公开(公告)号：US20110150736A1

公开(公告)日：2011-06-23

申请号：US13060161

申请日：2009-08-21

申请人： Yuji Hagiwara ,  Takanori Ochi ,  Kazunobu Ohata ,  Taisuke Kasahara ,  Taketo Toba ,  Keiichiro Mizuta ,  Hiromoto Katsuyama ,  Satoshi Ishida ,  Toshifumi Nishida

发明人： Yuji Hagiwara ,  Takanori Ochi ,  Kazunobu Ohata ,  Taisuke Kasahara ,  Taketo Toba ,  Keiichiro Mizuta ,  Hiromoto Katsuyama ,  Satoshi Ishida ,  Toshifumi Nishida

IPC分类号： C01B35/14 ,  C07F5/02

CPC分类号： C07F9/65688 ,  C07D233/58 ,  C07F5/02 ,  C07F5/022 ,  H01B1/122

摘要： The present invention provides a method of producing a tetracyanoborate-containing ionic compound in a milder condition more efficiently and less expensively than conventional methods, and a tetracyanoborate-containing ionic compound having a reduced content of impure components. An ionic compound of the present invention is represented by the following general formula (I), has a content of fluorine atom-containing impurities of 3 mol % or less per 100 mol % of the ionic compound, and a method for producing an ionic compound represented by the general formula (I) of the present invention comprises a step of reacting starting materials containing a cyanide and a boron compound. (In the formula, Ktm+ denotes an organic cation [Ktb]m+ or an inorganic cation [Ke]m+; and m denotes an integer of 1 to 3.)

摘要翻译： 本发明提供了一种以比常规方法更有效和低成本地更温和的方式制备含四氰基硼酸盐的离子化合物的方法，以及具有降低的不纯成分含量的含四氰基硼酸盐的离子化合物。 本发明的离子性化合物由下述通式（I）表示，相对于每100摩尔％的离子性化合物，含有氟原子的杂质含量为3摩尔％以下，以及离子性化合物的制造方法 由本发明的通式（I）表示的方法包括使含有氰化物和硼化合物的原料反应的步骤。 （式中，Ktm +表示有机阳离子[Ktb] m +或无机阳离子[Ke] m +，m表示1〜3的整数）

公开(公告)号：US09243013B2

公开(公告)日：2016-01-26

申请号：US13060161

申请日：2009-08-21

申请人： Yuji Hagiwara ,  Takanori Ochi ,  Kazunobu Ohata ,  Taisuke Kasahara ,  Taketo Toba ,  Keiichiro Mizuta ,  Hiromoto Katsuyama ,  Satoshi Ishida ,  Toshifumi Nishida

发明人： Yuji Hagiwara ,  Takanori Ochi ,  Kazunobu Ohata ,  Taisuke Kasahara ,  Taketo Toba ,  Keiichiro Mizuta ,  Hiromoto Katsuyama ,  Satoshi Ishida ,  Toshifumi Nishida

IPC分类号： C07F5/02 ,  C07F9/02 ,  C07F9/6568 ,  C07D233/58 ,  H01B1/12

CPC分类号： C07F9/65688 ,  C07D233/58 ,  C07F5/02 ,  C07F5/022 ,  H01B1/122

摘要： The present invention provides a method of producing a tetracyanoborate-containing ionic compound in a milder condition more efficiently and less expensively than conventional methods, and a tetracyanoborate-containing ionic compound having a reduced content of impure components. An ionic compound of the present invention is represented by the following general formula (I), has a content of fluorine atom-containing impurities of 3 mol % or less per 100 mol % of the ionic compound, and a method for producing an ionic compound represented by the general formula (I) of the present invention comprises a step of reacting starting materials containing a cyanide and a boron compound. (In the formula, Ktm+ denotes an organic cation [Ktb]m+ or an inorganic cation [Ke]m+; and m denotes an integer of 1 to 3.)

摘要翻译： 本发明提供了一种以比常规方法更有效和低成本地更温和的方式制备含四氰基硼酸盐的离子化合物的方法，以及具有降低的不纯成分含量的含四氰基硼酸盐的离子化合物。 本发明的离子性化合物由下述通式（I）表示，相对于每100摩尔％的离子性化合物，含有氟原子的杂质含量为3摩尔％以下，以及离子性化合物的制造方法 由本发明的通式（I）表示的方法包括使含有氰化物和硼化合物的原料反应的步骤。 （式中，Ktm +表示有机阳离子[Ktb] m +或无机阳离子[Ke] m +，m表示1〜3的整数）

公开(公告)号：US20140217322A1

公开(公告)日：2014-08-07

申请号：US13983428

申请日：2012-01-17

申请人： Kinji Yamada ,  Ho-Jin Lee ,  Toshimitsu Kikuchi ,  Taisuke Kasahara ,  Hiromoto Katsuyama

发明人： Kinji Yamada ,  Ho-Jin Lee ,  Toshimitsu Kikuchi ,  Taisuke Kasahara ,  Hiromoto Katsuyama

IPC分类号： H01G11/56

CPC分类号： H01G11/56 ,  H01G11/06 ,  H01G11/62 ,  H01G11/64 ,  Y02E60/13

摘要： A lithium-ion capacitor includes a non-aqueous electrolyte solution that includes (A) a compound represented by the following general formula (1), (B) a cyclic carbonate ester that includes at least one carbon-carbon unsaturated bond, and (C) a carboxylic ester, the non-aqueous electrolyte solution having a ratio (MB/MC) of 0.001 to 0.5, the ratio (MB/MC) being the ratio of the content (MB) (mmol/g) of the cyclic carbonate ester (B) to the content (MC) (mmol/g) of the carboxylic ester (C). Z+.[X(CN)m(Y)n]−  (1) wherein X is at least one element selected from boron, aluminum, silicon, phosphorus, and arsenic, Y is a halogen, Z is lithium or magnesium, m is an integer from 3 to 6, and n is an integer from 0 to 5, provided that m+n≧3.

摘要翻译： 锂离子电容器包括非水电解液，其包含（A）由以下通式（1）表示的化合物，（B）包含至少一个碳 - 碳不饱和键的环状碳酸酯和（C ）羧酸酯，所述非水电解质溶液的比例（MB / MC）为0.001〜0.5，所述比例（MB / MC）为所述环状碳酸酯的含量比（MB）（mmol / g） （B）至羧酸酯（C）的含量（MC）（mmol / g）。 Z +。[X（CN）m（Y）n] - （1）其中X是选自硼，铝，硅，磷和砷中的至少一种元素，Y是卤素，Z是锂或镁，m是 3〜6的整数，n为0〜5的整数，m +n≥3。

公开(公告)号：US20080206647A1

公开(公告)日：2008-08-28

申请号：US12071233

申请日：2008-02-19

申请人： Hiromoto Katsuyama ,  Kazuo Takei ,  Taketo Toba

发明人： Hiromoto Katsuyama ,  Kazuo Takei ,  Taketo Toba

IPC分类号： H01M6/18 ,  C08G65/04 ,  C08K5/09

CPC分类号： H01M4/621 ,  C08G65/10 ,  C08G65/14 ,  C08K5/098 ,  C08L2205/05 ,  H01M4/622 ,  H01M10/052 ,  H01M10/0565 ,  C08L71/02

摘要： An ethylene oxide copolymer of the present invention has a crystallization temperature of not more than 20° C. and a glass transition temperature of not more than −64° C. This makes it possible to provide an ethylene oxide copolymer in which increase in the glass transition temperature is small even when metal salt is added, and a polymer composition including the ethylene oxide copolymer.

摘要翻译： 本发明的环氧乙烷共聚物的结晶温度为20℃以下，玻璃化转变温度为-64℃以下。可以提供一种环氧乙烷共聚物，其中玻璃的增加 即使添加金属盐，转变温度也低，以及包含环氧乙烷共聚物的聚合物组合物。

公开(公告)号：US20050245410A1

公开(公告)日：2005-11-03

申请号：US11061893

申请日：2005-02-18

申请人： Masaki Tezuka ,  Hiroshi Tanaka ,  Takao Yokohashi ,  Takao Nishihata ,  Manabu Kikuta ,  Michiyuki Kono ,  Tetsuya Higashizaki ,  Kazuo Takei ,  Taketo Toba ,  Toshiaki Kuriyama ,  Izuho Okada ,  Fumihide Tamura ,  Ritsuo Kitada ,  Shigetaka Takamiya ,  Jun Iwamura ,  Takanori Murakami ,  Hiromoto Katsuyama ,  Teruki Matsushita

发明人： Masaki Tezuka ,  Hiroshi Tanaka ,  Takao Yokohashi ,  Takao Nishihata ,  Manabu Kikuta ,  Michiyuki Kono ,  Tetsuya Higashizaki ,  Kazuo Takei ,  Taketo Toba ,  Toshiaki Kuriyama ,  Izuho Okada ,  Fumihide Tamura ,  Ritsuo Kitada ,  Shigetaka Takamiya ,  Jun Iwamura ,  Takanori Murakami ,  Hiromoto Katsuyama ,  Teruki Matsushita

IPC分类号： B29B9/04 ,  C08G65/30 ,  C08G65/46 ,  C08J3/12 ,  C08L71/02 ,  C11D17/00

CPC分类号： C08J3/12 ,  B29B9/04 ,  C08G65/30 ,  C08J2371/00 ,  C08L71/02

摘要： The residual amount of a solvent in a water soluble nonionic alkylene oxide resin is decreased in an apparatus including an evaporation vessel and a stirring blade which scrapes-up and coats resin solution onto the inner wall surface of the evaporation vessel. A water soluble nonionic alkylene oxide resin having a crystallization temperature of 10 to 60° C. is extruded to a predetermined thickness in a molten state, the extruded molten resin is brought into contact with a metal surface which is at the crystallization temperature (Tc) or lower, and the thereby solidified resin may be cut into pellets. The resin pellets preferably are of rectangular shape and prescribed dimensions. The resin may be pulverized in a pulverizer by shearing force between a rotary blade and a fixed blade. In the pulverizer, grains smaller than a predetermined size pass through the screen, while larger grains are again pulverized.

摘要翻译： 在包括蒸发容器和搅拌叶片的装置中，水溶性非离子环氧烷烃树脂中的溶剂的残留量减少，所述搅拌叶片刮擦并将树脂溶液涂覆在蒸发容器的内壁表面上。 将结晶温度为10〜60℃的水溶性非离子性环氧烷树脂在熔融状态下挤出至规定厚度，使熔融树脂与结晶化温度（Tc）的金属表面接触， 或更低，并且由此固化的树脂可以切成颗粒。 树脂颗粒优选为矩形形状和规定尺寸。 树脂可以通过旋转叶片和固定叶片之间的剪切力在粉碎机中粉碎。 在粉碎机中，小于预定尺寸的颗粒通过筛网，而较大的颗粒再次被粉碎。