HIERARCHICAL POROUS ZRO2 MATERIAL, METHOD OF PREPARING THE SAME, AND APPLICATION THEREOF

    公开(公告)号:US20200325035A1

    公开(公告)日:2020-10-15

    申请号:US16826032

    申请日:2020-03-20

    IPC分类号: C01G25/02

    摘要: A method for preparing a hierarchical porous ZrO2 includes the following steps: S1, dissolving a triblock copolymer in an organic solvent to obtain a solution A, dissolving a tannin extract in distilled water to obtain a solution B, mixing the solution A and the solution B and stirring to obtain a mixed solution; S2, adding a zirconium salt to the mixed solution obtained in step S1 and stirring; S3, heating the mixed solution obtained in step S2 in an oven to obtain ZrO2, promoting the conversion of the crystal form of ZrO2; S4, calcining ZrO2 at a high temperature to obtain the hierarchical porous ZrO2.

    Hierarchical porous ZrO2 material, method of preparing the same, and application thereof

    公开(公告)号:US11299400B2

    公开(公告)日:2022-04-12

    申请号:US16826032

    申请日:2020-03-20

    IPC分类号: C01G25/02

    摘要: A method for preparing a hierarchical porous ZrO2 includes the following steps: S1, dissolving a triblock copolymer in an organic solvent to obtain a solution A, dissolving a tannin extract in distilled water to obtain a solution B, mixing the solution A and the solution B and stirring to obtain a mixed solution; S2, adding a zirconium salt to the mixed solution obtained in step S1 and stirring; S3, heating the mixed solution obtained in step S2 in an oven to obtain ZrO2, promoting the conversion of the crystal form of ZrO2; S4, calcining ZrO2 at a high temperature to obtain the hierarchical porous ZrO2.

    Method for preparing high fluffiness down by multiple treatments with metal salts

    公开(公告)号:US10760209B1

    公开(公告)日:2020-09-01

    申请号:US16805781

    申请日:2020-03-01

    IPC分类号: D06M19/00

    摘要: A method for preparing a high fluffiness down by multiple treatments with metal salts includes: degreasing a down sample with a degreasing agent; washing the down sample with water; oxidizing the down sample with an oxidizing agent; washing the down sample with water; conducting a first crosslinking treatment with basic zirconium sulfate; washing the down sample with water; conducting a second crosslinking treatment with basic aluminum sulfate; washing the down sample with water; and drying the down sample to obtain the high fluffiness down.