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    Preparation of ethylene polymers by the high-pressure method
    33.
    发明申请
    Preparation of ethylene polymers by the high-pressure method 失效
    通过高压法制备乙烯聚合物

    公开(公告)号：US20040210016A1

    公开(公告)日：2004-10-21

    申请号：US10845396

    申请日：2004-05-14

    Applicant: BASF Aktiengesellschaft

    Inventor： Lars Wittkowski ,  Andreas Deckers ,  Wilhelm Weber ,  Thomas Droge ,  Andrei Gonioukh ,  Frank-Olaf Mahling

    IPC: C08F002/00

    CPC classification number: A61Q1/06 ,  A61K8/8111 ,  A61Q1/02 ,  A61Q1/10 ,  C08F10/02 ,  C08F110/02 ,  C08K5/07 ,  C08K5/14 ,  Y10S585/946 ,  C08F4/36 ,  C08F2/00

    Abstract: A process for preparing ethylene polymers by the high-pressure method comprises dissolving one or more free-radical initiators in one or more ketones of the formula I 1 where R1 and R2 are identical or different and are selected from among C1-C6-alkyl and C3-C12-cycloalkyl and R1 and R2 may also be covalently linked to one another to form a 4- to 13-membered ring, prior to the polymerization, compressing the solution, metering it into the polymerization reactor at one or more points and subsequently carrying out the polymerization at from 150 to 380null C. and from 500 to 4500 bar.

    Abstract translation: 通过高压法制备乙烯聚合物的方法包括将一种或多种自由基引发剂溶解在式I中的一种或多种酮中，其中R 1和R 2相同或不同，并且选自C1 -C6-烷基和C3-C12-环烷基，并且R 1和R 2也可以彼此共价连接以形成4-至13-元环，在聚合之前，将溶液压缩，计量 在一个或多个点进入聚合反应器，随后在150至380℃和500至4500巴下进行聚合。

    Process for the preparation of polyolefin waxes
    35.
    发明授权
    Process for the preparation of polyolefin waxes 失效
    制备聚烯烃蜡的方法

    公开(公告)号：US5750813A

    公开(公告)日：1998-05-12

    申请号：US353144

    申请日：1994-12-09

    Applicant: Reiner Hess ,  Hartmut Voigt ,  Hans-Friedrich Herrmann ,  Ludwig Bohm ,  Walter Spaleck ,  Gerd Hohner

    Inventor： Reiner Hess ,  Hartmut Voigt ,  Hans-Friedrich Herrmann ,  Ludwig Bohm ,  Walter Spaleck ,  Gerd Hohner

    IPC: B01J19/00 ,  B01J19/18 ,  C08F4/62 ,  C08F4/659 ,  C08F10/00 ,  C08F110/06 ,  C10L1/16

    CPC classification number: C08F10/00 ,  B01J19/0013 ,  B01J19/1881 ,  B01J2219/00128 ,  C08F110/06 ,  C08F4/65912 ,  Y10S585/946

    Abstract: A process for the preparation of a polyolefin wax by polymerization or copolymerization of olefins or diolefins in suspension and in the presence of a catalyst. The process utilizes a metallocene and a cocatalyst, wherein the metallocene is a compound of the formula I ##STR1## in which M.sup.1 is a metal of group IVb, Vb or VIb of the Periodic Table of Elements, R.sup.1 and R.sup.2 are identical or different and are a hydrogen atom, a C.sub.1 -C.sub.10 -alkyl group, a C.sub.1 -C.sub.10 -alkoxy group, a C.sub.6 -C.sub.10 -aryl group, a C.sub.6 -C.sub.10 -aryloxy group, a C.sub.2 -C.sub.10 -alkenyl group, a C.sub.7 -C.sub.40 -arylalkyl group, a C.sub.7 -C.sub.40 -alkylaryl group, a C.sub.8 -C.sub.40 -arylalkenyl group or a halogen atom and R.sup.3 and R.sup.4 are identical or different and are a mononuclear or polynuclear hydrocarbon radical which may form a sandwich structure with the central atom M.sup.1, low-boiling hydrocarbons having 3 or 4 carbon atoms or low-boiling halogenated hydrocarbons are used as suspending agents and the heat of reaction is removed by evaporative cooling.

    Abstract translation: 一种通过在悬浮液中和在催化剂存在下聚合或共聚烯烃或二烯烃来制备聚烯烃蜡的方法。 该方法使用金属茂和助催化剂，其中茂金属是式I的化合物（Ⅰ），其中M1是元素周期表IVb族，Vb或VIb族的金属，R1和R2是相同的 或不同，为氢原子，C1-C10-烷基，C1-C10-烷氧基，C6-C10-芳基，C6-C10-芳氧基，C2-C10-烯基，C7 -C 40 - 芳基烷基，C 7 -C 40 - 烷基芳基，C 8 -C 40 - 芳基烯基或卤素原子，R 3和R 4相同或不同，并且是单核或多核烃基，其可形成具有中心 使用原子M1，具有3或4个碳原子的低沸点烃或低沸点卤代烃作为悬浮剂，通过蒸发冷却除去反应热。

    Method of hydroisomerizing paraffins emanating from the Fischer-Tropsch process using catalysts based on H-Y zeolite
    37.
    发明授权
    Method of hydroisomerizing paraffins emanating from the Fischer-Tropsch process using catalysts based on H-Y zeolite 失效
    使用基于H-Y沸石的催化剂从费 - 托方法发出的烷烃加氢异构化方法

    公开(公告)号：US5306860A

    公开(公告)日：1994-04-26

    申请号：US886224

    申请日：1992-05-21

    Applicant: Pierre-Henri Bigeard ,  Alain Billon ,  Pierre Dufresne ,  Samuel Mignard

    Inventor： Pierre-Henri Bigeard ,  Alain Billon ,  Pierre Dufresne ,  Samuel Mignard

    IPC: C10G65/04 ,  C07C5/13 ,  C07C5/22

    CPC classification number: C10G65/043 ,  Y10S208/95 ,  Y10S585/946

    Abstract: For Hydroisomerizering charges emanating from the Fischer-Tropsch process:a) hydrogen is reacted with the charge in contact with a catalyst 1 in a first reaction zone, the catalyst 1 comprising at least one alumina-based matrix and at least one hydro-dehydrogenation component andb) the effluent from the first reaction zone is put into contact with a catalyst 2 in a second reaction zone, the catalyst 2 comprising:20 to 97% by weight of at least one matrix,3 to 80% by weight of at least one Y zeolite in hydrogen form, the zeolite being characterized by an SiO.sub.2 /Al.sub.2 O.sub.3 molar ratio of over 4.5; a sodium content of less than 1% by weight determined at 1100.degree. C. under calcining conditions; an a.sub.o crystal parameter of the elemental mesh of less than 24.70.times.10.sup.-10 m; and a specific surface area determined by the BET method of over 400 m.sup.2.g.sup.-1, andat least one hydro-dehydrogenation component.

    Abstract translation: 对于从费 - 托方法产生的加氢异构化电荷：a）氢与在第一反应区中与催化剂1接触的电荷反应，催化剂1包含至少一种基于氧化铝的基体和至少一个氢脱氢组分 和b）来自第一反应区的流出物与第二反应区中的催化剂2接触，催化剂2包含：至少一种基质20至97重量％，至少3至80重量％ 一种Y型沸石为氢形式，沸石的特征在于SiO 2 / Al 2 O 3摩尔比超过4.5; 在1100℃下在煅烧条件下测定的钠含量小于1重量％ 元素网的ao晶体参数小于24.70×10-10 m; 并且通过BET法测定的比表面积超过400m 2·g -1，和至少一种加氢脱氢组分。

    Conversion of light hydrocarbons to higher hydrocarbons
    38.
    发明授权
    Conversion of light hydrocarbons to higher hydrocarbons 失效
    轻烃转化成高级烃

    公开(公告)号：US5157189A

    公开(公告)日：1992-10-20

    申请号：US616584

    申请日：1990-11-21

    Applicant: Sankaram B. Karra

    Inventor： Sankaram B. Karra

    IPC: C01B3/38 ,  C07C2/84

    CPC classification number: C07C2/84 ,  C01B3/386 ,  C01B2203/0261 ,  C01B2203/1041 ,  C01B2203/1241 ,  C07C2527/06 ,  C07C2527/08 ,  Y02P20/582 ,  Y10S585/946

    Abstract: A process is disclosed for catalytically converting light hydrocarbons, such as natural gas, to saturated or unsaturated higher molecular weight hydrocarbons, such as ethylene, propylene, ethyl benzene, and styrene. The process employs gaseous catalyst or a mixture of catalysts selected from hydrogen sulfide, hydrogen halides other then hydrogen fluoride, halogen other than fluorine, sulfur vapor, and/or sulfur containing hydrocarbons.

    Abstract translation: 公开了一种将轻质烃如天然气催化转化成饱和或不饱和的较高分子量烃如乙烯，丙烯，乙苯和苯乙烯的方法。 该方法使用气态催化剂或选自硫化氢，除氟化氢之外的卤化氢，氟以外的卤素，硫蒸气和/或含硫烃的催化剂混合物。

    Fabrication of atactic waxes of polyolefin
    39.
    发明授权
    Fabrication of atactic waxes of polyolefin 失效
    聚烯烃无规立构蜡的制造

    公开(公告)号：US3933934A

    公开(公告)日：1976-01-20

    申请号：US324898

    申请日：1973-01-18

    Applicant: Jean Claude Bailly ,  Daniel Durand ,  Pierre Mangin

    Inventor： Jean Claude Bailly ,  Daniel Durand ,  Pierre Mangin

    IPC: C08F4/00 ,  C08F4/60 ,  C08F4/6192 ,  C08F4/64 ,  C08F8/00 ,  C08F10/00 ,  C08F10/06 ,  C08F210/00 ,  C09G1/00 ,  C07C3/21

    CPC classification number: C08F10/06 ,  Y10S585/946

    Abstract: Atactic waxes and method for preparing same by polymerization of polyolefin alone or in combination with other monoolefins of the formula CH.sub.2 = CHR in which R is hydrogen or an alkyl radical having from 2 to 8 carbon atoms in which the polymerization is carried out at low pressure and in a hydrocarbon solvent in the presence of a catalyst formed of the product of the reaction of magnesium or a compound thereof, a compound of a transition metal selected from the sub-groups IVa, Va and VIa of the periodic classification of elements and an alkyl halide, and a co-catalyst in the form of an organometallic compound of a metal selected of groups II and III of the periodic classification of elements.

    Abstract translation: 无规立构蜡及其制备方法，其聚烯烃单独或与式CH 2 = CHR的其它单烯烃聚合，其中R是氢或具有2-8个碳原子的烷基，其中聚合在低压下进行 在烃溶剂中，在由镁或其化合物的反应产物形成的催化剂存在下，选自元素周期分类的IVa，Va和VIa族的过渡金属化合物和 烷基卤和选自元素周期分类的II和III族金属的有机金属化合物形式的助催化剂。

    Production of low molecular weight waxy polyethylenes
    40.
    发明授权
    Production of low molecular weight waxy polyethylenes 失效
    生产低分子量的聚苯乙烯

    公开(公告)号：US3835107A

    公开(公告)日：1974-09-10

    申请号：US29167172

    申请日：1972-09-25

    Applicant: BASF AG

    Inventor： URBAN F ,  PFANNMUELLER H ,  STARK K ,  GROPPER H

    IPC: C08F10/00 ,  C08F1/60 ,  C08F3/04

    CPC classification number: C08F10/00 ,  Y10S585/942 ,  Y10S585/946 ,  C08F4/28

    Abstract: A PROCESS FOR THE PRODUCTION OF WAXY, LOW MOLECULAR WEIGHT POLYETHYLENES IN WHICH ETHYLENE IS POLYMERIZED UNDER THE ACTION OF A POLYMERIZATION INITIATOR WHICH FORMS FREE RADICALS AND IN THE PRESENCE OF A POLYMERIZATION REGULATOR AT ELEVATED TEMPERATURE AND AT SUPERATMOSPHERIC PRESSURE. IT IS A CHARACTERISTIC OF THE PROCESS ACCORDING TO THE INVENTION THAT AS THE FREE RADICAL-FORMING POLYMERIZATION INITIATOR THERE ARE JOINTLY USED: (1) A SPECIFIC AMOUNT OF AN ORGANIC PEROXIDE HAVING A HALF-LIFE TEMPERATURE OF FROM 60* TO 112*C., AND (2) A SPECIFIC AMOUNT OF OXYGEN. HIGH YIELDS CAN BE OBTAINED BY THE PROCESS AND A PRODUCT CAN BE OBTAINED WHICH HAS PARTICULARLY GOOD OIL-BINDING PROPERTIES.

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