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公开(公告)号：US08785554B2
公开(公告)日：2014-07-22
申请号：US13165096
申请日：2011-06-21
申请人： Colin Li Pi Shan , Kim L. Walton , Gary R. Marchand , Edmund M. Carnahan , Eddy I. Garcia-Meitin , Thomas Karjala
发明人： Colin Li Pi Shan , Kim L. Walton , Gary R. Marchand , Edmund M. Carnahan , Eddy I. Garcia-Meitin , Thomas Karjala
IPC分类号： C08L53/00
CPC分类号： C08L23/10 , C08L23/06 , C08L23/142 , C08L23/20 , C08L2205/03 , C08L2205/035 , C08L2205/08
摘要： Embodiments of the invention provide crystalline block composites and their use as compatibilizers. The crystalline block composites comprise i) a crystalline ethylene based polymer; ii) a crystalline alpha-olefin based polymer and iii) a block copolymer comprising a crystalline ethylene block and a crystalline alpha-olefin block.
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公开(公告)号：US08273838B2
公开(公告)日：2012-09-25
申请号：US11686444
申请日：2007-03-15
申请人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa Wilson Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , XiaoHua Qiu , Angela N. Taha
发明人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa Wilson Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , XiaoHua Qiu , Angela N. Taha
IPC分类号： C08F210/06 , C08F4/659
CPC分类号： C08F210/06 , C08F297/08 , C08F297/083 , C08F210/16 , C08F2500/03
摘要： Embodiments of the invention provide a class of propylene/α-olefin block interpolymers. The propylene/α-olefin interpolymers are characterized by an average block index, ABI, which is greater than zero and up to about 1.0 and a molecular weight distribution, Mw/Mn, greater than about 1.3. Preferably, the block index is from about 0.2 to about 1. In addition or alternatively, the block propylene/α-olefin interpolymer is characterized by having at least one fraction obtained by Temperature Rising Elution Fractionation (“TREF”), wherein the fraction has a block index greater than about 0.3 and up to about 1.0 and the propylene/α-olefin interpolymer has a molecular weight distribution, Mw/Mn, greater than about 1.3.
摘要翻译： 本发明的实施方案提供一类丙烯/α-烯烃嵌段互聚物。 丙烯/α-烯烃互聚物的特征在于平均嵌段指数ABI，其大于零且高达约1.0，分子量分布Mw / Mn大于约1.3。 优选地，嵌段指数为约0.2至约1.另外或替代地，嵌段丙烯/α-烯烃互聚物的特征在于具有通过升温洗脱分级（“TREF”）获得的至少一个馏分，其中部分具有 大于约0.3且高达约1.0的嵌段指数，丙烯/α-烯烃互聚物的分子量分布Mw / Mn大于约1.3。
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公开(公告)号：US20110313106A1
公开(公告)日：2011-12-22
申请号：US13165054
申请日：2011-06-21
申请人： Colin Li Pi Shan , Edmund M. Carnahan , Gary R. Marchand , Kim L. Walton , Thomas Karjala , Jeffrey D. Weinhold
发明人： Colin Li Pi Shan , Edmund M. Carnahan , Gary R. Marchand , Kim L. Walton , Thomas Karjala , Jeffrey D. Weinhold
IPC分类号： C08L53/00
CPC分类号： C08L23/10 , C08L23/06 , C08L23/142 , C08L23/20 , C08L2205/03 , C08L2205/035 , C08L2205/08
摘要： Embodiments of the invention provide crystalline block composites and their use as compatibilizers.
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4.发明申请Catalyst Composition Comprising Shuttling Agent for Ethylene Multi-Block Copolymer Formation 有权催化剂组合物包含乙烯多嵌段共聚物形成的穿梭剂公开(公告)号：US20110118416A1
公开(公告)日：2011-05-19
申请号：US12962800
申请日：2010-12-08
申请人： Daniel J. Arriola , Edmund M. Carnahan , Yunwa Wilson Cheung , David D. Devore , David D. Graf , Phillip D. Hustad , Roger L. Kuhlman , Colin Li Pi Shan , Benjamin C. Poon , Gordon R. Roof , James C. Stevens , Pamela J. Stirn , Timothy T. Wenzel
发明人： Daniel J. Arriola , Edmund M. Carnahan , Yunwa Wilson Cheung , David D. Devore , David D. Graf , Phillip D. Hustad , Roger L. Kuhlman , Colin Li Pi Shan , Benjamin C. Poon , Gordon R. Roof , James C. Stevens , Pamela J. Stirn , Timothy T. Wenzel
IPC分类号： C08F210/16
CPC分类号： B32B27/327 , B32B27/06 , B32B27/32 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08F4/65925 , C08F4/65927 , C08F10/00 , C08F10/14 , C08F110/02 , C08F210/14 , C08F210/16 , C08F295/00 , C08F297/00 , C08F297/08 , C08F297/083 , C08F297/086 , C08F2410/01 , C08F2410/04 , C08F2420/02 , C08L23/02 , C08L23/06 , C08L23/0815 , C08L23/0853 , C08L23/10 , C08L53/00 , C08L53/005 , Y10T428/24942 , Y10T428/24992 , Y10T428/2826 , Y10T428/31573 , Y10T428/31587 , C08F2/38 , C08F4/65904 , C08L2666/06 , C08F2500/09 , C08F2500/03 , C08F4/64148 , C08F4/64193 , C08F4/64048 , C08F4/6411 , C08F4/64144 , C08F2500/08 , C08F4/64113 , C08L2666/02 , C08L2666/04 , C08F2500/12 , C08F2500/20 , C08F210/08 , C08F2500/11 , C08F2500/21 , C08F210/02 , C08F212/08 , C08F232/02 , C08F232/08
摘要： A composition for use in forming a multi-block copolymer, said copolymer containing therein two or more segments or blocks differing in chemical or physical properties, a polymerization process using the same, and the resulting polymers, wherein the composition comprises the admixture or reaction product resulting from combining: (A) a first metal complex olefin polymerization catalyst, (B) a second metal complex olefin polymerization catalyst capable of preparing polymers differing in chemical or physical properties from the polymer prepared by catalyst (A) under equivalent polymerization conditions, and (C) a chain shuttling agent.
摘要翻译： 一种用于形成多嵌段共聚物的组合物，所述共聚物中含有两个或更多个化学或物理性质不同的链段或嵌段，使用该多嵌段共聚物的聚合方法和所得聚合物，其中组合物包含混合物或反应产物 由（A）第一金属络合物烯烃聚合催化剂，（B）能够在等效聚合条件下制备由催化剂（A）制备的聚合物在化学或物理性质上不同的聚合物的第二金属络合物烯烃聚合催化剂，以及 （C）链式穿梭剂。
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公开(公告)号：US07893166B2
公开(公告)日：2011-02-22
申请号：US12558234
申请日：2009-09-11
申请人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa Wilson Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , Xiao Hua Qiu , Angela N. Taha
发明人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa Wilson Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , Xiao Hua Qiu , Angela N. Taha
IPC分类号： C08F293/00 , C08F255/00
CPC分类号： C08F212/08
摘要： Embodiments of the invention provide a class of ethylene/α-olefin block interpolymers. The ethylene/α-olefin interpolymers are characterized by an average block index, ABI, which is greater than zero and up to about 1.0 and a molecular weight distribution, Mw/Mn, greater than about 1.3. Preferably, the block index is from about 0.2 to about 1. In addition or alternatively, the block ethylene/α-olefin interpolymer is characterized by having at least one fraction obtained by Temperature Rising Elution Fractionation (“TREF”), wherein the fraction has a block index greater than about 0.3 and up to about 1.0 and the ethylene/α-olefin interpolymer has a molecular weight distribution, Mw/Mn, greater than about 1.3.
摘要翻译： 本发明的实施方案提供一类乙烯/α-烯烃嵌段互聚物。 乙烯/α-烯烃互聚物的特征在于平均嵌段指数ABI，其大于零且高达约1.0，分子量分布Mw / Mn大于约1.3。 优选地，嵌段指数为约0.2至约1.另外或替代地，嵌段乙烯/α-烯烃互聚物的特征在于具有通过升温洗脱分级（“TREF”）获得的至少一个馏分，其中部分具有 大于约0.3且高达约1.0的嵌段指数，并且乙烯/α-烯烃互聚物的分子量分布Mw / Mn大于约1.3。
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6.发明申请公开(公告)号：US20100197880A1
公开(公告)日：2010-08-05
申请号：US12668794
申请日：2008-07-14
申请人： Colin Li Pi Shan , Roger L. Kuhlman , Gary L. Rath , Pamela J. Kenny , Morgan M. Hughes , Rongjuan Cong
发明人： Colin Li Pi Shan , Roger L. Kuhlman , Gary L. Rath , Pamela J. Kenny , Morgan M. Hughes , Rongjuan Cong
IPC分类号： C08F210/02
CPC分类号： C08F210/16 , C08L23/02 , C08L23/08 , C08L23/0807 , C08L2205/02 , C08L2666/06 , C08F210/06 , C08F2500/03 , C08F2500/20 , C08F2500/12
摘要： The invention is related to an ethylene/α-olefin interpolymer having at least a hard segment and at least a soft segment. The soft segment contains a higher amount of comonomers than the hard segment. The hard segment has low crystallinity. The copolymer has a number of unique characteristics disclosed herein.ethylene/α-olefin interpolymers containing low crystallinity hard blocks
摘要翻译： 本发明涉及至少具有硬链段和至少一个软链段的乙烯/α-烯烃互聚物。 软链段含有比硬链段更高量的共聚单体。 硬链段结晶度低。 共聚物具有本文公开的许多独特特征。含有低结晶度硬嵌段的乙烯/α-烯烃互聚物
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公开(公告)号：US07608668B2
公开(公告)日：2009-10-27
申请号：US11376835
申请日：2006-03-15
申请人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa W. Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , Xiahua Qui , Angela N. Taha
发明人： Colin Li Pi Shan , Lonnie G. Hazlitt , Yunwa W. Cheung , Benjamin C. Poon , Phillip D. Hustad , Roger L. Kuhlman , Edmund M. Carnahan , Xiahua Qui , Angela N. Taha
IPC分类号： C08L23/00 , C08L23/04 , C08F210/00 , C08F210/16
CPC分类号： C08F212/08
摘要： Embodiments of the invention provide a class of ethylene/α-olefin block interpolymers. The ethylene/α-olefin interpolymers are characterized by an average block index, ABI, which is greater than zero and up to about 1.0 and a molecular weight distribution, Mw/Mn, greater than about 1.3. Preferably, the block index is from about 0.2 to about 1. In addition or alternatively, the block ethylene/α-olefin interpolymer is characterized by having at least one fraction obtained by Temperature Rising Elution Fractionation (“TREF”), wherein the fraction has a block index greater than about 0.3 and up to about 1.0 and the ethylene/α-olefin interpolymer has a molecular weight distribution, Mw/Mn, greater than about 1.3.
摘要翻译： 本发明的实施方案提供一类乙烯/α-烯烃嵌段互聚物。 乙烯/α-烯烃互聚物的特征在于平均嵌段指数ABI，其大于零且高达约1.0，分子量分布Mw / Mn大于约1.3。 优选地，嵌段指数为约0.2至约1.另外或替代地，嵌段乙烯/α-烯烃互聚物的特征在于具有通过升温洗脱分级（“TREF”）获得的至少一个馏分，其中部分具有 大于约0.3且高达约1.0的嵌段指数，并且乙烯/α-烯烃互聚物的分子量分布Mw / Mn大于约1.3。
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公开(公告)号：US20080166817A1
公开(公告)日：2008-07-10
申请号：US11794417
申请日：2006-01-19
申请人： David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
发明人： David T. Gillespie , Colin Li Pi Shan , Lonnie G. Hazlitt , Alexander W. Degroot , Peter B. Arnoudse , Charles Allen Williams
CPC分类号： G01N30/468 , G01N25/147 , G01N30/463 , G01N30/54 , G01N33/442 , G01N2030/008 , G01N2030/3007
摘要： Apparatus for GPC/TREF and TREF/GPC characterization of a polymer sample. The apparatus provides for the automated and integrated use of multiple TREF columns and a GPC system employing a multiple flow through detectors. In addition, a method for TREF/GPC characterization of a polymer sample by GPC analysis of TREF fractions at increasing TREF elution temperatures from multiple TREF columns operated in a coordinated and synchronized temperature cycle for increased sample throughput. Also, a method for GPC/TREF characterization of a polymer sample by GPC fractionation followed by TREF fractionation of the GPC fractionations.
摘要翻译： 用于GPC / TREF和TREF / GPC表征聚合物样品的装置。 该装置提供了多个TREF柱的自动化和集成使用以及采用多个流过检测器的GPC系统。 此外，通过在增加TREF洗脱温度的TREF洗脱温度下，通过GPC分析TREF级分，通过在协同和同步的温度循环中操作以提高样品通量的多个TREF柱来对聚合物样品进行TREF / GPC表征的方法。 此外，通过GPC分级随后进行GPC分馏的TREF分馏，GPC / TREF表征聚合物样品的方法。
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9.发明授权公开(公告)号：US08476393B2
公开(公告)日：2013-07-02
申请号：US12668794
申请日：2008-07-14
申请人： Colin Li Pi Shan , Roger L. Kuhlman , Gary L. Rath , Pamela J. Kenny , Morgan M. Hughes , Rongjuan Cong
发明人： Colin Li Pi Shan , Roger L. Kuhlman , Gary L. Rath , Pamela J. Kenny , Morgan M. Hughes , Rongjuan Cong
IPC分类号： C08F210/00 , C08F210/02
CPC分类号： C08F210/16 , C08L23/02 , C08L23/08 , C08L23/0807 , C08L2205/02 , C08L2666/06 , C08F210/06 , C08F2500/03 , C08F2500/20 , C08F2500/12
摘要： The invention is related to an ethylene/α-olefin interpolymer having at least a hard segment and at least a soft segment. The soft segment contains a higher amount of comonomers than the hard segment. The hard segment has low crystallinity. The copolymer has a number of unique characteristics disclosed herein. ethylene/α-olefin interpolymers containing low crystallinity hard blocks.
摘要翻译： 本发明涉及至少具有硬链段和至少一个软链段的乙烯/α-烯烃互聚物。 软链段含有比硬链段更高量的共聚单体。 硬链段结晶度低。 共聚物具有本文公开的许多独特特征。 含有低结晶度硬嵌段的乙烯/α-烯烃互聚物。
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10.发明申请Catalyst Composition Comprising Shuttling Agent for Ethylene Multi-Block Copolymer Formation 有权催化剂组合物包含乙烯多嵌段共聚物形成的穿梭剂公开(公告)号：US20130030092A1
公开(公告)日：2013-01-31
申请号：US13562600
申请日：2012-07-31
申请人： Daniel J. Arriola , Edmund M. Carnahan , Yunwa Wilson Cheung , David D. Devore , David D. Graf , Phillip D. Hustad , Roger L. Kuhlman , Colin Li Pi Shan , Benjamin C. Poon , Gordon R. Roof , James C. Stevens , Pamela J. Stirn , Timothy T. Wenzel
发明人： Daniel J. Arriola , Edmund M. Carnahan , Yunwa Wilson Cheung , David D. Devore , David D. Graf , Phillip D. Hustad , Roger L. Kuhlman , Colin Li Pi Shan , Benjamin C. Poon , Gordon R. Roof , James C. Stevens , Pamela J. Stirn , Timothy T. Wenzel
CPC分类号： B32B27/327 , B32B27/06 , B32B27/32 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08F4/65925 , C08F4/65927 , C08F10/00 , C08F10/14 , C08F110/02 , C08F210/14 , C08F210/16 , C08F295/00 , C08F297/00 , C08F297/08 , C08F297/083 , C08F297/086 , C08F2410/01 , C08F2410/04 , C08F2420/02 , C08L23/02 , C08L23/06 , C08L23/0815 , C08L23/0853 , C08L23/10 , C08L53/00 , C08L53/005 , Y10T428/24942 , Y10T428/24992 , Y10T428/2826 , Y10T428/31573 , Y10T428/31587 , C08F2/38 , C08F4/65904 , C08L2666/06 , C08F2500/09 , C08F2500/03 , C08F4/64148 , C08F4/64193 , C08F4/64048 , C08F4/6411 , C08F4/64144 , C08F2500/08 , C08F4/64113 , C08L2666/02 , C08L2666/04 , C08F2500/12 , C08F2500/20 , C08F210/08 , C08F2500/11 , C08F2500/21 , C08F210/02 , C08F212/08 , C08F232/02 , C08F232/08
摘要： A composition for use in forming a multi-block copolymer, said copolymer containing therein two or more segments or blocks differing in chemical or physical properties, a polymerization process using the same, and the resulting polymers, wherein the composition comprises the admixture or reaction product resulting from combining: (A) a first metal complex olefin polymerization catalyst, (B) a second metal complex olefin polymerization catalyst capable of preparing polymers differing in chemical or physical properties from the polymer prepared by catalyst (A) under equivalent polymerization conditions, and (C) a chain shuttling agent.
摘要翻译： 一种用于形成多嵌段共聚物的组合物，所述共聚物中含有两个或更多个化学或物理性质不同的链段或嵌段，使用该多嵌段共聚物的聚合方法和所得聚合物，其中组合物包含混合物或反应产物 由（A）第一金属络合物烯烃聚合催化剂，（B）能够在等效聚合条件下制备由催化剂（A）制备的聚合物在化学或物理性质上不同的聚合物的第二金属络合物烯烃聚合催化剂，以及 （C）链式穿梭剂。
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