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    Process for production of dihydric phenols
    2.
    发明授权
    Process for production of dihydric phenols 失效
    二元酚生产工艺

    公开(公告)号：US4560808A

    公开(公告)日：1985-12-24

    申请号：US688377

    申请日：1985-01-02

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C07C37/48 ,  C07C39/16

    CPC classification number: C07C37/48 ,  C07C319/22

    Abstract: A transalkylation process for the preparation of dihydric phenols comprising reacting, in the presence of an acid or base catalyst, at least one mole of an aromatic monohydroxy compound such as a phenol with at least one mole of an aromatic dihydroxy compound such as a dihydric phenol, thereby forming at least one dihydric phenol which is different than said aromatic dihydroxy compound.

    Abstract translation: 一种用于制备二元酚的烷基转移方法，包括在酸或碱催化剂存在下使至少一摩尔芳族单羟基化合物如苯酚与至少一摩尔芳族二羟基化合物如二元酚反应 从而形成与所述芳族二羟基化合物不同的至少一种二元酚。

    Flame retardant aromatic polycarbonate compositions made from fluorinated diphenols
    4.
    发明授权
    Flame retardant aromatic polycarbonate compositions made from fluorinated diphenols 失效
    由氟化二酚制成的阻燃芳族聚碳酸酯组合物

    公开(公告)号：US4379910A

    公开(公告)日：1983-04-12

    申请号：US221460

    申请日：1980-12-31

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C08L67/02 ,  C08G63/00 ,  C08G64/00 ,  C08L67/00 ,  C08L69/00 ,  C08G63/62

    CPC classification number: C08L69/00

    Abstract: Improved flame retardance is imparted to high molecular weight aromatic polycarbonate resins by selecting appropriate fluorinated diphenols and incorporating them in homopolymers or copolymers. The fluorinated diphenols have at least one fluorinated alkyl or fluorinated aryl group upon the methylene carbon atom positioned between the two phenol ring structures. The polycarbonates having improved flame retardance are made from fluorinated diphenols and halogen-containing carbonate precursors. Copolycarbonates having improved flame retardance are derived from the fluorinated diphenols and non-fluorinated diphenols. The flame retardant polycarbonates may be used in films and molded articles where improved resistance to flame is desirable.

    Abstract translation: 通过选择适当的氟化二酚并将其并入均聚物或共聚物中，可以对高分子量芳族聚碳酸酯树脂赋予更好的阻燃性。 氟化二酚在位于两个酚环结构之间的亚甲基碳原子上具有至少一个氟化烷基或氟化芳基。 具有改善的阻燃性的聚碳酸酯由氟化二酚和含卤素的碳酸酯前体制成。 具有改善的阻燃性的共聚碳酸酯衍生自氟化二酚和非氟化二酚。 阻燃聚碳酸酯可以用于薄膜和模塑制品中，其中希望提高耐火焰性。

    Fluorinated monophenols and diphenols and method for their preparation
    5.
    发明授权
    Fluorinated monophenols and diphenols and method for their preparation 失效
    氟化单酚和二酚及其制备方法

    公开(公告)号：US4358624A

    公开(公告)日：1982-11-09

    申请号：US221703

    申请日：1980-12-31

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C07C27/00 ,  C07C37/11 ,  C07C37/16 ,  C07C37/20 ,  C07C39/24 ,  C07C39/26 ,  C07C39/367 ,  C07C67/00 ,  C07C39/14

    CPC classification number: C07C37/20 ,  C07C37/115 ,  C07C37/16 ,  C07C39/24 ,  C07C39/26 ,  C07C39/367

    Abstract: Phenol reactants and fluorinated aldehydes or fluorinated ketones are reacted in the presence of organic sulfonic acid catalysts to yield fluorinated monophenols and fluorinated diphenols. Fluorinated monophenols can be isolated and reacted with additional phenol reactant in the presence of organic sulfonic acid catalysts to yield asymmetrical, as well as symmetrical, fluorinated diphenols. A preferred organic sulfonic acid catalyst is methanesulfonic acid. The novel fluorinated monophenols have a hydroxy group and a fluorinated aryl radical or fluorinated alkyl radical substituted upon the benzylic carbon atom. The novel fluorinated diphenols have at least one fluorinated aryl radical or fluorinated alkyl radical substituted upon the methylene carbon atom of the bisphenol.

    Abstract translation: 苯酚反应物和氟化醛或氟化酮在有机磺酸催化剂的存在下反应，得到氟化单酚和氟化二酚。 在有机磺酸催化剂的存在下，可以分离氟化单酚并与另外的酚反应物反应，以产生不对称以及对称的氟化二酚。 优选的有机磺酸催化剂是甲磺酸。 该新型氟化单酚具有在苄基碳原子上取代的羟基和氟化芳基或氟化烷基。 该新型氟化二酚具有在双酚的亚甲基碳原子上取代的至少一个氟化芳基或氟化烷基。

    Branched polycarbonate from carboxy containing diphenol
    8.
    发明授权
    Branched polycarbonate from carboxy containing diphenol 失效
    来自含羧基的二酚的支链聚碳酸酯

    公开(公告)号：US4562242A

    公开(公告)日：1985-12-31

    申请号：US685907

    申请日：1984-12-24

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C08G64/14 ,  C08G63/62

    CPC classification number: C08G64/14

    Abstract: High molecular weight, thermoplastic, randomly branched polycarbonates of an aromatic dihydric phenol, a carbonate precursor, and a chain branching agent comprising at least one compound selected from the formula: ##STR1## where A is selected from alkylene radicals from 1 to 6 carbons, alkylidene radicals from 2 to 6 carbons, cycloalkylene radicals and cycloalkylidene radicals containing from 4 to 6 carbon atoms;R and R' are independently selected from halogen radicals, monovalent hydrocarbon radicals of from 1 to 4 carbon atoms, and monovalent hydrocarbonoxy radicals of from 1 to 4 carbon atoms;n is an integer having a value of 0 or 1; andp and p' are integers having a value of 0 or 1.

    Abstract translation: 芳族二元酚的高分子量，热塑性，无规支化聚碳酸酯，碳酸酯前体和支链剂，其包含至少一种选自下式的化合物：其中A选自1至6个碳的亚烷基， 2至6个碳原子的亚烷基，含有4-6个碳原子的亚环烷基和亚环烷基; R和R'独立地选自卤素基团，1至4个碳原子的单价烃基和1至4个碳原子的单价烃氧基; n是0或1的整数; p和p'为0或1的整数。

    Polyestercarbonates exhibiting improved heat resistance from cycloalkylidene diphenol
    9.
    发明授权
    Polyestercarbonates exhibiting improved heat resistance from cycloalkylidene diphenol 失效
    表现出环烷基二酚具有改善的耐热性的聚酯碳酸酯

    公开(公告)号：US4554330A

    公开(公告)日：1985-11-19

    申请号：US621472

    申请日：1984-06-18

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C07C37/20 ,  C07C27/00 ,  C07C37/62 ,  C07C39/17 ,  C07C39/42 ,  C07C67/00 ,  C08G64/00 ,  C08G64/06 ,  C08L69/00 ,  C08G63/64 ,  C08L67/02

    CPC classification number: C08G64/06

    Abstract: Linear thermoplastic polycarbonates derived from:(i) a carbonate precursor; and(ii) at least one dihydric phenol represented by the general formula ##STR1## wherein R is independently selected from hydrogen and lower alkyl radicals,X is selected from monocyclic cycloalkylidene radicals containing from 8 to about 16 ring carbon atoms, andn and n' are independently selected from whole numbers having a value of from 0 to 2 inclusive, with the proviso that the sum of n plus n' is at least one.

    Abstract translation: 线性热塑性聚碳酸酯衍生自：（i）碳酸酯前体; 和（ii）由通式“IMAGE”表示的至少一种二元酚，其中R独立地选自氢和低级烷基，X选自含有8至约16个环碳原子的单环亚环烷基，n和n '独立地选自具有0至2的值的整数，其中n + n'的和为至少1。

    Polyester carbonate from branched chain alkylidene dihydric phenol
    10.
    发明授权
    Polyester carbonate from branched chain alkylidene dihydric phenol 失效
    来自支链亚烷基二元酚的聚酯碳酸酯

    公开(公告)号：US4547564A

    公开(公告)日：1985-10-15

    申请号：US599661

    申请日：1984-04-12

    Applicant: Victor Mark ,  Charles V. Hedges

    Inventor： Victor Mark ,  Charles V. Hedges

    IPC: C08G64/06 ,  C08G63/62

    CPC classification number: C08G64/06

    Abstract: Aromatic copolyester-carbonates derived from a carbonate precursor, at least one difunctional carboxylic acid or a reactive derivative thereof, and at least one branched alkylidene dihydric phenol represented by the general formula ##STR1## wherein: R and R' are independently selected from halogen and monovalent hydrocarbon radicals;R.sup.1 and R.sup.3 are independently selected from hydrogen and alkyl radicals;R.sup.2 is selected from alkyl radicals, with the proviso that if R.sup.1 and R.sup.3 are both hydrogen then R.sup.2 is selected from branched alkyl radicals containing at least three carbon atoms; andn and n' are independently selected from whole numbers having a value of from 0 to 4 inclusive.These copolyester-carbonates are useful in making molded articles, films, and the like.

    Abstract translation: 衍生自碳酸酯前体的芳族共聚酯 - 碳酸酯，至少一种双官能羧酸或其活性衍生物，以及由通式（IMAGE）表示的至少一种支链亚烷基二元酚，其中：R和R'独立地选自卤素和 一价烃基; R1和R3独立地选自氢和烷基; R2选自烷基，条件是如果R 1和R 3均为氢，则R 2选自含有至少三个碳原子的支链烷基; n和n'独立地选自0〜4的整数。 这些共聚酯 - 碳酸酯可用于制造模塑制品，薄膜等。

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