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    METHOD FOR PRODUCING FLUORINE-CONTAINING ALKANE
    17.
    发明申请
    METHOD FOR PRODUCING FLUORINE-CONTAINING ALKANE 审中-公开

    公开(公告)号：US20160168059A1

    公开(公告)日：2016-06-16

    申请号：US15050739

    申请日：2016-02-23

    Applicant: DAIKIN INDUSTRIES, LTD.

    Inventor： Yuko SHIOTANI ,  Kakeru HANABUSA ,  Takehiro CHAKI ,  Kazuhiro TAKAHASHI

    IPC: C07C17/354

    CPC classification number: C07C17/23 ,  C07C17/354 ,  C07C19/08

    Abstract: The present invention provides a method for producing a fluorine-containing alkane, which comprises reacting at least one fluorine-containing compound selected from the group consisting of chlorine-containing fluoroalkanes and fluorine-containing alkenes with hydrogen gas in the presence of catalysts, wherein two or more catalysts having different catalytic activities are used, and the fluorine-containing compound and hydrogen gas, which are starting materials, are sequentially brought into contact with the catalysts in the order of the catalyst having a lower catalytic activity followed by the catalyst having a higher catalytic activity. According to the present invention, in the method for producing a fluorine-containing alkane by using chlorine-containing fluoroalkane or fluorine-containing alkene as a starting material, and subjection it to a reduction reaction or a hydrogen addition reaction, the objective fluorine-containing alkane can be produced with high productivity.

    Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb)
    18.
    发明授权
    Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb) 有权
    制备2-氯-1,1,1,2-四氟丙烷（HCFC-244bb）的方法

    公开(公告)号：US09242910B2

    公开(公告)日：2016-01-26

    申请号：US14208411

    申请日：2014-03-13

    Applicant: Honeywell International, Inc.

    Inventor： Haluk Kopkalli ,  Daniel C. Merkel ,  Ron Joseph Roof

    IPC: C07C17/25 ,  C07C17/08 ,  C07C17/087 ,  C07C17/20 ,  C07C17/23

    CPC classification number: C07C17/08 ,  C07C17/087 ,  C07C17/206 ,  C07C17/23 ,  C07C17/25 ,  C07C19/10 ,  C07C21/18 ,  C07C19/08

    Abstract: The invention relates to a process to produce HCFC-244bb from HCFO-1233xf wherein, in one embodiment, co-feed species HFC-245cb is added to the reaction at a pressure of at least about 100 psig; and in another embodiment it is added to maintain a mole ratio of HFC-245cb to HCFO-1233xf of between about 0.005:1 to about 1:1. The HFC-245cb may be added as recycled by-product of the reaction and/or added as fresh feed. The HFC-245cb provides elevated pressures to the reaction thereby facilitating reactor operation, mixing and HCFC-244bb product removal. Other co-feed species are also disclosed.

    Abstract translation: 本发明涉及从HCFO-1233xf生产HCFC-244bb的方法，其中在一个实施方案中，在至少约100psig的压力下将共进料物质HFC-245cb加入到反应中; 并且在另一个实施方案中，加入以保持HFC-245cb与HCFO-1233xf的摩尔比在约0.005:1至约1:1之间。 可以将HFC-245cb作为反应的副产物加入和/或作为新鲜饲料加入。 HFC-245cb为反应提供升高的压力，从而便于反应器操作，混合和HCFC-244bb产品的去除。 还公开了其他共同饲料物种。

    Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb)
    19.
    发明授权
    Process to manufacture 2-chloro-1,1,1,2-tetrafluoropropane (HCFC-244bb) 有权
    制备2-氯-1,1,1,2-四氟丙烷（HCFC-244bb）的方法

    公开(公告)号：US09233895B2

    公开(公告)日：2016-01-12

    申请号：US14695579

    申请日：2015-04-24

    Applicant: Honeywell International, Inc.

    Inventor： Haluk Kopkalli ,  Daniel C. Merkel ,  Ron Joseph Roof

    IPC: C07C17/087 ,  C07C17/08 ,  C07C17/20 ,  C07C17/23 ,  C07C17/25

    CPC classification number: C07C17/087 ,  C07C17/08 ,  C07C17/206 ,  C07C17/23 ,  C07C17/25 ,  C07C19/10 ,  C07C21/18 ,  C07C19/08

    Abstract: The invention relates to a process to produce HCFC-244bb from HCFO-1233xf wherein, in one embodiment, one or more co-feed species having a normal boiling point of between about −80° C. to about 0° C., such as HFC-245cb, is added to the reaction at a pressure of at least about 100 psig; and in another embodiment it is added to maintain a mole ratio of HFC-245cb to HCFO-1233xf of between about 0.005:1 to about 1:1. The HFC-245cb may be added as recycled by-product of the reaction and/or added as fresh feed. The HFC-245cb provides elevated pressures to the reaction thereby facilitating reactor operation, mixing and HCFC-244bb product removal. Other co-feed species are also disclosed.

    Abstract translation: 本发明涉及一种从HCFO-1233xf生产HCFC-244bb的方法，其中在一个实施方案中，一种或多种具有约-80℃至约0℃之间的标准沸点的共进料物质，例如 将HFC-245cb在至少约100psig的压力下加入到反应中; 并且在另一个实施方案中，加入以保持HFC-245cb与HCFO-1233xf的摩尔比在约0.005:1至约1:1之间。 可以将HFC-245cb作为反应的副产物加入和/或作为新鲜饲料加入。 HFC-245cb为反应提供升高的压力，从而便于反应器操作，混合和HCFC-244bb产品的去除。 还公开了其他共同饲料物种。

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