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    Solvent-free alkane sulfonation
    1.
    发明授权
    Solvent-free alkane sulfonation 有权

    公开(公告)号：US10961182B2

    公开(公告)日：2021-03-30

    申请号：US16349113

    申请日：2017-11-27

    Applicant: BASF SE

    Inventor： Timo Ott ,  Ingo Biertümpel

    IPC: C07C303/06 ,  C07C409/44 ,  C07C303/44 ,  C07C309/04 ,  C07C407/00

    Abstract: The present invention relates to an alkane-sulfonation process using alkane and sulfur trioxide, especially pure sulfur trioxide (100%) under solvent-free conditions in the presence of an initiator. It further relates to the use of a precursor which forms “in-situ” an initiator for manufacturing of alkanesulfonic acids, especially methanesulfonic acids.

    Methods and compositions relating to insect repellents from a novel endophytic fungus
    3.
    发明授权
    Methods and compositions relating to insect repellents from a novel endophytic fungus 失效
    与新生内生真菌的驱虫剂相关的方法和组合物

    公开(公告)号：US07267975B2

    公开(公告)日：2007-09-11

    申请号：US10687546

    申请日：2003-10-15

    Applicant: Gary Strobel ,  Bryn Daisy

    Inventor： Gary Strobel ,  Bryn Daisy

    IPC: A01N25/00 ,  A01N63/00 ,  A01N63/04 ,  A01N65/00 ,  C12N1/00 ,  C12P1/02 ,  C12P7/00 ,  C07C409/44

    CPC classification number: C12R1/645 ,  A01N63/04 ,  C12P5/005 ,  Y10S435/911

    Abstract: The present invention relates to the discovery of a novel endophytic fungus, Muscodor vitigenus, from the liana, Paullinia paullinioides. This fungus produces naphthalene under certain cultural conditions that has chromatographic and mass spectral properties that are identical to authentic naphthalene. In a preferred embodiment, the naphthalene in the gas phase of M. vitigenus is useful in the repellency of unwanted insect pests. The unique biological activity of the novel endophyte suggests a wide range of potential practical applications, particularly in the area of insect repellents, insecticides, antimicrobials, anthelmintics and vermicides.

    Abstract translation: 本发明涉及一种新颖的内生真菌，来自木犀草的保护性痢疾杆菌（Paillinia paullinioides）。 这种真菌在某些文化条件下产生萘，其色谱和质谱光谱性质与真正的萘相同。 在优选的实施方案中，维生素M.的气相中的萘可用于不期望的害虫的排斥。 新型内生真菌的独特生物活性表明广泛的潜在实际应用，特别是在驱虫剂，杀虫剂，抗微生物剂，驱肠虫剂和杀真菌剂方面。

    Peroxidic perfluoropolyethers
    4.
    发明申请
    Peroxidic perfluoropolyethers 有权
    过氧化全氟聚醚

    公开(公告)号：US20050197469A1

    公开(公告)日：2005-09-08

    申请号：US11063976

    申请日：2005-02-24

    Applicant: Giuseppe Marchionni ,  Pier Guarda

    Inventor： Giuseppe Marchionni ,  Pier Guarda

    IPC: C07C407/00 ,  C07C409/20 ,  C07C409/42 ,  C08G65/00 ,  C08G65/30 ,  C08G65/32 ,  C08G65/332 ,  C08G65/334 ,  C07C409/44 ,  C07C409/24 ,  C08G59/14

    CPC classification number: C08G65/32 ,  C08G65/007

    Abstract: Peroxidic perfluoropolyethers having formula: X1—O(CF2O)n1(CF2CF2O)m1(CF2(CF2)zCF2O)p1(O)h—X2  (I)wherein: X1 and X2, equal to or different from each other, are chain end groups selected among —CF2COF, —COF, —SO2F; n1, m1, p1 and h are integers such that the number average molecular weight is in the range 700-100,000; z=1 or 2; with the proviso that: the m1/n1 ratio is between 0.2 and 10; the p1/(n1+m1) ratio is lower than 0.05; the h/(n1+m1+p1) ratio is such that the PO content, defined as grams of active oxygen/100 g of compound, is in the range 0.8-4.5, preferably 1.4-3.8; the perfluorooxyalkylene units being statistically distributed along the polymeric chain.

    Abstract translation: 具有下式的过氧化全氟聚醚：<？in-line-formula description =“In-line Formulas”end =“lead”？> X 1 -O（CF 2 O） （CF 2）2（CF 2）2（CF 2）（CF 2）（CF 2） （O） > 2 <？in-line-formula description =“In-line Formulas”end =“tail”？>其中：X 1和X 2 < SUB>，彼此相同或不同，为选自-CF 2 COF，-COF，-SO 2 F的链端基; n1，m1，p1和h是数均分子量在700-100,000范围内的整数; z = 1或2; 条件是：m1 / n1比在0.2和10之间; p1 /（n1 + m1）比低于0.05; h /（n1 + m1 + p1）的比例使得定义为活性氧克数/ 100g化合物的PO含量在0.8-4.5，优选1.4-3.8的范围内; 全氟氧化烯单元沿着聚合物链统计分布。

    Process for preparing a sulfinate
    5.
    发明申请
    Process for preparing a sulfinate 失效
    亚磺酸盐的制备方法

    公开(公告)号：US20020013493A1

    公开(公告)日：2002-01-31

    申请号：US09891434

    申请日：2001-06-26

    Inventor： Takatugu Suzuki

    IPC: C07C409/44

    CPC classification number: C07C313/04

    Abstract: Disclosed is a process to prepare a sulfinate, which is useful for preparing a synthetic intermediate of an organic compound, especially for a color coupler, characterized by reducing a sulfonyl chloride with a sulfite or a hydrogensulfite in the presence of a hydrogenphosphate.

    Abstract translation: 公开了一种制备亚磺酸盐的方法，其可用于制备有机化合物的合成中间体，特别是用于着色成色剂，其特征在于在磷酸氢盐存在下用亚硫酸盐或亚硫酸氢盐还原磺酰氯。

    CONTINUOUS RECOVERY OF (METH)ACRYLIC ACID
    6.
    发明申请
    CONTINUOUS RECOVERY OF (METH)ACRYLIC ACID 失效
    （甲基）丙烯酸的连续回收

    公开(公告)号：US20010056204A1

    公开(公告)日：2001-12-27

    申请号：US09362912

    申请日：1999-07-29

    Inventor： OTTO MACHHAMMER ,  PETER ZEHNER ,  FILIP DEBERDT

    IPC: C07C409/44 ,  C07C051/42

    CPC classification number: C07C51/42 ,  C07C57/04

    Abstract: A process for the continuous recovery of (meth) acrylic acid from the reaction gases of a catalytic gas-phase oxidation by (I) absorption in a high-boiling solvent, (II) isolation of the (meth)acrylic acid from the mixture with the solvent and, if required, further purification of the (meth)acrylic acid isolated, (III) purification of the solvent and (IV) recycling of the purified solvent to absorption stage (I) is proposed, the temperature in each process stage not exceeding 155null C., in particular 140null C., preferably 120null C.

    Abstract translation: （I）在高沸点溶剂中的吸收从催化气相氧化的反应气体中连续回收（甲基）丙烯酸的方法，（II）从（甲基）丙烯酸与混合物的分离 溶剂，并且如果需要，进一步纯化分离的（甲基）丙烯酸，（III）溶剂的纯化和（IV）将纯化溶剂再循环至吸收级（I），每个过程阶段的温度不是 超过155℃，特别是140℃，优选120℃。

    Process for the preparation of N-carboxy-t-leucine anhydride
    7.
    发明申请
    Process for the preparation of N-carboxy-t-leucine anhydride 失效
    制备N-羧基-t-亮氨酸酐的方法

    公开(公告)号：US20010041812A1

    公开(公告)日：2001-11-15

    申请号：US09852849

    申请日：2001-05-11

    Applicant: DSM N.V.

    Inventor： Robert P. Hof ,  Wilhelmus Zwaan

    IPC: C07C409/44 ,  C07C053/00 ,  C07C057/00 ,  C07C059/00 ,  C07C061/00

    CPC classification number: C07D263/44

    Abstract: Process for the preparation of N-carboxy-t-leucine anhydride in which the corresponding N-carboxy-t-leucine is subjected to a cyclization with the aid of an acyl halogenide. Preferably, acetyl chloride is used as acyl halogenide. The N-carboxy-t-leucine anhydride obtained optionally is subsequently converted into a t-leucine-N-substituted amide with the aid of the corresponding amine. Preferably, methyl amine is chosen as the amine, and the reaction is carried out in a mixture of water and methanol as solvent.

    Abstract translation: N-羧基-t-亮氨酸酐的制备方法，其中相应的N-羧基-t-亮氨酸借助于酰基卤化物进行环化。 优选地，使用乙酰氯作为酰卤。 任选地获得的N-羧基-t-亮氨酸酐随后通过相应的胺转化成t-亮氨酸-N-取代的酰胺。 优选地，选择甲胺作为胺，并且反应在水和甲醇的混合物中作为溶剂进行。

    Frozen organic peroxide emulsion
    9.
    发明授权
    Frozen organic peroxide emulsion 失效
    冷冻有机过氧化物乳液

    公开(公告)号：US3988261A

    公开(公告)日：1976-10-26

    申请号：US599797

    申请日：1975-07-28

    Applicant: James A. Barter ,  Henry C. Stevens ,  John F. Van Hoozer

    Inventor： James A. Barter ,  Henry C. Stevens ,  John F. Van Hoozer

    IPC: C08F4/00 ,  B01F17/00 ,  C07C67/00 ,  C07C407/00 ,  C07C409/00 ,  C07C409/24 ,  C07C409/32 ,  C07C409/38 ,  C07C409/44 ,  C08F2/00 ,  C08F4/28 ,  C08F4/34

    CPC classification number: C08F4/34

    Abstract: A solid, frozen organic peroxide emulsion comprising from 30 to 75 weight percent organic peroxide, an emulsifying amount of surfactant(s) and the remainder water is described. Organic peroxides described include: dialkyl peroxydicarbonates, e.g., di-secondarybutyl peroxydicarbonate, diacyl peroxides, e.g., diisobutyryl peroxide, and acyl sulfonyl peroxides, e.g., acetylcyclohexylsulfonyl peroxide. The surfactant can be anionic, cationic, or nonionic, preferably nonionic, or mixtures of compatible surfactants.

    Abstract translation: 描述了包含30至75重量％有机过氧化物，乳化量的表面活性剂和其余水的固体，冷冻的有机过氧化物乳液。 所述的有机过氧化物包括：过氧化二碳酸二烷基酯，例如过氧化二碳酸二仲丁基酯，二酰基过氧化物，例如二异丁酰过氧化物和酰基磺酰基过氧化物，例如乙酰基环己基磺酰基过氧化物。 表面活性剂可以是阴离子的，阳离子的或非离子的，优选非离子的，或相容表面活性剂的混合物。

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