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    PROCESS FOR THE PRODUCTION OF CHLORINATED ALKANES
    1.
    发明申请
    PROCESS FOR THE PRODUCTION OF CHLORINATED ALKANES 有权
    生产氯化碱的方法

    公开(公告)号：US20150045592A1

    公开(公告)日：2015-02-12

    申请号：US14358079

    申请日：2012-11-13

    Applicant: Matthew L. Grandbois ,  William J. Kruper, JR.

    Inventor： Matthew L. Grandbois ,  William J. Kruper, JR.

    IPC: C07C17/013

    CPC classification number: C07C17/013 ,  C07C17/10 ,  C07C19/01

    Abstract: Processes for the production of chlorinated alkanes are provided. The present processes comprise reacting one or more mono- and/or dichloroalkanes to form tri-, tetra- and/or pentachloroalkanes, with high regioselectivity. In those embodiments wherein a dichloroalkane is desirably utilized, it may advantageously be a vicinal dichloroalkane. Further, only one catalyst is utilized. The present processes make use of sulfuryl chloride as a chlorinating agent, rather than a gaseous chlorinating agent such as chlorine gas. Finally, the process uses lower intensity process conditions than at least some conventional processes, and thus, operating costs are saved.

    Abstract translation: 提供了生产氯代烷烃的方法。 本方法包括使一种或多种单 - 和/或二氯烷烃反应形成具有高区域选择性的三，四和/或五氯代烷烃。 在其中希望使用二氯烷烃的那些实施方案中，它可以有利地是连续的二氯烷烃。 此外，仅使用一种催化剂。 本方法使用磺酰氯作为氯化剂，而不是气态氯化剂如氯气。 最后，该方法使用比至少一些常规方法更低强度的工艺条件，因此节省了操作成本。

    PROCESS FOR THE PRODUCTION OF CHLORINATED PROPENES
    2.
    发明申请
    PROCESS FOR THE PRODUCTION OF CHLORINATED PROPENES 有权
    生产氯化丙烯的方法

    公开(公告)号：US20140081055A1

    公开(公告)日：2014-03-20

    申请号：US14123139

    申请日：2012-05-18

    Applicant: Max M. Tirtowidjojo ,  William J. Kruper, JR. ,  Barry B. Fish ,  David S. Laitar

    Inventor： Max M. Tirtowidjojo ,  William J. Kruper, JR. ,  Barry B. Fish ,  David S. Laitar

    IPC: C07C17/25

    CPC classification number: C07C17/25 ,  C07C17/10 ,  C07C19/01 ,  C07C21/04

    Abstract: Processes for the production of chlorinated propenes are provided. The present processes make use of 1,2-dichloropropane, a by-product in the production of chlorohydrin, as a low cost starting material, alone or in combination with 1,2,3-trichloropropane. The present processes can also generate anhydrous HCl as a byproduct that can be removed from the process and used as a feedstock for other processes, providing further time and cost savings. Finally, the processes are advantageously conducted in the liquid phase, thereby presenting additional savings as compared to conventional, gas phase processes.

    Abstract translation: 提供了生产氯化丙烯的方法。 本发明方法利用1,2-二氯丙烷作为生产氯代醇中的副产物，作为低成本原料，单独使用或与1,2,3-三氯丙烷组合使用。 本方法还可以产生作为副产物的无水HCl，其可从该方法中除去并用作其它方法的原料，从而进一步节省时间和成本。 最后，该方法有利地在液相中进行，从而与常规的气相方法相比可以节省更多的费用。

    Activator composition comprising aluminum compound mixture
    6.
    发明授权
    Activator composition comprising aluminum compound mixture 有权
    包含铝化合物混合物的活化剂组合物

    公开(公告)号：US06387838B2

    公开(公告)日：2002-05-14

    申请号：US09772592

    申请日：2001-01-30

    Applicant: Eugene Y. Chen ,  Gordon R. Roof ,  William J. Kruper, Jr. ,  David J. Schwartz ,  Joey W. Storer

    Inventor： Eugene Y. Chen ,  Gordon R. Roof ,  William J. Kruper, Jr. ,  David J. Schwartz ,  Joey W. Storer

    IPC: B01J3100

    CPC classification number: C07F5/066 ,  C07F7/10 ,  C07F17/00 ,  C08F10/00 ,  C08F110/06 ,  C08F210/16 ,  C08F4/61912 ,  C08F210/14 ,  C08F2500/12 ,  C08F4/65927 ,  C08F4/6592 ,  C08F4/65912

    Abstract: Compositions comprising: A) an aluminum compound corresponding to the formula AlArf3, where Arf is a fluorinated aromatic hydrocarbyl moiety of from 6 to 30 carbon atoms; B) an aluminum compound corresponding to the formula: AlArfQ1Q2, or a dimer, adduct, or mixture thereof; where: Arf is as previously defined; Q1 is Arf or a C1-20 hydrocarbyl group, optionally substituted with one or more cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally, such substituents may be covalently linked with each other to form one or more fused rings or ring systems; and Q2 is an aryloxy, arylsulfide or di(hydrocarbyl)amido group, optionally substituted with one or more hydrocarbyl, cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally such substituents may be covalently linked with each other to form one or more fused rings or ring systems, said Q2 having from 3 to 20 atoms other than hydrogen; and the molar ratio of A):B) in the composition being from 0.1:1 to 10:1 are useful as activators for olefin polymerizations.

    Abstract translation: 组合物，其包含：A）对应于式AlArf 3的铝化合物，其中Arf为6至30个碳原子的氟化芳族烃基部分; B）对应于式AlArfQ1Q2的铝化合物或其二聚物，加合物或其混合物 ; 其中：Arf如前所定义; Q 1是Arf或C 1-20烃基，任选被一个或多个环烃基，烃氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基 ，二（烃基）膦基或具有除氢以外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可彼此共价连接以形成一个或多个稠环或环系; 环烷氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）氨基， 烃基）膦基或具有除氢之外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可以彼此共价连接以形成一个或多个稠环或环系，所述Q2具有3至20个原子的其它 比氢; 并且组分中A）：B）的摩尔比为0.1:1至10:1可用作烯烃聚合的活化剂。

    Three coordinate aluminum catalyst activator composition
    7.
    发明授权
    Three coordinate aluminum catalyst activator composition 有权
    三配位铝催化剂活化剂组成

    公开(公告)号：US06187940B1

    公开(公告)日：2001-02-13

    申请号：US09330671

    申请日：1999-06-11

    Applicant: Eugene Y. Chen ,  William J. Kruper, Jr. ,  Gordon R. Roof ,  David J. Schwartz ,  Joey W. Storer

    Inventor： Eugene Y. Chen ,  William J. Kruper, Jr. ,  Gordon R. Roof ,  David J. Schwartz ,  Joey W. Storer

    IPC: C07F506

    CPC classification number: C08F10/00 ,  C07F5/062 ,  C07F5/066 ,  C08F4/6592 ,  C08F4/65927 ,  C08F110/06 ,  C08F210/16 ,  Y10S526/943 ,  C08F4/642 ,  C08F4/65912 ,  C08F210/14 ,  C08F2500/12

    Abstract: Compounds corresponding to the formula: AlArfQ1Q2, or a dimer, adduct, or mixture thereof and further mixtures with aluminum compounds of the formula AlArf3, where: Arf is a fluorinated aromatic hydrocarbyl moiety of from 6 to 30 carbon atoms; Q1 is Af or a C1-20 hydrocarbyl group, optionally substituted with one or more cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally, such substituents may be covalently linked with each other to form one or more fused rings or ring systems; and Q2 is an aryloxy, arylsulfide or di(hydrocarbyl)amido group, optionally substituted with one or more hydrocarbyl, cyclohydrocarbyl, hydrocarbyloxy, hydrocarbylsiloxy, hydrocarbylsilylamino, hydrocarbylsilyl, silylhydrocarbyl, di(hydrocarbylsilyl)amino, hydrocarbylamino, di(hydrocarbyl)amino, di(hydrocarbyl)phosphino, or hydrocarbylsulfido groups having from 1 to 20 atoms other than hydrogen, or, further optionally such substituents may be covalently linked with each other to form one or more fused rings or ring systems, said Q2 having from 3 to 20 atoms other than hydrogen are useful as activators for olefin polymerizations.

    Abstract translation: 对应于下式的AlArfQ1Q2或其二聚物，加合物或其混合物的化合物以及与式AlArf 3的铝化合物的进一步混合物，其中：Arf为6至30个碳原子的氟化芳族烃基部分; Q1为Af或 任选被一个或多个环烃基，烃氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）膦基或烃基亚磺酰基取代的C 1-20烃基， 至20个除氢以外的原子，或者进一步任选地，这些取代基可彼此共价连接以形成一个或多个稠环或环系; 环烷氧基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷氧基，烃基甲硅烷基氨基，烃基甲硅烷基，甲硅烷基烃基，二（烃基甲硅烷基）氨基，烃基氨基，二（烃基）氨基，二（烃基）氨基， 烃基）膦基或具有除氢之外的1至20个原子的烃基硫基，或者进一步任选地，这些取代基可以彼此共价连接以形成一个或多个稠环或环系，所述Q2具有3至20个原子的其它 氢可用作烯烃聚合的活化剂。

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