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22 条记录 (耗时 0.026 秒)

    Process For Production Of 2-Chloro-3,3,3-Trifluoropropene
    1.
    发明申请
    Process For Production Of 2-Chloro-3,3,3-Trifluoropropene 失效
    2-氯-3,3,3-三氟丙烯的制备方法

    公开(公告)号：US20120123173A1

    公开(公告)日：2012-05-17

    申请号：US13383708

    申请日：2010-07-16

    申请人： Yasuo Hibino ,  Fumihiro Kawagoe ,  Fuyuhiko Sakyu

    发明人： Yasuo Hibino ,  Fumihiro Kawagoe ,  Fuyuhiko Sakyu

    IPC分类号： C07C19/08

    CPC分类号： C07C17/23 ,  B01J21/18 ,  B01J23/44 ,  B01J23/628 ,  B01J23/6447 ,  C07C21/18

    摘要： There is provided according the present invention a process for producing 2-chloro-3,3,3-trifluoropropene, comprising: hydrogenating 1,2-dichloro-3,3,3-trifluoropropene with hydrogen (H2) in the presence of a catalyst having a transition metal and a poisoning substance supported on a support. The present production process is industrially advantageous as the target 2-chloro-3,3,3-trifluoropropene can be obtained with high selectivity and high yield under moderate reaction conditions and with easy waste treatment.

    摘要翻译： 根据本发明提供了一种2-氯-3,3,3-三氟丙烯的制备方法，包括：在催化剂存在下用氢气（H 2）氢化1,2-二氯-3,3,3-三氟丙烯 具有负载在载体上的过渡金属和中毒物质。 本发明的制备方法在工业上是有利的，因为在中等反应条件下容易的废物处理可以以高选择性和高收率获得目标2-氯-3,3,3-三氟丙烯。

    Method for producing 1,1,1,3,3-pentafluoropropane
    6.
    发明授权
    Method for producing 1,1,1,3,3-pentafluoropropane 失效

    公开(公告)号：US06316681B1

    公开(公告)日：2001-11-13

    申请号：US08982803

    申请日：1996-12-04

    申请人： Satoshi Yoshikawa ,  Ryouichi Tamai ,  Fuyuhiko Sakyu ,  Yasuo Hibino ,  Yoshihiko Gotoh

    发明人： Satoshi Yoshikawa ,  Ryouichi Tamai ,  Fuyuhiko Sakyu ,  Yasuo Hibino ,  Yoshihiko Gotoh

    IPC分类号： C07C1708

    CPC分类号： C07C19/08 ,  B01J27/125 ,  C07C17/00 ,  C07C17/21 ,  C07C21/18

    摘要： The present invention relates to a method for producing 1,1,1,3,3-pentafluoropropane. This method includes a first step of fluorinating 1-chloro-3,3,3-trifluoropropene in a liquid phase by hydrogen fluoride in the presence of an antimony compound as a catalyst, or a second step of fluorinating 1-chloro-3,3,3-trifluoropropene in a gas phase by hydrogen fluoride in the presence of a fluorination catalyst. If the first step is taken, 1,1,1,3,3-pentafluoropropane can be produced with a high yield. If the second step is taken, 1,1,1,3,3-pentafluoropropane can continuously be easily produced. Therefore, the second step is useful for an industrial scale production thereof. According to the invention, 1-chloro-3,3,3-trifluoropropene may be produced by a method including a step of reacting 1,1,1,3,3-pentachloropropane with hydrogen fluoride in a gas phase in the presence of a fluorination catalyst. This method is useful, because yield of 1-chloro-3,3,3-trifluoropropene is high.

    Process for producing 1,3,3,3-tetrafluoropropene
    7.
    发明授权
    Process for producing 1,3,3,3-tetrafluoropropene 有权
    制备1,3,3,3-四氟丙烯的方法

    公开(公告)号：US09051231B2

    公开(公告)日：2015-06-09

    申请号：US13119658

    申请日：2009-09-24

    申请人： Fuyuhiko Sakyu ,  Satoshi Yoshikawa ,  Satoru Okamoto ,  Yasuo Hibino ,  Yoshio Nishiguchi

    发明人： Fuyuhiko Sakyu ,  Satoshi Yoshikawa ,  Satoru Okamoto ,  Yasuo Hibino ,  Yoshio Nishiguchi

    IPC分类号： C07C17/20 ,  C07C17/38

    CPC分类号： C07C17/20 ,  C01B7/07 ,  C01B7/195 ,  C07C17/206 ,  C07C17/25 ,  C07C17/38 ,  C07C21/18

    摘要： According to the first characteristic of the present invention, there is provided a production process for 1,3,3,3-tetrafluoropropene including: the first step of reacting 1,1,1,3,3-pentachloropropane with hydrogen fluoride thereby obtaining 1-chloro-3,3,3-trifluoropropene; and the second step of reacting 1-chloro-3,3,3-trifluoropropene obtained in the first step with hydrogen fluoride in a gaseous phase in the presence of a fluorination catalyst. According to the second characteristic of the present invention, there is provided a dehydration process including bringing 1,3,3,3-tetrafluoropropene containing at least water into contact with zeolite.

    摘要翻译： 根据本发明的第一特征，提供了一种1,3,3,3-四氟丙烯的制备方法，包括：使1,1,1,3,3-五氯丙烷与氟化氢反应的第一步骤，从而得到1 - 氯-3,3,3-三氟丙烯; 在氟化催化剂存在下，将第一步得到的1-氯-3,3,3-三氟丙烯与氟化氢反应的气相的第二步。 根据本发明的第二特征，提供了使至少含有水的1,3,3,3-四氟丙烯与沸石接触的脱水方法。

    Process for production of 2-chloro-3,3,3-trifluoropropene
    8.
    发明授权
    Process for production of 2-chloro-3,3,3-trifluoropropene 失效
    2-氯-3,3,3-三氟丙烯的制备方法

    公开(公告)号：US08563790B2

    公开(公告)日：2013-10-22

    申请号：US13383708

    申请日：2010-07-16

    申请人： Yasuo Hibino ,  Fumihiro Kawagoe ,  Fuyuhiko Sakyu

    发明人： Yasuo Hibino ,  Fumihiro Kawagoe ,  Fuyuhiko Sakyu

    IPC分类号： C07C19/08

    CPC分类号： C07C17/23 ,  B01J21/18 ,  B01J23/44 ,  B01J23/628 ,  B01J23/6447 ,  C07C21/18

    摘要： There is provided according the present invention a process for producing 2-chloro-3,3,3-trifluoropropene, comprising: hydrogenating 1,2-dichloro-3,3,3-trifluoropropene with hydrogen (H2) in the presence of a catalyst having a transition metal and a poisoning substance supported on a support. The present production process is industrially advantageous as the target 2-chloro-3,3,3-trifluoropropene can be obtained with high selectivity and high yield under moderate reaction conditions and with easy waste treatment.

    摘要翻译： 根据本发明提供了一种2-氯-3,3,3-三氟丙烯的制备方法，包括：在催化剂存在下用氢气（H 2）氢化1,2-二氯-3,3,3-三氟丙烯 具有负载在载体上的过渡金属和中毒物质。 本发明的制备方法在工业上是有利的，因为在中等反应条件下容易的废物处理可以以高选择性和高收率获得目标2-氯-3,3,3-三氟丙烯。

    Production Method Of Trans-1,3,3,3-Tetrafluoropropene
    9.
    发明申请
    Production Method Of Trans-1,3,3,3-Tetrafluoropropene 审中-公开
    反式1,3,3,3-四氟丙烯的制备方法

    公开(公告)号：US20120123172A1

    公开(公告)日：2012-05-17

    申请号：US13273985

    申请日：2011-10-14

    申请人： Yasuo Hibino ,  Satoshi Yoshikawa ,  Yoshio Nishiguchi ,  Satoru Okamoto ,  Fuyuhiko Sakyu

    发明人： Yasuo Hibino ,  Satoshi Yoshikawa ,  Yoshio Nishiguchi ,  Satoru Okamoto ,  Fuyuhiko Sakyu

    IPC分类号： C07C17/20

    CPC分类号： C07C17/206 ,  B01J21/04 ,  B01J21/18 ,  B01J23/26 ,  B01J27/12 ,  B01J27/128 ,  B01J27/132 ,  B01J27/135 ,  B01J27/138 ,  B01J37/0201 ,  B01J37/26 ,  C01B7/0737 ,  C01B7/196 ,  C01B7/197 ,  C07C17/38 ,  C07C17/383 ,  Y02P20/582 ,  C07C21/18

    摘要： Production of trans-1,3,3,3-tetrafluoropropene by reacting 1-chloro-3,3,3-trifluoropropene with hydrogen fluoride to obtain a reaction product A containing formed trans-1,3,3,3-tetrafluoropropene, unreacted 1-chloro-3,3,3-trifloropropene and hydrogen fluoride, and by-product cis-1,3,3,3-tetrafluoropropene, 1,1,1,3,3-pentafluoropropane and hydrogen chloride; distilling reaction product A to recover a distillation bottom product containing 1-chloro-3,3,3-trifloropropene and hydrogen fluoride and supplying recovered distillation bottom product to the reacting step; recovering hydrogen fluoride from a residue B remaining after recovery of the distillation bottom product and supplying recovered hydrogen fluoride to the reacting step; contacting a residue C remaining after recovery of hydrogen fluoride with water or aqueous sodium hydroxide solution to separate hydrogen chloride; dehydrating a residue D remaining after separation of hydrogen chloride; and distilling a residue E remaining after the dehydration to obtain trans-1,3,3,3-tetrafluoropropene. The method reuses unreacted reactants and produces the target compound efficiently.

    摘要翻译： 通过使1-氯-3,3,3-三氟丙烯与氟化氢反应制备反式-1,3,3,3-四氟丙烯，得到含有形成的反式-1,3,3,3-四氟丙烯的反应产物A，未反应 1-氯-3,3,3-三氟丙烯和氟化氢，以及副产物顺式-1,3,3,3-四氟丙烯，1,1,1,3,3-五氟丙烷和氯化氢; 蒸馏反应产物A以回收含有1-氯-3,3,3-三氯丙烯和氟化氢的蒸馏塔底产物，并将回收的蒸馏塔底产物供应至反应步骤; 从蒸馏塔底产物回收剩余的残渣B回收氟化氢，并将回收的氟化氢供应到反应步骤; 使氟化氢与水或氢氧化钠水溶液回收后残留的C残留物与氯化氢分离; 使氯化氢分离后剩余的残渣D脱水; 并蒸馏出脱水后残留的E，得到反式-1,3,3,3-四氟丙烯。 该方法重新使用未反应的反应物并有效地产生目标化合物。

    Protective Gas For Metal Production
    10.
    发明申请
    Protective Gas For Metal Production 审中-公开
    金属生产用保护气体

    公开(公告)号：US20080163956A1

    公开(公告)日：2008-07-10

    申请号：US11884734

    申请日：2006-04-26

    申请人： Yasuo Hibino ,  Ryoichi Tamai ,  Satoru Okamoto ,  Fuyuhiko Sakyu

    发明人： Yasuo Hibino ,  Ryoichi Tamai ,  Satoru Okamoto ,  Fuyuhiko Sakyu

    IPC分类号： C23C26/00 ,  C09K15/04

    CPC分类号： B22D21/007 ,  B22D46/00

    摘要： There is provided a protective gas composition for preventing a rapid oxidation or combustion of a molten magnesium/magnesium alloy, comprising a fluorine-containing organic compound and a carrier gas. Furthermore, there is provided a method for preventing a rapid oxidation or combustion of a molten magnesium or magnesium alloy, which is characterized in that the above gas composition is used as a protective gas for preventing an oxidation or combustion of a molten magnesium or magnesium alloy in a magnesium or magnesium alloy production.

    摘要翻译： 提供了一种用于防止包含含氟有机化合物和载气的熔融镁/镁合金的快速氧化或燃烧的保护气体组合物。 此外，提供了一种防止镁或镁合金熔融物的快速氧化或燃烧的方法，其特征在于，上述气体组合物用作防止熔融镁或镁合金的氧化或燃烧的保护气体 在镁或镁合金生产中。