摘要:
The invention relates to a method and reagent mixture for the staining and thus visualization of amino acids, peptides and similar compounds, in particular after separation by means of thin-layer chromatography. The staining is carried out using ninhydrin for the detection of amino acids, peptides or proteins in combination with at least one ionic liquid.
摘要:
The invention relates to a method and reagent mixture for the staining and thus visualisation of amino acids, peptides and similar compounds, in particular after separation by means of thin-layer chromatography. The staining is carried out using NIN-HYDRIN for the detection of amino acids, peptides or proteins in combination with at least one ionic liquid.
摘要:
The present invention is directed to a process for producing inorganic particulate material, the material obtainable by such process, a modified release delivery system comprising the material and the use of the material for the administration of a bioactive agent.
摘要:
A process for preparing N,N-dimethylacetamide (DMAC) by continuously reacting methyl acetate (MeOAc) with dimethylamine (DMA) in the presence of a basic catalyst, wherein MeOAc is used in the form of a methanolic solution and the continuous distillative workup is effected in such a way that methanol and any other low boilers are initially removed overhead in a column A and the bottom effluent of column A is fed to a column B in which DMAC is removed via a side draw a purity of ≧99.7% by weight.
摘要:
A measuring device for contactless detection of a ferromagnetic object, comprising at least one magnet; a magnetic field-sensitive element arranged so that an air gap is provided between the magnetic field-sensitive element and the ferromagnetic object; and a soft-magnetic component located between magnet and the magnetic field-sensitive element on a face of the magnet which points in a direction of the ferromagnetic object to be detected, said soft-magnetic component being formed as a cap-shaped element that has a recess that is open in a direction away from said magnetic field-sensitive element to house the magnet and an opening that is open in a direction of the magnetic field-sensitive element, to house the magnet and opening that is open in a direction of the magnetic field-sensitive element, the soft-magnetic component having a first side wall defining said recess and also having a portion which forms a second side wall defining said opening, said first side wall and said second side wall being in alignment with one another.
摘要:
Ruthenium complexes of the formula I or IV RuX2(═CH—CH2R)L1L2 (I) RuXY(═CH═CH2R)L1L2 (IV) where X, Y are anionic ligands, R is hydrogen or a substituted or unsubstituted C1-C20-alkyl radical or C6-C20-aryl radical and L1 and L2 are, independently of one another, uncharged electron donor ligands, are prepared by (a) reaction of RuX3 with L1 and L2 in an inert solvent in the presence of a reducing agent and hydrogen and (b) reaction with compounds of the formula II R—C≡CH (II) where R is as defined above, in the presence or absence of water, and, if desired after isolation of the intermediate, with HY, [HL1]Y or [HL2]Y.
摘要:
A catalyst containing Re.sub.2 O.sub.7 on an inorganic support, wherein the Re.sub.2 O.sub.7 component is on the support in the form of Re.sub.2 O.sub.7 particles having a diameter of
摘要翻译:在无机载体上含有Re 2 O 7的催化剂,其中Re 2 O 7组分以直径<1nm的Re 2 O 7颗粒的形式在载体上,由N 2 O脉冲化学吸附确定的铼表面积为至少0.4m 2 / g, 并且Re 2 O 7组分以最大厚度为1.5mm的外壳的形式分布在支撑件上。
摘要:
Epoxides are prepared from olefins using bis(triorganosilyl) peroxides in the presence of activators based on metalic acid derivatives of the formula ##STR1## where M is a metal of transition groups IV to VII, in particular molybdenum, tungsten or rheniumL is an uncharged ligand selected from the group consisting of amine oxides, phosphine oxides, arsine oxides, phosphoric triamides, formamides and pyridine N-oxidesX is an inorganic ligandx is from 1 to 5y is 0, 1 or 2,Z is 1 or 2 andn is 1 or 2.
摘要:
Olefins can be epoxidized using catalysts I ##STR1## where M is a metal of the 4th to 7th transition group of the Periodic Table of the Elements,L.sup.1 is an amine oxide, phosphine oxide, arsine oxide, pyridine N-oxide or pyridine ligand of the formula II, III, VII or VIII,L.sup.2 is a customary auxiliary ligand or a further ligand L.sup.1 or a free coordination site,X is oxo oxygen or an imido ligand,m is 1 or 2, andn is 1, 2 or 3.
摘要:
A process for preparing N,N-dimethylacetamide (DMAC) by continuously reacting methyl acetate (MeOAc) with dimethylamine (DMA) in the presence of a basic catalyst, wherein MeOAc is used in the form of a methanolic solution which is obtained as a byproduct in the preparation of polyTHF by transesterifying polyTHF diacetate with methanol.