solvate of a compound represented by formula (I) (D1): a solvate of a salt of a compound represented by formula (I)

    摘要翻译： 通过捏合从（A1），（B1），（C1）和（D1）组成的组中选择的至少一种橡胶组分和填料获得的橡胶组合物和改进硫化橡胶的粘弹性的方法， 包括：捏合从（A1），（B1），（C1）和（D1）组成的组中选出的至少一种的橡胶组分，填料和硫组分的第一步骤，以及第二步， 在上一步中获得的材料。 （A1）：由式（I）表示的化合物（B1）：由式（I）表示的化合物的盐（C1）：由式（I）（D1）表示的化合物的溶剂合物： 由式（I）表示的化合物的盐

    PROCESS FOR PRODUCING AMINOALKYLTHIOSULFURIC ACID COMPOUND
    9.
    发明申请
    PROCESS FOR PRODUCING AMINOALKYLTHIOSULFURIC ACID COMPOUND 有权
    生产氨基二硫代磷酸酯化合物的方法

    公开(公告)号：US20130116468A1

    公开(公告)日：2013-05-09

    申请号：US13808945

    申请日：2011-07-22

    申请人： Orhan Ozturk

    发明人： Orhan Ozturk

    IPC分类号： C07C381/04

    CPC分类号： C07C381/04 ,  C07C381/02

    摘要： An aminoalkylthiosulfuric acid compound represented by formula (1): is produced. In step (A1), a hydrochloride of a chloroalkylamine compound represented by formula (2): is reacted with an alkali metal salt of thiosulfuric acid in the presence of 2 to 6 parts by weight of water with respect to 1 part by weight of the hydrochloride between 50° C. and 100° C. R1 and R2 each represents a hydrogen atom and the like, and n represents an integer of 2 to 9. In step (B1), a mixture of a solid containing the aminoalkylthiosulfuric acid compound and a liquid containing an alkali metal chloride is obtained by adjusting the temperature of the mixture of step (A1) to between −15° C. and 50° C. In step (C1), the aminoalkylthiosulfuric acid compound is obtained as solid by separating the solid containing the aminoalkylthiosulfuric acid compound and the liquid containing the alkali metal chloride from the mixture of (B1).

    摘要翻译： 制备由式（1）表示的氨基烷基硫代硫酸化合物。 在步骤（A1）中，将式（2）表示的氯代烷基胺化合物的盐酸盐与硫代硫酸的碱金属盐在2至6重量份水的存在下相对于1重量份的 盐酸盐在50℃至100℃之间.R 1和R 2各自表示氢原子等，n表示2至9的整数。在步骤（B1）中，将含有氨基烷基硫代酸化合物的固体和 通过将步骤（A1）的混合物的温度调节至-15℃和50℃之间来获得含有碱金属氯化物的液体。在步骤（C1）中，通过将步骤（A1）的混合物的温度分离，得到氨基烷基硫代硫酸化合物 从（B1）的混合物中含有氨基烷基硫代酸化合物和含有碱金属氯化物的液体的固体。