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    Process for the manufacture of ethylenediamine
    1.
    发明授权
    Process for the manufacture of ethylenediamine 失效
    制造乙二胺的方法

    公开(公告)号：US4400539A

    公开(公告)日：1983-08-23

    申请号：US307215

    申请日：1981-09-30

    Applicant: Charles A. Gibson ,  John R. Winters

    Inventor： Charles A. Gibson ,  John R. Winters

    IPC: C07B61/00 ,  B01J23/00 ,  B01J23/84 ,  C07C67/00 ,  C07C209/00 ,  C07C209/16 ,  C07C209/60 ,  C07C211/10 ,  C07C85/06 ,  C07C89/02

    CPC classification number: C07C209/60

    Abstract: There is described a continuous process for the manufacture of ethylenediamine from the products of the reaction of ethylene oxide and ammonia, provision of a continuous recycle stream of monoethanolamine to the products of the reaction of ethylene oxide and ammonia, the amination of such products of the reaction of ethylene oxide and ammonia combined with the monoethanolamine recycle in which the feed stream to the amination reaction zone contains at least 70 weight percent monoethanolamine as well as diethanolamine and triethanolamine, the moles of ammonia provided to the amination reaction exceeds the molar concentration of alcoholic hydroxyl groups present in the amination feed, and the feed to the amination reactor contains at least a 5% increase in the concentration of monoethanolamine over the concentration of monoethanolamine in the reaction product stream from the reaction of ethylene oxide and ammonia.

    Abstract translation: 描述了从环氧乙烷和氨的反应产物制备乙二胺的连续方法，提供了单乙醇胺的连续再循环流到环氧乙烷和氨的反应产物，胺化这些产物的 环氧乙烷和氨与单乙醇胺再循环的反应，其中进入胺化反应区的进料流含有至少70重量％的单乙醇胺以及二乙醇胺和三乙醇胺，提供给胺化反应的氨的摩尔数超过醇的摩尔浓度 存在于胺化进料中的羟基，并且来自胺化反应器的进料包含来自环氧乙烷和氨的反应的反应产物流中单乙醇胺浓度比单乙醇胺浓度增加至少5％。

    Articulated catheter
    3.
    发明授权
    Articulated catheter 有权
    铰接导管

    公开(公告)号：US08007462B2

    公开(公告)日：2011-08-30

    申请号：US10536109

    申请日：2005-05-17

    Applicant: Charles A. Gibson ,  Gary O'Boyle ,  Gary S. Falwell

    Inventor： Charles A. Gibson ,  Gary O'Boyle ,  Gary S. Falwell

    IPC: A61M31/00 ,  A61M37/00 ,  A61M25/00

    CPC classification number: A61M25/0147 ,  A61M25/0041 ,  A61M25/0054 ,  A61M25/0108 ,  A61M25/0141 ,  A61M25/0144 ,  A61M2025/0161

    Abstract: Methods and apparatuses for manipulating an elongated flexible shaft of a catheter provide case and reliability of positioning electrodes against or near tissue. Dual-bend flexible distal tips (30) may be used in combination with flat wires. In some embodiments, flat wires which are free to rotate upon initial bending of shaft segments are employed. In some embodiments, one or more transition segments (48) are used to relocate the satellite lumen-to-main lumen transition of pull wires (42, 40) away from a change in shaft stiffness.

    Abstract translation: 用于操纵导管的细长柔性轴的方法和装置提供了定位电极抵靠或靠近组织的壳体和可靠性。 双弯曲柔性远端头（30）可以与扁平线组合使用。 在一些实施例中，采用在轴段的初始弯曲时自由旋转的扁平线。 在一些实施例中，一个或多个过渡段（48）用于将拉线（42,44）的卫星管腔到主腔的过渡位置远离轴刚度的变化。

    Irrigated Catheter
    4.
    发明申请
    Irrigated Catheter 有权
    灌溉导管

    公开(公告)号：US20100152727A1

    公开(公告)日：2010-06-17

    申请号：US11596722

    申请日：2005-05-17

    Applicant: Charles A. Gibson ,  Gary S. Falwell ,  Hab Seang

    Inventor： Charles A. Gibson ,  Gary S. Falwell ,  Hab Seang

    IPC: A61B18/14

    CPC classification number: A61B18/1492 ,  A61B2018/00029

    Abstract: Apparatus for irrigating an electrode of a catheter are disclosed. Among other things, a catheter is disclosed that comprises a shaft portion including a fluid passage to conduct fluid, an electrode coupled to a distal end of the shaft portion, and a handle portion coupled to a proximal end of the shaft portion. A portion of the fluid passage defines an opening in the shaft portion. The opening is constructed and arranged such that when fluid is conducted through the fluid passage, at least some of the fluid will contact the electrode after passing through the opening in the shaft portion.

    Abstract translation: 公开了一种用于冲洗导管电极的装置。 除其他之外，公开了一种导管，其包括轴部分，其包括用于传导流体的流体通道，耦合到所述轴部分的远端的电极以及联接到所述轴部分的近端的手柄部分。 流体通道的一部分在轴部分中限定开口。 开口被构造和布置成使得当流体通过流体通道传导时，至少一些流体在通过轴部分中的开口之后将接触电极。

    Internal mechanism for displacing a slidable electrode
    5.
    发明授权
    Internal mechanism for displacing a slidable electrode 有权
    用于移动可滑动电极的内部机构

    公开(公告)号：US06178354B1

    公开(公告)日：2001-01-23

    申请号：US09203922

    申请日：1998-12-02

    Applicant: Charles A. Gibson

    Inventor： Charles A. Gibson

    IPC: A61N105

    CPC classification number: A61B18/1492 ,  A61B18/1815 ,  A61B2018/00369 ,  A61B2018/00916 ,  A61B2018/00946

    Abstract: A medical device is disclosed which includes a displaceable electrode slidably mounted over the device. An electrode displacement mechanism is connected to the electrode, and may be actuated to displace the electrode relative to the medical device. The medical device may be used for therapeutic, diagnostic, or other medical procedures.

    Abstract translation: 公开了一种医疗装置，其包括可滑动地安装在装置上的可移位电极。 电极位移机构连接到电极，并且可以被致动以使电极相对于医疗装置移位。 该医疗装置可用于治疗，诊断或其他医疗程序。

    Aminoethylethanolamine producers composition and method for producing same
    6.
    发明授权
    Aminoethylethanolamine producers composition and method for producing same 失效
    氨基乙基乙醇胺生产者的组成及其制备方法

    公开(公告)号：US4973692A

    公开(公告)日：1990-11-27

    申请号：US102931

    申请日：1987-09-30

    Applicant: Lloyd M. Burgess ,  Charles A. Gibson

    Inventor： Lloyd M. Burgess ,  Charles A. Gibson

    IPC: C07C209/16 ,  C07C213/02 ,  C07D295/023

    CPC classification number: C07D295/023 ,  C07C209/16 ,  C07C213/02

    Abstract: A continuously generated alkyleneamines producers composition comprising, based on 100% of the moles of the composition and exclusive of any MEA and water present,(a) about 50 to about 90 mole % AEEA,(b) less than about 3 mole % EDA but more than 0.01 mole % EDA,(c) less than about 2 mole % DETA but more than 0.01 mole % DETA,(d) about 5 to about 18 mole % of the combination of PIP, AEP and HEP,(e) about 5 to about 20 mole % of one or more of TETAs and TEPAs,(f) less than about 1 mole % of other polyalkylene polyamines,(g) a mole ratio of AEEA to the combination of PIP, AEP, HEP, DETA and EDA is greater than about 2.5,(h) an AEEA to EDA mole ratio greater than about 22 and(i) an AEEA to PIP mole ratio greater than about 7;and a process of manufacturing the same, which comprises feeding hydrogen and MEA to a reaction zone containing a fixed bed of a reductive amination catalyst, wherein the hydrogen comprises about 20 to about 80 mole percent of the feed in the reaction zone, the temperature of the reaction zone is about 120.degree. C. to about 300.degree. C., the pressure of the reaction zone is about 200 to about 1200 psig, the conversion of MEA is about 15 to about 42 weight percent, and recovering said producers composition from the reaction zone.

    Abstract translation: 连续生成的亚烷基胺生产商组合物包含基于组合物摩尔数的100％而不是存在的任何MEA和水，（a）约50至约90摩尔％的AEEA，（b）小于约3摩尔％的EDA，但 大于0.01摩尔％的EDA，（c）小于约2摩尔％的DETA但大于0.01摩尔％的DETA，（d）约5至约18摩尔％的PIP，AEP和HEP的组合，（e）约5摩尔％ 至约20摩尔％的一种或多种TETA和TEPAs，（f）小于约1摩尔％的其它多亚烷基多胺，（g）AEEA与PIP，AEP，HEP，DETA和EDA的组合的摩尔比为 大于约2.5，（h）AEEA与EDA摩尔比大于约22，和（i）AEEA至PIP摩尔比大于约7; 以及其制造方法，其包括将氢气和MEA进料到含有还原胺化催化剂的固定床的反应区，其中氢包含反应区中进料的约20至约80摩尔％，温度 反应区为约120℃至约300℃，反应区的压力为约200至约1200psig，MEA的转化率为约15至约42重量％，并将所述生产者组合物从 反应区。

    Steerable catheter
    9.
    发明授权
    Steerable catheter 有权
    导向导管

    公开(公告)号：US07232422B2

    公开(公告)日：2007-06-19

    申请号：US10929629

    申请日：2004-08-30

    Applicant: Charles A. Gibson ,  Hab Seang

    Inventor： Charles A. Gibson ,  Hab Seang

    IPC: A61M31/00 ,  A61M37/00

    CPC classification number: A61M25/0147 ,  A61M2025/0161

    Abstract: A catheter includes a pull wire which extends through two different lumen and attaches to the distal end of the catheter at an off-axis location. By tensioning the pull wire, the catheter can assume various complex curves, depending on the respective lumen through which the pull wire passes.

    Abstract translation: 导管包括拉线，其延伸穿过两个不同的内腔并且在离轴位置处附接到导管的远端。 通过拉紧拉线，根据拉丝通过的相应内腔，导管可以呈现各种复杂曲线。

    Method for decolorization of alkanolamines and alkyleneamines
    10.
    发明授权
    Method for decolorization of alkanolamines and alkyleneamines 失效
    链烷醇胺和亚烷基胺脱色方法

    公开(公告)号：US5331102A

    公开(公告)日：1994-07-19

    申请号：US083663

    申请日：1993-06-28

    Applicant: Charles A. Gibson

    Inventor： Charles A. Gibson

    IPC: B01J27/053 ,  B01J27/125 ,  B01J27/135 ,  C07B61/00 ,  C07C209/84 ,  C07C211/14 ,  C07C213/10 ,  C07C215/14

    CPC classification number: C07C209/84

    Abstract: Color-containing alkanolamines or alkyleneamines, having color numbers of up to 100 PtCo or higher, can be treated with inorganic solid acidic catalysts. Inorganic support materials having bonded inorganic acid functionalities may be used as the inorganic solid acidic catalysts. In the presence of water, these inorganic solid acidic catalysts produce decolorized alkanolamines or alkyleneamines having color numbers of 20 PtCo or less. The process of decolorization can be carried out in batch or continuous mode processes thus providing low cost, high quality and high purity end products.

    Abstract translation: 具有高达100 PtCo或更高颜色的含颜料的链烷醇胺或亚烷基胺可用无机固体酸性催化剂处理。 可以使用具有键合的无机酸官能团的无机载体材料作为无机固体酸性催化剂。 在水的存在下，这些无机固体酸性催化剂产生颜色为20 PtCo或更低的脱色烷醇胺或亚烷基胺。 脱色过程可以分批或连续模式进行，从而提供低成本，高质量和高纯度的最终产品。

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