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1.发明授权
公开(公告)号：US6075101A
公开(公告)日：2000-06-13
申请号：US802230
申请日：1997-02-19
IPC分类号： B05B1/02 , B01J8/00 , B01J8/24 , B01J10/00 , B01J19/24 , B01J19/26 , B05B7/04 , B05B7/08 , C08F2/01 , C08F2/02 , C08F2/04 , C08F2/34 , C08F10/00 , C08F210/16
CPC分类号： B01J4/002 , B01J19/26 , B01J8/0015 , B01J8/1827 , B05B7/0433 , B05B7/08 , C08F10/00 , C08F210/16
摘要： The use of perpendicular spray nozzles to deliver liquid catalyst to a gas-phase polymerization reactor is taught. Moreover, a method of reducing the amount of gas needed to deliver catalyst is also taught.
摘要翻译： 教导了使用垂直喷嘴将液体催化剂输送到气相聚合反应器。 此外，还教导了减少输送催化剂所需气体量的方法。
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2.发明授权
公开(公告)号：US5962606A
公开(公告)日：1999-10-05
申请号：US802231
申请日：1997-02-19
IPC分类号： B05B1/02 , B01J8/00 , B01J8/24 , B01J10/00 , B01J19/24 , B01J19/26 , B05B7/04 , C08F2/01 , C08F2/34 , C08F10/00 , C08F210/16
CPC分类号： B01J8/1827 , B01J19/26 , B01J8/0015 , B05B7/0433 , C08F10/00 , B01J2208/00672 , B01J2219/00164 , B01J2219/00182 , B01J2219/00186 , B05B7/0466 , C08F210/16 , Y10S526/901 , Y10S526/904 , Y10S526/943
摘要： The present invention teaches the use of an effervescent nozzle to deliver liquid catalyst to a gas phase polymerization system.
摘要翻译： 本发明教导了使用泡腾喷嘴将液体催化剂输送到气相聚合系统。
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3.发明授权Method for feeding a liquid catalyst to a fluidized bed polymerization reactor 失效将液体催化剂送入流化床聚合反应器的方法
公开(公告)号：US5948871A
公开(公告)日：1999-09-07
申请号：US864769
申请日：1997-05-29
IPC分类号： C08F2/00 , B01J8/00 , B01J8/24 , B01J19/26 , C08F2/01 , C08F2/34 , C08F4/44 , C08F4/52 , C08F4/602 , C08F4/64 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F4/72 , C08F10/00 , C08F10/02 , C08F10/06 , C08F32/00 , C08F36/06 , C08F110/06 , C08F210/16
CPC分类号： B01J8/1827 , B01J19/26 , B01J8/004 , C08F10/00 , C08F10/02 , B01J2208/00017 , B01J2208/00539 , B01J2208/00752 , C08F210/16 , C08F4/65912 , C08F4/6592 , Y10S526/901 , Y10S526/943
摘要： For gas phase polymerization reactions in the presence of an unsupported polymerization catalyst, there is provided a process for introducing a liquid catalyst so as to provide a resin particle lean zone such that the average particle size of the resin produced ranges from about 0.01 to about 0.06 inches.
摘要翻译： 对于在无载体聚合催化剂存在下的气相聚合反应，提供了一种引入液体催化剂以提供树脂颗粒贫区的方法，使得所生产的树脂的平均粒度范围为约0.01至约0.06 英寸
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4.发明授权Method for feeding a liquid catalyst to a fluidized bed polymerization reactor 失效将液体催化剂送入流化床聚合反应器的方法
公开(公告)号：US5693727A
公开(公告)日：1997-12-02
申请号：US659764
申请日：1996-06-06
IPC分类号： C08F2/00 , B01J8/00 , B01J8/24 , B01J19/26 , C08F2/01 , C08F2/34 , C08F4/44 , C08F4/52 , C08F4/602 , C08F4/64 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F4/72 , C08F10/00 , C08F10/02 , C08F10/06 , C08F32/00 , C08F36/06 , C08F110/06 , C08F210/16
CPC分类号： B01J8/1827 , B01J19/26 , B01J8/004 , C08F10/00 , C08F10/02 , B01J2208/00017 , B01J2208/00539 , B01J2208/00752 , C08F210/16 , C08F4/65912 , C08F4/6592 , Y10S526/901 , Y10S526/943
摘要： For gas phase polymerization reactions in the presence of an unsupported polymerization catalyst, there is provided a process for introducing a liquid catalyst so as to provide a resin particle lean zone such that the average particle size of the resin produced ranges from about 0.01 to about 0.06 inches.
摘要翻译： 对于在无载体聚合催化剂存在下的气相聚合反应，提供了一种引入液体催化剂以提供树脂颗粒贫区的方法，使得所生产的树脂的平均粒度范围为约0.01至约0.06 英寸
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公开(公告)号：US06211310B1
公开(公告)日：2001-04-03
申请号：US09194988
申请日：1998-12-04
申请人： Mark Gregory Goode , Clark Curtis Williams , Timothy Roger Lynn , Robert Converse Brady, III , Jody Michael Moffett
发明人： Mark Gregory Goode , Clark Curtis Williams , Timothy Roger Lynn , Robert Converse Brady, III , Jody Michael Moffett
IPC分类号： C08F234
CPC分类号： C08F10/00 , B01J8/004 , B01J8/1827 , B01J19/26 , B01J2208/00017 , B01J2208/00539 , B01J2208/00752 , C08F4/65912 , C08F4/6592 , C08F10/02 , C08F210/06 , C08F210/16 , Y10S526/901 , Y10S526/943 , C08F2/34 , C08F4/65927 , C08F210/08 , C08F2500/12 , C08F2500/15 , C08F210/14
摘要： The present invention teaches the use of particular soluble metallocene catalysts to produce stereoregular polymers in gas phase polymerizations wherein the catalysts are fed into a particular lean zone in the reactor. The metallocene catalysts are bridged bis(substituted indenyl) compounds.
摘要翻译： 本发明教导了使用特定的可溶性茂金属催化剂在气相聚合中产生立体规则聚合物，其中将催化剂进料到反应器中的特定贫区中。 茂金属催化剂是桥连双（取代茚基）化合物。
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公开(公告)号：US5912202A
公开(公告)日：1999-06-15
申请号：US781196
申请日：1997-01-10
申请人： John Henry Oskam , Thomas Henry Peterson , David James Schreck , Purna Chand Sishta , Timothy Todd Wenzel , Gregory Todd Whiteker , Clark Curtis Williams
发明人： John Henry Oskam , Thomas Henry Peterson , David James Schreck , Purna Chand Sishta , Timothy Todd Wenzel , Gregory Todd Whiteker , Clark Curtis Williams
IPC分类号： C08F4/651 , C08F4/609 , C08F4/64 , C08F4/6592 , C08F10/00 , C08F210/16
CPC分类号： C08F10/00 , C08F210/16 , C08F4/6592 , C08F4/65922 , Y10S526/943
摘要： A method for preparing an activated catalyst composition comprising a single site catalyst precursor and an activating cocatalyst, which comprises contacting outside of a polymerization reactor a single site catalyst precursor with an activating cocatalyst before, during, or after contacting the single site catalyst precursor with a weakly coordinating electron donor such as 1-hexene.
摘要翻译： 一种制备包含单中心催化剂前体和活化助催化剂的活化催化剂组合物的方法，其包括在将单一位点催化剂前体与一个位点催化剂前体接触之前，期间或之后与聚合反应器的外部接触一单位催化剂前体与活化助催化剂 弱配位电子给体如1-己烯。
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公开(公告)号：US06365695B1
公开(公告)日：2002-04-02
申请号：US09547265
申请日：2000-04-11
IPC分类号： C08F11002
CPC分类号： C08F10/00 , B01J8/0035 , B01J8/1809 , B01J8/20 , B01J8/40 , B01J19/26 , Y10S526/901 , Y10S526/914 , Y10S526/919 , C08F2/34 , C08F2/01
摘要： Liquid catalyst composition is fed to a fluidized bed olefin polymerization reactor through an ultrasonic nozzle, enabling improved control over average catalyst composition droplet size and size distribution, which provides better control over resin particle size. The spray may be surrounded by a shroud of gas which creates a particle lean zone, thus reducing the likelihood of contact by the catalyst composition with existing product particles already suspended in the fluid bed.
摘要翻译： 液体催化剂组合物通过超声波喷嘴进料到流化床烯烃聚合反应器中，从而能够改进对平均催化剂组成的液滴尺寸和尺寸分布的控制，从而提供对树脂粒度的更好控制。 喷雾可以由产生贫灰区的气体罩包围，从而减少催化剂组合物与已经悬浮在流化床中的现有产品颗粒接触的可能性。
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公开(公告)号：US6150478A
公开(公告)日：2000-11-21
申请号：US325823
申请日：1999-06-04
IPC分类号： C08F2/00 , B01J8/00 , B01J8/18 , B01J8/20 , B01J8/40 , B01J19/26 , C08F2/34 , C08F10/00 , C08F10/02
CPC分类号： C08F10/00 , B01J19/26 , B01J8/0035 , B01J8/1809 , B01J8/20 , B01J8/40 , Y10S526/901 , Y10S526/914 , Y10S526/919
摘要： Liquid catalyst composition is fed to a fluidized bed olefin polymerization reactor through an ultrasonic nozzle, enabling improved control over average catalyst composition droplet size and size distribution, which provides better control over resin particle size. The spray may be surrounded by a shroud of gas which creates a particle lean zone, thus reducing the likelihood of contact by the catalyst composition with existing product particles already suspended in the fluid bed.
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公开(公告)号：US6111034A
公开(公告)日：2000-08-29
申请号：US224036
申请日：1998-12-31
申请人： Mark Gregory Goode , Clark Curtis Williams , Fathi David Hussein , Thomas James McNeil , Kiu Hee Lee
发明人： Mark Gregory Goode , Clark Curtis Williams , Fathi David Hussein , Thomas James McNeil , Kiu Hee Lee
IPC分类号： C08F2/01 , C08F4/659 , C08F4/6592 , C08F10/00
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F4/65922 , Y10S526/901 , Y10S526/943
摘要： Addition of water to a gas phase olefin polymerization reactor in amounts greater than 3 ppmv permits an increase in the level of condensable gas and facilitates operation of the reactor at an elevated dew point by ameliorating electrostatic phenomena in the reactor; the process inhibits sheeting.
摘要翻译： 以大于3ppmv的量向气相烯烃聚合反应器中加入水可以提高可冷凝气体的水平，并且通过改善反应器中的静电现象便于反应器在升高的露点下操作; 该过程抑制片材。
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公开(公告)号：US5744556A
公开(公告)日：1998-04-28
申请号：US712930
申请日：1996-09-13
申请人： George Ernest Keller , Keith Ernest Carmichael , Jean Bowman Cropley , Eldon Ronald Larsen , Arakalud Venkatapathia Ramamurthy , Mark Wilton Smale , Timothy Todd Wenzel , Clark Curtis Williams
发明人： George Ernest Keller , Keith Ernest Carmichael , Jean Bowman Cropley , Eldon Ronald Larsen , Arakalud Venkatapathia Ramamurthy , Mark Wilton Smale , Timothy Todd Wenzel , Clark Curtis Williams
IPC分类号： C08F2/34 , B01J20060101 , C08F20060101 , C08F4/00 , C08F4/602 , C08F4/619 , C08F4/642 , C08F4/6592 , C08F10/00 , C08F36/06 , C08F210/16 , C08G20060101
CPC分类号： C08F10/00 , C08F210/16 , C08F4/619 , Y10S526/901 , Y10S526/943
摘要： A process for the gas-phase polymerization of polymers which allows for the introduction of an unsupported polymerization catalyst system into the gas-phase reactor, wherein the unsupported polymerization catalyst system comprises (i) a non-volatile materials fraction containing a polymerization catalyst; (ii) a solvent fraction which is at least partially miscible with the non-volatile materials fraction and which is sufficiently volatile to allow for the formation of polymerization catalyst particles when the mixture of the solvent fraction and the non-volatile materials fraction is sprayed into the reactor; (iii) a compressed fluid; and (iv) optionally a slowly vaporizing solvent.
摘要翻译： 一种聚合物的气相聚合方法，其允许在气相反应器中引入无载体的聚合催化剂体系，其中所述未负载的聚合催化剂体系包含（i）含有聚合催化剂的非挥发性物质部分; （ii）溶剂级分，其与非挥发性物质馏分至少部分混溶，并且当将溶剂馏分和非挥发性物质馏分的混合物喷入时，其挥发性足以形成聚合催化剂颗粒 反应堆; （iii）压缩流体; 和（iv）任选地缓慢蒸发的溶剂。
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