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61.发明申请公开(公告)号：US20140353216A1
公开(公告)日：2014-12-04
申请号：US14365739
申请日：2012-12-14
申请人： SIME S.R.L.
发明人： Luciano Scibola , Stefano Favilli
IPC分类号： C10G7/08
CPC分类号： C10G7/08 , B01D3/141 , B01D3/40 , C07C7/08 , C10G2300/1096 , C10G2300/203 , C10G2300/4056 , C10G2400/02 , C10G2400/30 , C07C15/00
摘要： A column for consecutive extractive distillations, in particular of crude hydrocarbon mixes comprising aromatic, naphthene and paraffin hydrocarbons. The invention also relates to methods for separating and recovering the components of a crude hydrocarbon mix comprising aromatic, naphthene and paraffin hydrocarbons by consecutive extractive distillations provided by means of the column for consecutive extractive distillations, to which the invention also relates.
摘要翻译： 用于连续萃取蒸馏的塔，特别是包含芳烃，环烷烃和链烷烃的粗烃混合物。 本发明还涉及通过本发明还涉及的用于连续萃取蒸馏的塔提供的连续萃取馏出物来分离和回收包含芳烃，环烷烃和链烷烃的粗烃混合物的组分的方法。
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公开(公告)号：US08840854B2
公开(公告)日：2014-09-23
申请号：US13971977
申请日：2013-08-21
申请人： UOP LLC
CPC分类号： B01D3/009 , B01J8/00 , C10G7/08 , C10G45/02 , C10G45/32 , C10G45/44 , C10G47/00 , C10G47/04 , C10G47/14 , C10G47/16 , C10G65/12 , C10G69/02 , C10G2400/04 , C10G2400/30
摘要： An apparatus is disclosed for hydrocracking hydrocarbon feed in a hydrocracking unit and hydrotreating a diesel product from the hydrocracking unit in a hydrotreating unit. The hydrocracking unit and the hydrotreating unit shares the same recycle gas compressor. A warm separator separates recycle gas and hydrocarbons from diesel in the hydrotreating effluent, so fraction of the diesel is relatively simple. The warm separator also keeps the diesel product separate from the more sulfurous diesel in the hydrocracking effluent, and still retains heat needed for fractionation of lighter components from the low sulfur diesel product.
摘要翻译： 公开了一种用于在加氢裂化装置中加氢裂化烃进料并在加氢处理装置中从加氢裂化装置加氢处理柴油产品的装置。 加氢裂化装置和加氢处理装置共享相同的循环气体压缩机。 热分离器在加氢处理流出物中将循环气体和碳氢化合物与柴油分离，因此柴油馏分比较简单。 暖型分离器还使柴油机与加氢裂化废液中的更多的亚硫酸柴油分离，并且仍然保留了从低硫柴油产品中分馏较轻组分所需的热量。
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公开(公告)号：US20130225838A1
公开(公告)日：2013-08-29
申请号：US13707554
申请日：2012-12-06
发明人： Fu-Ming Lee , Tzong-Bin Lin , Kuang-Yeu Wu , Jyh-Haur Hwang , Jeffrey Tsung-Min Chiu , Jeng-Cheng Lee , Yu-Ming Wu , Han-Tjen Jan
IPC分类号： C07D333/48
CPC分类号： C07D333/48 , B01D3/40 , B01D11/0484 , B01D11/0488 , C07C7/08 , C07C7/10 , C10G7/08 , C10G21/16 , C10G21/27 , C10G21/28 , C10G2300/44 , C07C15/02
摘要： Recovering a polar hydrocarbon (HC) selective solvent substantially free of hydrocarbons (HCs) and other impurities from a lean solvent stream containing the selective solvent, measurable amounts of heavy aromatic HCs, and polymeric materials that are generated in an extractive distillation (ED) or liquid-liquid extraction (LLE) process. At least a portion of the lean solvent stream is contact in a solvent clean-up zone with a slip stream from the HC feed stream of the ED or LLE process or an external stream. The HC feed stream, such as pyrolysis gasoline or reformate, contains significant amounts of benzene and at least 50% polar (aromatic) HCs and serves as a displacement agent to remove the heavy HCs and polymeric material from the lean solvent stream. A magnetic filter can be used to remove the paramagnetic contaminants from the lean solvent.
摘要翻译： 从含有选择性溶剂的贫溶剂流中回收基本上不含烃（HC）和其他杂质的极性烃（HC）选择性溶剂，可测量的重芳烃HC和在萃取蒸馏（ED）中产生的聚合材料） 液 - 液萃取（LLE）方法。 贫溶剂流的至少一部分在溶剂清洁区中与来自ED或LLE方法的HC进料流的滑流或外部流接触。 HC进料流，如热解汽油或重整油，含有大量的苯和至少50％的极性（芳香族）HC，并且用作从稀溶剂流中除去重的HC和聚合物材料的置换剂。 磁性过滤器可用于从贫溶剂中除去顺磁性污染物。
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公开(公告)号：US08237004B2
公开(公告)日：2012-08-07
申请号：US12650816
申请日：2009-12-31
CPC分类号： C10G7/00 , C10G7/08 , C10G29/205 , C10G45/60 , C10G50/00 , C10G57/00 , C10G57/005 , C10G57/02 , C10G2300/305 , C10G2300/4081 , C10G2400/02
摘要： A process for making products with low hydrogen halide, comprising: a) stripping or distilling an effluent from a reactor into a first fraction having an amount of hydrogen halide, and a second fraction having a reduced amount of hydrogen halide; wherein the reactor comprises: an ionic liquid catalyst having a metal halide, and a hydrogen halide or an organic halide; and b) recovering one or more product streams, from the second fraction, having less than 25 wppm hydrogen halide. In one embodiment the ionic liquid catalyst has metal halide; and the recovering recovers propane, n-butane, and alkylate gasoline having less than 25 wppm hydrogen halide. In another embodiment the recovering uses a distillation column having poor corrosion resistance to hydrogen halide; and the distillation column does not exhibit corrosion. There is also provided an alkylate gasoline having less than 5 wppm hydrogen halide, a high RON, and low RVP.
摘要翻译： 一种制备具有低卤化氢的产物的方法，包括：a）将反应器的流出物汽提或蒸馏成具有一定量卤化氢的第一级分，和具有减少量的卤化氢的第二级分; 其中所述反应器包括：具有金属卤化物的离子液体催化剂和卤化氢或有机卤化物; 和b）从具有小于25wppm卤化氢的第二级分回收一种或多种产物流。 在一个实施方案中，离子液体催化剂具有金属卤化物; 并且回收回收具有小于25wppm卤化氢的丙烷，正丁烷和烷基化汽油。 在另一个实施方案中，回收使用对卤化氢具有差的耐腐蚀性的蒸馏塔; 并且蒸馏塔不显示腐蚀。 还提供了具有小于5wppm卤化氢，高RON和低RVP的烷基化汽油。
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公开(公告)号：US20110155632A1
公开(公告)日：2011-06-30
申请号：US12650816
申请日：2009-12-31
CPC分类号： C10G7/00 , C10G7/08 , C10G29/205 , C10G45/60 , C10G50/00 , C10G57/00 , C10G57/005 , C10G57/02 , C10G2300/305 , C10G2300/4081 , C10G2400/02
摘要： A process for making products with low hydrogen halide, comprising: a) stripping or distilling an effluent from a reactor into a first fraction having an amount of hydrogen halide, and a second fraction having a reduced amount of hydrogen halide; wherein the reactor comprises: an ionic liquid catalyst having a metal halide, and a hydrogen halide or an organic halide; and b) recovering one or more product streams, from the second fraction, having less than 25 wppm hydrogen halide. In one embodiment the ionic liquid catalyst has metal halide; and the recovering recovers propane, n-butane, and alkylate gasoline having less than 25 wppm hydrogen halide. In another embodiment the recovering uses a distillation column having poor corrosion resistance to hydrogen halide; and the distillation column does not exhibit corrosion. There is also provided an alkylate gasoline having less than 5 wppm hydrogen halide, a high RON, and low RVP.
摘要翻译： 一种制备具有低卤化氢的产物的方法，包括：a）将反应器的流出物汽提或蒸馏成具有一定量卤化氢的第一级分，和具有减少量的卤化氢的第二级分; 其中所述反应器包括：具有金属卤化物的离子液体催化剂和卤化氢或有机卤化物; 和b）从具有小于25wppm卤化氢的第二级分回收一种或多种产物流。 在一个实施方案中，离子液体催化剂具有金属卤化物; 并且回收回收具有小于25wppm卤化氢的丙烷，正丁烷和烷基化汽油。 在另一个实施方案中，回收使用对卤化氢具有差的耐腐蚀性的蒸馏塔; 并且蒸馏塔不显示腐蚀。 还提供了具有小于5wppm卤化氢，高RON和低RVP的烷基化汽油。
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公开(公告)号：US20090306450A1
公开(公告)日：2009-12-10
申请号：US12157300
申请日：2008-06-09
IPC分类号： C07C7/00
摘要： A method for reducing corrosion in a diolefin extractive distillation process comprising preventing the formation of ammonium carbonate by promoting the formation of a carbonate salt that does not dissociate in the ammonium carbonate dissociation temperature range of that extractive distillation process.
摘要翻译： 一种用于减少二烯萃取蒸馏方法中的腐蚀的方法，包括通过促进在该萃取蒸馏过程的碳酸铵解离温度范围内不解离的碳酸盐的形成来防止形成碳酸铵。
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公开(公告)号：US07563360B2
公开(公告)日：2009-07-21
申请号：US11043751
申请日：2005-01-26
CPC分类号： C10G31/00 , C10G7/00 , C10G7/08 , C10G2300/205
摘要： A top temperature T1 of a distillation tower 1 is held below a liquefying temperature of a light fraction by returning a part of an exhaust gas W, which is cooled by a condenser 5, to the upper zone of the distillation tower 1. A bottom temperature T2 is raised up to 300° C. at highest by returning a part of a liquid product P from a re-boiler 3 to a lower zone of the distillation tower 1. When a liquid hydrocarbon L comes in countercurrent contact with a stripping gas G inside the distillation tower 1 with the temperature profile that an inner temperature gradually falls down along an upward direction, mercury is efficiently transferred from the liquid L to a vapor phase without effusion of the light fraction in accompaniment with the exhaust gas W.
摘要翻译： 通过将由冷凝器5冷却的一部分废气W返回到蒸馏塔1的上部区域，蒸馏塔1的顶部温度T1保持在轻馏分的液化温度以下。底部温度 通过将液体产物P的一部分从再沸器3返回到蒸馏塔1的下部区域，将T2升高到最高300℃。当液体烃L与汽提气体G逆流接触时 在内部温度沿着向上的方向逐渐下降的温度分布的蒸馏塔1内部，水银从液体L有效地传递到汽相，而不伴随废气瓦斯W的轻馏分。
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68.发明授权公开(公告)号：US06679975B2
公开(公告)日：2004-01-20
申请号：US10036416
申请日：2002-01-07
申请人： Géraldine Laborie , Fabrice Lecomte , Annick Pucci
发明人： Géraldine Laborie , Fabrice Lecomte , Annick Pucci
IPC分类号： B01D336
摘要： The present invention aims to isolate the azeotropes formed in a distillation column (B1) by methanol, propane and butane. The azeotropes are then liquefied in heat exchanger (E2) and mixed in contactor (M1) with water in order to dissolve the methanol in water. The mixture is then fed into a decantation tank (D2) to separate the aqueous phase from the liquid hydrocarbon phase. Finally, an aqueous phase containing methanol is discharged and the methanol-depleted hydrocarbon phase is recycled to distillation column (B1) as reflux.
摘要翻译： 本发明的目的是通过甲醇，丙烷和丁烷来分离在蒸馏塔（B1）中形成的共沸物。 然后将共沸物在热交换器（E2）中液化，并在接触器（M1）中与水混合，以便将甲醇溶解在水中。 然后将混合物进料到倾析罐（D2）中以将水相与液态烃相分离。 最后，排出含有甲醇的水相，将甲醇耗尽的烃相作为回流再循环至蒸馏塔（B1）。
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69.发明授权公开(公告)号：US06413378B1
公开(公告)日：2002-07-02
申请号：US09647789
申请日：2000-10-05
IPC分类号： B01D340
CPC分类号： C10G7/12 , B01D3/40 , B01D3/4244 , C07C7/08 , C10G7/08 , Y10S203/19 , Y10S208/01 , Y10S585/956
摘要： An extractive distillation tower 4 supplied with a feedstock containing butadiene and a solvent and for distilling the feedstock to separate and purify the butadiene. The tower 4 includes sensors 32, 34 for detecting concentrations of specific impurities other than butadiene; a sensor for detecting a concentration of the butadiene; a sensor 30 for detecting a differential pressure between the top and bottom of the tower 4; a valve 48 for controlling the flow rate of part of fluid taken out from a bottom of the tower 4 and returned to the tower 4; a valve 23 for controlling a ratio of a solvent fed to the tower 4; a reflux ratio valve 28 for controlling the flow rate of part of remaining component of the feedstock taken out from a top of the tower 4 and refluxed; a heater 36 for controlling a bottom temperature of the tower 4; and a predictive control 60 for calculating forecasted values of the concentrations of the specific impurity and the butadiene after a time based on these sensors and controlling the system based on the forecasted values.
摘要翻译： 提供含有丁二烯和溶剂的原料并用于蒸馏原料以分离和纯化丁二烯的萃取蒸馏塔4。 塔4包括用于检测除丁二烯以外的特定杂质的浓度的传感器32,34; 用于检测丁二烯浓度的传感器; 用于检测塔架4的顶部和底部之间的差压的传感器30; 用于控制从塔架4的底部取出并返回到塔架4的部分流体的流量的阀门48; 用于控制供给到塔架4的溶剂的比例的阀23; 用于控制从塔4的顶部取出的原料的剩余成分的一部分的流量并回流的回流比阀28; 用于控制塔架4的底部温度的加热器36; 以及用于基于这些传感器计算一段时间后特定杂质和丁二烯的浓度的预测值的预测控制器60，并且基于预测值来控制系统。
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70.发明授权公开(公告)号：US06358402B1
公开(公告)日：2002-03-19
申请号：US09473463
申请日：1999-12-28
申请人： Robert C. Schucker
发明人： Robert C. Schucker
IPC分类号： C10G2920
CPC分类号： C10G7/08
摘要： A method for separating sulfur species from hydrocarbon streams, particularly cracked naphtha streams, using extractive distillation. The method effectively separates sulfur species from cracked naphtha streams without substantially lowering the olefin content.
摘要翻译： 使用萃取蒸馏从烃流，特别是裂解石脑油流中分离硫物质的方法。 该方法有效地将硫物质与裂解的石脑油流分离，而不会显着降低烯烃含量。
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