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    Binary phase transfer/amine catalyst for making aromatic polycarbonates
    1.
    发明授权
    Binary phase transfer/amine catalyst for making aromatic polycarbonates 失效
    用于制备芳族聚碳酸酯的二元相转移/胺催化剂

    公开(公告)号：US5739257A

    公开(公告)日：1998-04-14

    申请号：US734769

    申请日：1996-10-21

    申请人： Eugene P. Boden ,  Larry I. Flowers ,  Peter D. Phelps ,  David L. Ramsey ,  Paul D. Sybert

    发明人： Eugene P. Boden ,  Larry I. Flowers ,  Peter D. Phelps ,  David L. Ramsey ,  Paul D. Sybert

    IPC分类号： C08G64/24 ,  C08G64/00

    CPC分类号： C08G64/24

    摘要： A composition and method is provided for making polycarbonate utilizing an effective amount of a binary catalyst system, comprising a phase transfer catalyst selected from the group consisting of methyltributylammonium halide and hexabutylbutylenediammonium halide and a tertiary organic amine, as a condensation catalyst during the interfacial phosgenation of a bisphenol, such as bisphenol A. Improved phosgene utilization and the substantial elimination of emulsion formation in the interfacial polymerization reactor and the processing units downstream thereof results.

    摘要翻译： 提供了一种组合物和方法，用于使用有效量的二元催化剂体系制备聚碳酸酯，其包括在界面光气化期间作为缩合催化剂的选自甲基三丁基卤化铵和六丁基丁烯二胺的卤化物和叔有机胺的相转移催化剂 双酚A.双酚A.改善的光气利用率和在界面聚合反应器及其下游处理单元中乳液形成的显着消除。

    Flame retardant poly(siloxane-etherimide) copolymer compositions, methods of manufacture, and articles formed therefrom
    7.
    发明授权
    Flame retardant poly(siloxane-etherimide) copolymer compositions, methods of manufacture, and articles formed therefrom 有权
    阻燃聚（硅氧烷 - 醚酰亚胺）共聚物组合物，制造方法和由其形成的制品

    公开(公告)号：US08937127B2

    公开(公告)日：2015-01-20

    申请号：US13251130

    申请日：2011-09-30

    申请人： Paul D. Sybert ,  Thomas L. Evans

    发明人： Paul D. Sybert ,  Thomas L. Evans

    IPC分类号： C08L69/00 ,  C08L79/08 ,  C08G73/10 ,  C09K21/14 ,  C08L83/12 ,  C08G77/455 ,  C08G77/46

    CPC分类号： C08G73/106 ,  C08G73/1042 ,  C08G73/1046 ,  C08G77/455 ,  C08G77/46 ,  C08L69/00 ,  C08L79/08 ,  C08L83/12 ,  C09K21/14 ,  Y10T428/31507 ,  Y10T428/31721 ,  C08L83/10

    摘要： A composition comprising: a first polymer comprising a poly(etherimide-siloxane) copolymer comprising (a) a repeating polyetherimide unit, and (b) a poly(siloxane) block unit, a second polymer different from the first polymer and comprising bromine; and optionally, a third polymer comprising a polycarbonate different from the first polymer and second polymer; wherein polysiloxane block units are present in the composition in an amount of at least 0.3 wt %, and bromine is present in the composition in an amount of at least 7.8 wt %, each based on the sum of the wt % of the first, second, and third polymers; and further wherein an article molded from the composition has an OSU integrated 2 minute heat release test value of less than 65 kW-min/m2 and a peak heat release rate of less than 65 kW/m2, and an E662 smoke test Dmax value of less than 200.

    摘要翻译： 一种组合物，其包含：包含（a）重复聚醚酰亚胺单元的聚（醚酰亚胺 - 硅氧烷）共聚物的第一聚合物和（b）聚（硅氧烷）嵌段单元，不同于第一聚合物并包含溴的第二聚合物; 和任选地，包含不同于第一聚合物和第二聚合物的聚碳酸酯的第三聚合物; 其中聚硅氧烷嵌段单元以至少0.3重量％的量存在于组合物中，并且组合物中溴以至少7.8重量％的量存在，每个量基于第一，第二 和第三聚合物; 并且其中由所述组合物成型的制品具有小于65kW-min / m 2的OSU集成的2分钟的热释放试验值和小于65kW / m 2的峰值放热率，以及E662烟雾试验Dmax值 小于200。

    Weatherable, thermostable polymers having improved flow composition
    9.
    发明授权
    Weatherable, thermostable polymers having improved flow composition 有权
    具有改善流动组成的耐候性耐热聚合物

    公开(公告)号：US07605221B2

    公开(公告)日：2009-10-20

    申请号：US11426680

    申请日：2006-06-27

    申请人： Gary C. Davis ,  Brian D. Mullen ,  Paul D. Sybert

    发明人： Gary C. Davis ,  Brian D. Mullen ,  Paul D. Sybert

    IPC分类号： C08G77/14

    CPC分类号： C08G64/186 ,  C08G63/64 ,  C08G63/6956 ,  C08G77/448 ,  C08L69/00 ,  C08L83/10 ,  C08L2666/02

    摘要： A copolymer composition comprises a polysiloxane block of Formula XIX or XXII, having 4 to 50 siloxane units, and a polyarylate-polycarbonate block consisting essentially of 50 to 99 mol % arylate polyester units and 1 to 50 mol % aromatic carbonate units, wherein 1 to 30 mole percent of the aromatic carbonate units are resorcinol carbonates, and 0 to 35 mol % of the aromatic carbonate units are bisphenol carbonates; wherein the sum of mole percentages of arylate polyester units, and aromatic carbonate units is 100 mol %; the polysiloxane blocks connect to an arylate ester unit, and/or an aromatic carbonate unit; the siloxane units of the polysiloxane block are present at 0.2 to 10 wt % based on weight of the copolymer composition; and a molded article of 3.2±0.12 millimeters thickness and consisting of the copolymer composition has a percent transmittance greater than or equal to 70%, according to ASTM D1003-00.

    摘要翻译： 共聚物组合物包含具有4至50个硅氧烷单元的式XIX或XXII的聚硅氧烷嵌段和基本上由50至99mol％芳基化聚酯单元和1至50mol％芳族碳酸酯单元组成的聚芳酯 - 聚碳酸酯嵌段，其中1至 30摩尔％的芳族碳酸酯单元是间苯二酚碳酸酯，0-35摩尔％的芳族碳酸酯单元是双酚碳酸酯; 其中芳基化聚酯单元和芳族碳酸酯单元的摩尔百分比之和为100摩尔％。 聚硅氧烷嵌段连接到芳基酯单元和/或芳族碳酸酯单元; 聚硅氧烷嵌段的硅氧烷单元以基于共聚物组合物的重量计为0.2-10重量％存在; 并且根据ASTM D1003-00，由共聚物组合物组成的3.2±0.12毫米厚的模制品具有百分比透射率大于或等于70％。

    Transparent compositions, methods for the preparation thereof, and articles derived therefrom
    10.
    发明授权
    Transparent compositions, methods for the preparation thereof, and articles derived therefrom 有权
    透明组合物，其制备方法和由其衍生的制品

    公开(公告)号：US07323535B2

    公开(公告)日：2008-01-29

    申请号：US11263515

    申请日：2005-10-31

    申请人： Gordon A. Berkstresser, IV ,  Brian D. Mullen ,  Paul D. Sybert

    发明人： Gordon A. Berkstresser, IV ,  Brian D. Mullen ,  Paul D. Sybert

    IPC分类号： C08G63/02

    CPC分类号： C08L69/005 ,  C08G63/19 ,  C08G63/64 ,  C08G63/82 ,  C08L69/00 ,  C08L2666/18

    摘要： A reaction product comprises a polyester-polycarbonate comprising a polyester unit and a polycarbonate unit, a polycarbonate polymer, and a transesterification catalyst, wherein the polyester-polycarbonate comprises greater than or equal to 75 mole % aromatic ester units, and less than 25 mole % carbonate units. The reaction product has a haze of less than 1.7%, specifically less than 1.0% as measured at a thickness of 3.2 mm according to ASTM D1003-00. A thermoplastic composition comprising the reaction product and articles formed from therefrom are disclosed. A method of forming the reaction product is also disclosed.

    摘要翻译： 反应产物包括聚酯 - 聚碳酸酯，其包含聚酯单元和聚碳酸酯单元，聚碳酸酯聚合物和酯交换催化剂，其中聚酯 - 聚碳酸酯包含大于或等于75摩尔％的芳族酯单元和小于25摩尔％ 碳酸盐单位。 根据ASTM D1003-00，反射产物的雾度小于1.7％，特别是小于1.0％，其厚度为3.2mm。 公开了一种包含反应产物和由其形成的制品的热塑性组合物。 还公开了形成反应产物的方法。