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公开(公告)号：US20100193347A1
公开(公告)日：2010-08-05
申请号：US12696613
申请日：2010-01-29
IPC分类号： B01D3/36
CPC分类号： B01D11/0426 , B01D11/0492
摘要： Processes for the preparation and purification of hydrofluoroolefins such as tetrafluorinated propenes. A process is provided for separating a first hydrofluoroolefin from a second hydrofluoroolefin by a) providing a mixture comprising a first hydrofluoroolefin and a second hydrofluoroolefin, which first hydrofluoroolefin is preferentially more reactive with an amine than the second hydrofluoroolefin; b) adding a sufficient amount of an amine to the mixture to form a combination comprising the second hydrofluoroolefin and a reaction product of the first hydrofluoroolefin and the amine; and then c) separating the reaction product from the combination. This is particularly useful for removing 1,2,3,3,3-pentafluoropropene (HFO-1225ye) impurities from the hydrofluoroolefin 2,3,3,3-tetrafluoropropene (HFO-1234yf). HFO-1234yf is a refrigerant with low global warming potential.
摘要翻译： 用于制备和纯化氢氟烯烃如四氟化丙烯的方法。 提供了一种通过以下方法提供第一氢氟烯烃与第二氢氟烯烃的分离：a）提供包含第一氢氟烯烃和第二氢氟烯烃的混合物，该第一氢氟烯烃优选比第二氢氟烯烃更能反应胺; b）向混合物中加入足量的胺以形成包含第二氢氟烯烃和第一氢氟烯烃与胺的反应产物的组合; 然后c）将反应产物与组合物分离。 这对于从氢氟烯烃2,3,3,3-四氟丙烯（HFO-1234yf）中除去1,2,3,3,3-五氟丙烯（HFO-1225ye）杂质是特别有用的。 HFO-1234yf是一种全球变暖潜力较低的制冷剂。
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公开(公告)号：US20110252694A1
公开(公告)日：2011-10-20
申请号：US12762801
申请日：2010-04-19
CPC分类号： A01N29/00 , A01N25/04 , A01N2300/00
摘要： Soil fumigation compositions are provided herein that include methyl iodide, at least one fluorocarbon or hydrofluorocarbon, at least one surfactant, and water. The fumigant can be produced by combining the water and surfactant with an initial mixture that is an azeotropic or azeotrope-like mixture of methyl iodide and at least one fluorocarbon or hydrofluorocarbon. The fumigant compositions can be utilized in drip fumigation processes, and have increased volatility as compared to methyl iodide alone, which can reduce the risk of water contamination when utilizing methyl iodide as a fumigant.
摘要翻译： 本文提供了包括甲基碘，至少一种碳氟化合物或氢氟烃，至少一种表面活性剂和水的土壤熏蒸组合物。 熏蒸剂可以通过将水和表面活性剂与初始混合物（其是甲基碘和至少一种碳氟化合物或氢氟烃的共沸或类共沸混合物）混合来制备。 熏蒸剂组合物可用于滴水熏蒸方法，并且与单独的甲基碘相比具有增加的挥发性，当使用甲基碘作为熏蒸剂时，这可以降低水污染的风险。
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23.发明申请AZEOTROPE-LIKE COMPOSITIONS OF HEPTAFLUOROPROPANE AND TRIFLUOROIODOMETHANE 有权四氢呋喃和三氟甲磺酸的AZEOTROPE-LIKE组合物公开(公告)号：US20100176332A1
公开(公告)日：2010-07-15
申请号：US12352859
申请日：2009-01-13
CPC分类号： C09K5/045 , A62D1/00 , A62D1/0057 , A62D1/0071 , A62D1/0092 , C08J9/144 , C08J2203/142 , C08J2203/182 , C09K3/30 , C09K2205/122 , C09K2205/32
摘要： Provided are azeotrope-like compositions comprising heptafluoropropane and trifluoroiodomethane and uses thereof, including use in refrigerant compositions, refrigeration systems, blowing agents, fire suppressant compositions, and aerosol propellants.
摘要翻译： 提供包含七氟丙烷和三氟碘甲烷的类共沸组合物及其用途，包括用于制冷剂组合物，制冷系统，发泡剂，灭火剂组合物和气溶胶推进剂中。
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公开(公告)号：US20090305876A1
公开(公告)日：2009-12-10
申请号：US12351807
申请日：2009-01-09
CPC分类号： C08J9/144 , B01D11/0288 , B01J35/0006 , B01J37/0219 , C08G18/4816 , C08G2101/0025 , C08J9/146 , C08J9/147 , C08J2203/162 , C08J2325/06 , C08J2375/04 , C09D7/20 , C09K3/00 , C09K3/30 , C09K5/044 , C09K5/045 , C09K2205/122 , C09K2205/126 , C09K2205/22 , C09K2205/24 , C11B9/025 , Y02C20/30
摘要： Various uses of fluorinated alkenes, particularly HFO-1234 and HFCO-1233zd in a variety of applications, including refrigeration, foams, blowing agents, aerosols, propellants, solvent compositions, fire extinguishing and suppressing agents, extraction agents and catalyst deposition are disclosed.
摘要翻译： 公开了氟代烯烃，特别是HFO-1234和HFCO-1233zd在各种应用中的各种用途，包括制冷，泡沫，发泡剂，气溶胶，推进剂，溶剂组合物，灭火和抑制剂，萃取剂和催化剂沉积。
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公开(公告)号：US20090269478A1
公开(公告)日：2009-10-29
申请号：US12422260
申请日：2009-04-11
CPC分类号： A61B5/1172
摘要： A method and composition for transforming a latent physiological biometric into a visible physiological biometric are provided, the method comprising: providing a latent biometric disposed on a surface of an article, wherein said biometric comprises at least one eccrine-derived compound; contacting said latent biometric with a developing solution, wherein said developing solution comprises at least one imaging reagent selected from ninhydrin and 1,8-diazafluoren-9-one and a carrier solvent comprising at least one C3-C4 hydrofluorocarbon; and reacting said imaging reagent with said eccrine-derived compound to produce a visible physiological biometric.
摘要翻译： 提供了一种用于将潜在生理学生物转化为可见生理生物学的方法和组合物，所述方法包括：提供设置在制品表面上的潜伏生物测定，其中所述生物测定包含至少一种衍生化合物; 使所述潜在生物测定与显影溶液接触，其中所述显影溶液包含至少一种选自茚三酮和1,8-二氮杂芴-9-酮的成像试剂和包含至少一种C 3 -C 4氢氟烃的载体溶剂; 并使所述成像试剂与所述外分泌衍生的化合物反应以产生可见的生理学生物学特征。
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26.发明授权Azeotrope-like composition of 1-chloro-1,3,3,3-tetrafluoropropane and hydrogen fluoride 有权1-氯-1,3,3,3-四氟丙烷和氟化氢的类共沸组合物公开(公告)号：US06903063B2
公开(公告)日：2005-06-07
申请号：US10283400
申请日：2002-10-29
CPC分类号： C07C19/10 , C07C17/00 , C07C17/38 , C07C17/383
摘要： The invention relates to azeotropic and azeotrope-like mixtures of 1-chloro-1,3,3,3-tetrafluoropropane (HCFC-244fa) and hydrogen fluoride, which are useful as intermediates in the production of HCFC-244fa.
摘要翻译： 本发明涉及可用作生产HCFC-244fa的中间体的1-氯-1,3,3,3-四氟丙烷（HCFC-244fa）和氟化氢的共沸和类共沸混合物。
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27.发明授权Method and apparatus to reduce fractionation of fluid blend during storage and transfer 失效在储存和转移期间减少流体混合物分馏的方法和装置公开(公告)号：US06234352B1
公开(公告)日：2001-05-22
申请号：US09371319
申请日：1999-08-10
IPC分类号： B65D3500
CPC分类号： F17C1/00 , F17C7/00 , F17C2201/0109 , F17C2201/018 , F17C2201/032 , F17C2201/058 , F17C2203/0643 , F17C2203/0646 , F17C2203/0648 , F17C2205/0308 , F17C2205/0329 , F17C2221/038 , F17C2223/0123 , F17C2223/0153 , F17C2260/031
摘要： A method and apparatus for storing and dispensing in liquid form a blend of fluids which normally fractionate upon boiling. The apparatus includes a container having an internal bladder dividing the container into two chambers. The first chamber contains the liquid blend, and the second chamber contains a pressurizing fluid in sufficient quantity to maintain the pressure on the other side of the bladder in the first chamber above the bubble point pressure of the liquid blend. In this manner, the vapor space above the fluid blend is eliminated, and thus the effect of fractionation caused by vaporization is essentially eliminated during dispensing or leakage of the blend from the package.
摘要翻译： 用于储存和分配液体的方法和装置形成通常在沸腾时分馏的流体混合物。 该装置包括具有将容器分成两个室的内部囊的容器。 第一室包含液体共混物，第二室含有足够量的加压流体，以将第一室中的气囊的另一侧的压力保持在液体共混物的泡点压力以上。 以这种方式，消除了流体共混物上方的蒸汽空间，因此在从包装中分配或泄漏共混物的过程中基本上消除了由汽化引起的分馏作用。
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公开(公告)号：US5736063A
公开(公告)日：1998-04-07
申请号：US736613
申请日：1996-10-24
CPC分类号： C09K5/045 , C09K2205/106 , C09K2205/12 , C09K2205/134 , C09K2205/22 , C09K2205/34
摘要： The present invention provides refrigerant blends which are replacements for chlorodifluoromethane(HCFC-22). The present blends have refrigeration characteristics which are similar to HCFC-22. The blends comprise from about 10 to about 90 weight percent of a first component selected from the group consisting of 1,1,1-trifluoroethane, difluoromethane, propane, and mixtures thereof; from about 1 to about 50 weight percent of a second component selected from the group consisting of hydrofluorocarbon having 1 to 3 carbon atoms, fluorocarbon having 1 to 3 carbon atoms, inorganic compound, and mixtures thereof having a boiling point at atmospheric pressure in the range from about -90 degrees C. to less than -50 degrees C.; and from about 1 to about 50 weight percent of a third component which is hydrofluorocarbon having 1 to 3 carbon atoms, other than 1,1,1-trifluoroethane, having a boiling point at atmospheric pressure in the range from about -50 degrees C. to about -10 degrees C. The refrigerant compositions have a vapor pressure substantially equal to the vapor pressure of HCFC-22.
摘要翻译： 本发明提供了用于二氯甲烷（HCFC-22）的替代物的制冷剂共混物。 本发明共混物具有类似于HCFC-22的制冷特性。 共混物包含约10至约90重量％的选自1,1,1-三氟乙烷，二氟甲烷，丙烷及其混合物的第一组分; 约1至约50重量％的选自碳原子数1〜3的氢氟烃，第1至3个碳原子的碳氟化合物的第二组分，无机化合物及其在大气压下的沸点范围内的混合物 从约-90摄氏度到低于-50摄氏度; 和约1至约50重量％的第三组分，其是具有1至3个碳原子的氢氟烃，不同于1,1,1-三氟乙烷，其沸点在大气压下在约-50℃的范围内。 至约-10℃。制冷剂组合物的蒸气压基本上等于HCFC-22的蒸气压。
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29.发明授权Azeotrope-like compositions of trifluoromethane, carbon dioxide, ethane and hexafluoroethane 失效三氟甲烷，二氧化碳，乙烷和六氟乙烷的类共沸组合物
公开(公告)号：US5728315A
公开(公告)日：1998-03-17
申请号：US641584
申请日：1996-05-01
申请人： Rajiv Ratna Singh , Ian Robert Shankland , Roy Phillip Robinson , Hang Thanh Pham , Raymond Hilton Percival Thomas , Peter Brian Logsdon
发明人： Rajiv Ratna Singh , Ian Robert Shankland , Roy Phillip Robinson , Hang Thanh Pham , Raymond Hilton Percival Thomas , Peter Brian Logsdon
CPC分类号： C08J9/127 , C09K3/30 , C09K5/045 , C08J2203/14 , C08J2203/142 , C08J2207/04 , C08J2375/04 , C09K2205/106 , C09K2205/12 , C09K2205/128 , C09K2205/32 , Y10S264/05 , Y10S521/91
摘要： Azeotrope-like compositions of trifluoromethane, carbon dioxide, ethane, and hexafluoroethane are provided. The compositions of the invention are environmentally desirable for use as refrigerants, aerosol propellants, blowing agents for polymer foam, heat transfer media, and gaseous dielectrics.
摘要翻译： 提供了三氟甲烷，二氧化碳，乙烷和六氟乙烷的类共沸组合物。 本发明的组合物在用作制冷剂，气溶胶推进剂，聚合物泡沫的发泡剂，传热介质和气体电介质中是环境需要的。
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公开(公告)号：US08592538B2
公开(公告)日：2013-11-26
申请号：US13331588
申请日：2011-12-20
CPC分类号： C08F2/06 , C08F110/10 , C08F2500/01
摘要： Azeotropic or azeotrope-like compositions of the present technology include methyl chloride and at least one hydrofluorocarbon or hydrofluoro-olefin. In some examples, the at least one hydrofluorocarbon or hydrofluoro-olefin can be selected from the group consisting of 1,1,1,2-tetrafluoroethane and 1,3,3,3-tetrafluoropropene. The azeotropic or azeotrope-like compositions can be used as solvents or diluents in polymerization processes, including slurry polymerization processes.
摘要翻译： 本技术的共沸或类共沸组合物包括甲基氯和至少一种氢氟烃或氢氟烯烃。 在一些实例中，至少一种氢氟烃或氢氟烯烃可以选自1,1,1,2-四氟乙烷和1,3,3,3-四氟丙烯。 共沸或类共沸组合物可用作聚合过程中的溶剂或稀释剂，包括淤浆聚合方法。
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