公开(公告)号：US5556509A

公开(公告)日：1996-09-17

申请号：US268213

申请日：1994-06-29

申请人： Paul D. Trokhan ,  Dean V. Phan

发明人： Paul D. Trokhan ,  Dean V. Phan

IPC分类号： D21F1/46 ,  D21F3/02 ,  D21F11/00 ,  D21H27/00 ,  D21H15/02

CPC分类号： D21F11/006 ,  Y10S162/90 ,  Y10T428/24322 ,  Y10T428/24446 ,  Y10T428/24455

摘要： A paper structure having at least three regions is disclosed. The paper structure has a first region, a patterned second region, and a third transition region connecting the first and second regions. The first and second regions are disposed at different elevations, and can each have a thickness less than a thickness of the transition region. An apparatus and process for making such a paper structure are also disclosed.

摘要翻译： 公开了具有至少三个区域的纸结构。 纸结构具有第一区域，图案化第二区域和连接第一和第二区域的第三过渡区域。 第一和第二区域设置在不同的高度处，并且每个区域的厚度都可以小于过渡区域的厚度。 还公开了用于制造这种纸结构的设备和方法。

公开(公告)号：US5451452A

公开(公告)日：1995-09-19

申请号：US249510

申请日：1994-05-26

申请人： Dean V. Phan ,  Paul D. Trokhan

发明人： Dean V. Phan ,  Paul D. Trokhan

IPC分类号： A61F13/53 ,  A61L15/24 ,  A61L15/42 ,  A61L15/60 ,  C08F20/38 ,  C08F20/52 ,  C08F26/02 ,  C08F28/00 ,  C08F220/04 ,  C08F220/38 ,  C08F222/40 ,  C08F226/02 ,  C08F228/02 ,  C08G59/40 ,  C08G69/00 ,  C08G69/04 ,  C08J9/14 ,  B32B27/00

CPC分类号： A61L15/60 ,  A61L15/24 ,  A61L15/425 ,  Y10T428/2481 ,  Y10T428/24851 ,  Y10T428/249975 ,  Y10T428/249979 ,  Y10T428/24998 ,  Y10T428/249986 ,  Y10T442/652

摘要： An improved superabsorbent polymer foam having a morphology to provide improved absorptive properties is disclosed. The foam preferably comprises a superabsorbent polymer formed from a substantially water-soluble, unsaturated monomer having neutralized carboxyl groups and a substantially water-soluble internal crosslinking agent. The monomer and crosslinking agent are expanded in the presence of a substantially water-insoluble blowing agent and a suitable solvent and reacted to form a superabsorbent polymer foam having substantially continuous, intercommunicating channels substantially throughout the foam and a relatively high surface area to mass ratio.Methods for making the foam and absorbent products, members and articles containing the foam are also disclosed.

摘要翻译： 公开了具有提供改善的吸收性能的形态的改进的超吸收聚合物泡沫体。 泡沫体优选包含由具有中和的羧基和基本上水溶性的内部交联剂的基本上水溶性的不饱和单体形成的超吸收性聚合物。 单体和交联剂在基本上不溶于水的发泡剂和合适的溶剂的存在下膨胀，并反应以形成具有基本上连续的，相互连通的通道，基本上贯穿整个泡沫体和相对较高的表面积与质量比的超吸收性聚合物泡沫体。 还公开了制造泡沫和吸收产品，含有泡沫的物品和制品的方法。

公开(公告)号：US5443691A

公开(公告)日：1995-08-22

申请号：US71834

申请日：1993-07-28

申请人： Dean V. Phan ,  Paul D. Trokhan

发明人： Dean V. Phan ,  Paul D. Trokhan

IPC分类号： D21F1/44 ,  D21F11/00 ,  D21H27/00 ,  F22B37/48 ,  D21H27/02

CPC分类号： D21F11/006 ,  D21F11/00 ,  F22B37/483 ,  Y10T428/24273 ,  Y10T428/24322 ,  Y10T428/24331 ,  Y10T428/24339 ,  Y10T428/24455 ,  Y10T428/24562 ,  Y10T428/24992

摘要： A process for making a cellulosic fibrous structure such as paper. In one embodiment, the fibrous structure has high and low basis weight regions. The high basis weight region is subdivided into low density regions, so that a fibrous structure having three regions is produced. In a second embodiment, the fibrous structure has four regions. Both the high and low basis weight regions are further subdivided into high and low density regions. The process comprises applying noncoincident differential pressure to selected regions of an embryonic fibrous structure.

摘要翻译： 制造纤维素纤维结构如纸的方法。 在一个实施方案中，纤维结构具有高和低的基重区域。 高基重区域被细分为低密度区域，从而产生具有三个区域的纤维结构体。 在第二实施例中，纤维结构具有四个区域。 高和低基重区域都进一步细分为高密度和低密度区域。 该方法包括对胚胎纤维结构的选定区域施加非重合差压。

公开(公告)号：US5503715A

公开(公告)日：1996-04-02

申请号：US66828

申请日：1993-05-24

申请人： Paul D. Trokhan ,  Dean V. Phan ,  Larry L. Huston

发明人： Paul D. Trokhan ,  Dean V. Phan ,  Larry L. Huston

IPC分类号： D21F1/66 ,  D21F1/76 ,  D21F7/00 ,  D21F11/00 ,  D21F11/14 ,  D21H15/02 ,  D21H27/00 ,  D21H27/02 ,  D21F1/10

CPC分类号： D21F11/006 ,  D21H27/02 ,  Y10S162/903

摘要： Disclosed herein is a cellulosic fibrous structure having multiple regions distinguished from one another by basis weight. The structure is a paper having an essentially continuous high basis weight network, and discrete regions of low basis weight which circumscribe discrete regions of intermediate basis weight. The cellulosic fibers forming the low basis weight regions may be radially oriented relative to the centers of the regions. The paper may be formed by using a forming belt having zones with different flow resistances. The basis weight of a region of the paper is generally inversely proportional to the flow resistance of the zone of the forming belt, upon which such region was formed. The zones of different flow resistances provide for selectively draining a liquid carrier having suspended cellulosic fibers through the different zones of the forming belt.

摘要翻译： 本文公开了具有通过基重彼此区分的多个区域的纤维素纤维结构。 该结构是具有基本上连续的高基重网络的纸，以及低基重的离散区域，其限制了中间基重的离散区域。 形成低基重区域的纤维素纤维可以相对于区域的中心径向定向。 纸可以通过使用具有不同流阻的区域的成形带来形成。 纸张的区域的基重通常与形成该区域的成形带的区域的流动阻力成反比。 不同流动阻力的区域提供选择性排出具有悬浮的纤维素纤维的液体载体穿过成形带的不同区域。

公开(公告)号：US5427696A

公开(公告)日：1995-06-27

申请号：US4333

申请日：1993-01-14

申请人： Dean V. Phan ,  Paul D. Trokhan ,  Toan Trinh

发明人： Dean V. Phan ,  Paul D. Trokhan ,  Toan Trinh

IPC分类号： C07C219/06 ,  D21H17/06 ,  D21H17/07 ,  D21H17/14 ,  D21H21/24

CPC分类号： C07C219/06 ,  D21H17/06 ,  D21H17/07 ,  D21H17/14

摘要： Biodegradable chemical softening compositions are provided comprising a mixture of a quaternized ester-amine compound and a polyhydroxy compound. Preferred biodegradable quaternized ester-amine compounds include diester dialkyl dimethyl ammonium salts such as diester ditallow dimethyl ammonium chloride, diester di(touch hydrogenated)tallow dimethyl ammonium chloride and diester di(hydrogenated)tallow dimethyl ammonium chloride. Preferred polyhydroxy compounds are selected from the group consisting of glycerol, and polyethylene glycols and polypropylene glycols having a weight average molecular weight from about 200 to 4000.The biodegradable chemical softening compositions are prepared by first mixing the quaternized ester-amine compound into the polyhydroxy compound at a specific temperature range wherein the polyhydroxy compound is miscible with the quaternized ester-amine compound and then diluting the mixture with a liquid carrier at a specific pH and temperature range to form an aqueous vesicle dispersion suitable for treating fibrous cellulosic material. The biodegradable chemical softening compositions disclosed herein are primarily intended for softening disposable paper products such as tissues and towels. However, the biodegradable chemical softening compositions can also be used to soften fibrous cellulosic materials in textile form.

摘要翻译： 提供可生物降解的化学软化组合物，其包含季铵化的酯 - 胺化合物和多羟基化合物的混合物。 优选的可生物降解的季铵酯化合物包括二酯二烷基二甲基铵盐如二酯二牛脂二甲基氯化铵，二酯（触摸氢化）牛脂二甲基氯化铵和二酯二（氢化）牛脂二甲基氯化铵。 优选的多羟基化合物选自甘油，聚乙二醇和重均分子量为约200至4000的聚丙二醇。可生物降解的化学软化组合物通过首先将季铵化的酯 - 胺化合物混合到多羟基化合物 在特定的温度范围内，其中多羟基化合物与季铵化的酯 - 胺化合物混溶，然后在特定的pH和温度范围内用液体载体稀释混合物，形成适于处理纤维状纤维素材料的水性囊泡分散体。 本文公开的可生物降解的化学软化组合物主要用于软化一次性纸制品如组织和毛巾。 然而，可生物降解的化学软化组合物也可用于以纺织形式软化纤维状纤维素材料。

公开(公告)号：US5397435A

公开(公告)日：1995-03-14

申请号：US140571

申请日：1993-10-22

申请人： Ward W. Ostendorf ,  Stephen R. Kelly ,  Paul D. Trokhan ,  Dean V. Phan

发明人： Ward W. Ostendorf ,  Stephen R. Kelly ,  Paul D. Trokhan ,  Dean V. Phan

IPC分类号： A47K7/00 ,  A47K10/16 ,  D21H17/06 ,  D21H17/07 ,  D21H17/27 ,  D21H17/47 ,  D21H17/53 ,  D21H21/20 ,  D21H21/24 ,  D21H27/00 ,  D21H27/30 ,  D21H27/40 ,  D21H21/22

CPC分类号： D21H17/07 ,  D21H17/06 ,  D21H21/24 ,  D21H27/30

摘要： Multi-ply facial tissue paper products comprising chemical softener compositions and a combination of a wet strength binder, permanent and/or temporary, and a dry strength binder is disclosed.The multi-ply facial tissue paper products contain a chemical softening composition comprising a mixture of a quaternary ammonium compound and a polyhydroxy compound. Preferred quaternary ammonium compounds include dialkyl dimethyl ammonium salts such as di(hydrogenated)tallow dimethyl ammonium chloride and/or di(hydrogenated)tallow dimethyl ammonium methyl sulfate. Preferred polyhydroxy compounds are selected from the group consisting of glycerol, polyglycerols having a weight average molecular weight of from about 150 to about 800, polyoxyethylene glycols and polyoxypropylene glycols having a weight average molecular weight from about 200 to 1000. The multi-ply facial tissue paper products also contain an effective amount of a wet strength binder, permanent and/or temporary, and a dry strength binder to control linting and/or to offset the loss in tensile strength, if any, resulting from the use of the chemical softening compositions. The use of both wet strength binder, either permanent ot temporary, and a dry strength binder also improves the retention of the chemical softening composition in the sheet.Preferably, the majority of the chemical softening compositions will be disposed on the outer layers of the multi-ply facial tissue paper products where they are most effective. In other words, the chemical softening compositions and the wet strength binder, permanent and/or temporary, and a dry strength binder can be selectively distributed within the multi-ply facial tissue paper product to enhance the softness, absorbency and/or lint resistance of a particular layer or ply.

摘要翻译： 公开了包含化学软化剂组合物和湿强度粘合剂，永久和/或临时和干强度粘合剂的组合的多层面巾纸产品。 多层面巾纸产品含有包含季铵化合物和多羟基化合物的混合物的化学软化组合物。 优选的季铵化合物包括二烷基二甲基铵盐如二（氢化）牛脂二甲基氯化铵和/或二（氢化）牛脂二甲基铵甲基硫酸盐。 优选的多羟基化合物选自甘油，重均分子量为约150至约800的聚甘油，重均分子量为约200至1000的聚氧乙烯二醇和聚氧丙烯二醇。多层面巾纸 纸制品还含有有效量的湿强度粘合剂，永久和/或临时的，以及干强度粘合剂，用于控制使用化学软化组合物产生的拉伸强度（如果有的话）的损失和/或抵消 。 使用湿强度粘合剂（永久暂时的）和干强度粘合剂的使用也改善了片材中化学软化组合物的保留性。 优选地，大多数化学软化组合物将被布置在多层面巾纸产品的外层上，在其最有效的地方。 换句话说，化学软化组合物和湿强度粘合剂（永久和/或临时）和干强度粘合剂可以选择性地分布在多层面巾纸产品中以增强柔软度，吸收性和/或绒毛抗性 特定的层或层。

公开(公告)号：US5264082A

公开(公告)日：1993-11-23

申请号：US865597

申请日：1992-04-09

申请人： Dean V. Phan ,  Paul D. Trokhan

发明人： Dean V. Phan ,  Paul D. Trokhan

IPC分类号： C07C219/06 ,  C08L101/16 ,  D21H17/06 ,  D21H17/07 ,  D21H17/14 ,  D21H21/22

CPC分类号： D21H17/14 ,  C07C219/06 ,  D21H17/06 ,  D21H17/07

摘要： Tissue paper webs useful in the manufacture of soft, absorbent products such as paper towels, napkins, and facial tissues, and processes for making the webs. The tissue paper webs comprise papermaking fibers, a biodegradable quaternized amine-ester softening compound, a wetting agent, and a permanent wet strength resin. The process comprises a first step of forming an aqueous papermaking furnish from the above-mentioned components. The second and third steps in the basic process are the deposition of the papermaking furnish onto a foraminous surface such as a Fourdrinier wire and removal of the water from the deposited furnish. An alternate process involves the use of the furnish containing the aforementioned components in a papermaking process which will produce a pattern densified fibrous web having a relatively high bulk field of relatively low fiber density in a patterned array of spaced zones of relatively high fiber density.

摘要翻译： 可用于制造软质吸收性产品如纸巾，餐巾和面巾纸的组织纸网，以及用于制造网的方法。 薄纸纸包括造纸纤维，可生物降解的季铵化胺 - 酯软化化合物，润湿剂和永久湿强度树脂。 该方法包括从上述组分形成水性造纸配料的第一步骤。 基本过程中的第二和第三步骤是将造纸配料沉积到诸如长网的多孔表面上，并从沉积的配料中除去水。 替代方法涉及在造纸方法中使用含有上述组分的配料，其将在具有相对较高纤维密度的间隔区域的图案化阵列中产生具有相对较高纤维密度的较高体积的图案致密化纤维网。

公开(公告)号：US5240562A

公开(公告)日：1993-08-31

申请号：US966794

申请日：1992-10-27

申请人： Dean V. Phan ,  Paul D. Trokhan

发明人： Dean V. Phan ,  Paul D. Trokhan

IPC分类号： D06M13/463 ,  A61K8/02 ,  A61Q19/10 ,  C11D1/62 ,  C11D3/20 ,  C11D3/37 ,  C11D17/04 ,  D06M13/02 ,  D06M13/322 ,  D21H17/06 ,  D21H17/07 ,  D21H17/09 ,  D21H19/10 ,  D21H21/22

CPC分类号： D21H17/06 ,  A61K8/0208 ,  A61Q19/10 ,  C11D1/62 ,  C11D17/049 ,  C11D3/2065 ,  C11D3/2068 ,  C11D3/3707 ,  D21H17/07 ,  D21H17/09 ,  D21H21/22

摘要： Fibrous cellulose material useful in the manufacture of soft, absorbent paper products such as paper towels, facial tissues, and toilet tissue are disclosed. The paper products contain a chemical softening composition comprising a mixture of a quaternary ammonium compound and a polyhydroxy compound. Preferred quaternary ammonium compound include dialkyldimethylammonium salts such as di(hydrogenated) tallow dimethyl ammonium chloride and di(hydrogenated) tallow dimethyl ammonium methyl sulfate. Preferred polyhydroxy compounds are selected from the group consisting of glycerol, and polyethylene glycols and polypropylene glycols having a weight average molecular weight from about 200 to 4000. The chemical softening compositions are prepared by first mixing the polyhydroxy compound into the quaternary ammonium compound at a specific temperature range wherein the polyhydroxy compound is miscible with the quaternary ammonium compound and then diluting the mixture with water at an elevated temperature to form an aqueous vesicle dispersion suitable for treating the fibrous cellulose material.

摘要翻译： 公开了用于制造柔软，吸收性纸制品如纸巾，面巾纸和卫生纸的纤维素纤维素材料。 纸制品含有包含季铵化合物和多羟基化合物的混合物的化学软化组合物。 优选的季铵化合物包括二（二氢化）牛脂二甲基氯化铵和二（氢化）牛脂二甲基铵甲基硫酸二烷基二甲基铵盐。 优选的多羟基化合物选自甘油，聚乙二醇和重均分子量为约200至4000的聚丙二醇。化学软化组合物是通过首先将多羟基化合物以特定的 温度范围，其中多羟基化合物与季铵化合物可混溶，然后在高温下用水稀释混合物，形成适于处理纤维状纤维素材料的水性囊泡分散体。

公开(公告)号：US5624532A

公开(公告)日：1997-04-29

申请号：US388970

申请日：1995-02-15

申请人： Paul D. Trokhan ,  Dean V. Phan

发明人： Paul D. Trokhan ,  Dean V. Phan

IPC分类号： A47K7/00 ,  D21H17/05 ,  D21H17/06 ,  D21H17/53 ,  D21H21/10 ,  D21H21/18 ,  D21H23/26 ,  D21H21/22

CPC分类号： D21H23/26 ,  D21H17/06 ,  D21H17/53 ,  D21H21/10 ,  D21H21/18

摘要： Tissue paper having an enhanced bulk softness through incorporation of an effective amount of a polyhydroxy compound is disclosed. Preferably, from about 0.1% to about 2.0% of the polyhydroxy compound, on a dry fiber weight basis. These nonionic compounds have high rates of retention when applied to wet tissue paper webs according to the process described herein. Tissue embodiments of the present invention may further comprise a quantity of strength additive, such as starch, to increase paper strength.

摘要翻译： 公开了通过加入有效量的多羟基化合物具有增强的体柔性的组织纸。 优选地，约0.1％至约2.0％的多羟基化合物，基于干纤维重量。 这些非离子化合物根据本文所述的方法应用于湿纸巾幅时具有高的保留率。 本发明的组织实施方案还可以包含一定量的强度添加剂，例如淀粉，以增加纸强度。

公开(公告)号：US5547747A

公开(公告)日：1996-08-20

申请号：US576322

申请日：1995-12-21

申请人： Paul D. Trokhan ,  Dean V. Phan

发明人： Paul D. Trokhan ,  Dean V. Phan

IPC分类号： A61F13/53 ,  A61F13/15 ,  A61F13/49 ,  A61F13/534 ,  A61F13/539 ,  D04H13/00 ,  D06M10/00 ,  D21H19/24 ,  A61F13/20

CPC分类号： A61F13/53713 ,  A61F13/53717 ,  A61F2013/1543 ,  A61F2013/15439 ,  A61F2013/53726 ,  A61F2013/53734 ,  Y10T428/249994

摘要： A process for making an absorbent structure having a capillary substrate and regions of osmotic absorbent on the capillary substrate. The osmotic absorbent is cured from a liquid precursor applied to the capillary substrate. The capillary substrate has regions of topographically different elevations, taken normal to the plane of the capillary substrate. The capillary substrate is passed through a gap between a transfer roll and an anvil roll in a printing apparatus. The transfer roll has a liquid precursor on its periphery. The liquid precursor is applied to only the topographically elevated regions of the capillary substrate which contact the periphery of the transfer roll. By changing the topography of the capillary substrate, the liquid precursor can be applied to the capillary substrate in different pattern, without changing the transfer roll. This arrangement allows for absorbent structures having various patterns of osmotic absorbent on a capillary substrate to be readily produced with great flexibility in the manufacturing process.

摘要翻译： 一种制造具有毛细管基底的吸收结构和毛细管基底上的渗透吸收区的方法。 渗透吸收剂从施加到毛细管基底上的液体前体固化。 毛细管基底具有垂直于毛细管基底的平面的地形不同的高度的区域。 在打印装置中毛细管基底通过转印辊和砧辊之间的间隙。 转印辊在其周边上具有液体前体。 液体前体仅施加到接触转移辊周边的毛细管基底的地形上升的区域。 通过改变毛细管基底的形貌，液体前体可以以不同的图案施加到毛细管基底上，而不改变转移辊。 这种布置允许在毛细管基底上具有各种图案的渗透吸收剂的吸收结构在制造过程中容易地以很大的灵活性产生。