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公开(公告)号：US20040225155A1
公开(公告)日：2004-11-11
申请号：US10864263
申请日：2004-06-09
Applicant: Boehringer Ingelheim Pharma KG
Inventor： Oliver Meyer , Ingo Heddesheimer
IPC: C07C29/24
CPC classification number: C07C217/58
Abstract: Process for preparing vanillylamine or one of the salts thereof by reacting vanillin with hydroxylamine or the salts thereof in the presence of an organic salt, which may optionally be produced in situ, wherein the reaction is carried out in an inorganic or organic acid as diluent, and subsequently hydrogenating the resulting vanillyloxime with hydrogen in the presence of a suitable catalyst and an organic and/or inorganic acid.
Abstract translation: 通过香草醛与羟胺或其盐在有机盐存在下反应来制备香兰胺或其盐之一的方法，所述有机盐可以任意地原位制备，其中反应在无机或有机酸中作为稀释剂进行， 随后在合适的催化剂和有机和/或无机酸的存在下用氢氢化所得的钒酸肟。
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2.发明申请Process for preparing N-methyldialkylamines from secondary dialkylamines and formaldehyde 失效从仲二烷基胺和甲醛制备N-甲基二烷基胺的方法公开(公告)号：US20040204611A1
公开(公告)日：2004-10-14
申请号：US10804747
申请日：2004-03-19
Inventor： Peter Lappe , Helmut Springer
IPC: C07C29/24
CPC classification number: C07C209/28 , C07C211/07 , C07C211/08 , C07C211/21 , C07C211/27 , C07C211/35
Abstract: The present invention relates to a process for preparing N-methyldialkyl-amines by reacting secondary dialkylamines with formaldehyde at a temperature of from 100 to 200null C., by using from 1.5 to 3 mol of formaldehyde per mole of secondary dialkylamine and degassing the resulting reaction product, removing the aqueous phase and distilling the organic phase.
Abstract translation: 本发明涉及通过使仲胺二胺与甲醛在100〜200℃的温度下反应来制备N-甲基二烷基胺的方法，通过使用1.5至3摩尔甲醛/摩尔次级二烷基胺，并将所得 反应产物，除去水相并蒸馏出有机相。
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公开(公告)号：US20040171883A1
公开(公告)日：2004-09-02
申请号：US10794758
申请日：2004-03-05
Inventor： Heinz Steiner , Marc Thommen , Hans-Peter Jalett , Markus Benz
IPC: C07C29/24
CPC classification number: C07C209/26 , C07C209/52 , C07C2602/10 , C07C211/42
Abstract: The invention relates to a process for the cis-selective preparation of cyclic amines of the sertralin type by reductive alkylation of cyclic imines or their precursors and catalytic hydrogenation in the presence of copper-containing catalysts and in the presence of a protic solvent.
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公开(公告)号：US20040147762A1
公开(公告)日：2004-07-29
申请号：US10701081
申请日：2003-11-05
Inventor： Xumu Zhang
IPC: C07C29/24 , C07D207/00
CPC classification number: C07C211/27 , C07B2200/07 , C07C213/00 , C07C217/84
Abstract: Processes for the preparation of compounds having a chiral carbon substituted with an amine are disclosed. The processes include admixing a ketone with an amine in the presence of a catalyst having a chiral phosphine ligand and an acid. The admixture can also contain a reducing additive. The admixture is then exposed to hydrogen to directly and asymmetrically aminate the ketone.
Abstract translation: 公开了制备具有被胺取代的手性碳的化合物的方法。 所述方法包括在具有手性膦配体和酸的催化剂的存在下将酮与胺混合。 混合物还可以含有还原添加剂。 然后将混合物暴露于氢气以直接和不对称地胺化酮。
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5.发明授权Treatment of butanediol obtained as a condensate during the manufacture of polybutylene terephthalate 失效在制备聚对苯二甲酸丁二醇酯期间作为冷凝液获得的丁二醇的处理
公开(公告)号：US4154970A
公开(公告)日：1979-05-15
申请号：US913643
申请日：1978-06-08
Applicant: Ludwig Beer , Heinrich Mandel
Inventor： Ludwig Beer , Heinrich Mandel
Abstract: A process for treating butanediol obtained as a condensate during the manufacture of polybutylene terephthalate, wherein an alkali metal alcoholate or alkali metal hydride is added to the condensate at an elevated temperature. After purification, the butanediol obtained is re-used for the manufacture of polybutylene terephthalate.
Abstract translation: 在制备聚对苯二甲酸丁二醇酯期间作为冷凝物处理丁二醇的方法，其中在升高的温度下向冷凝物中加入碱金属醇盐或碱金属氢化物。 纯化后，所得的丁二醇被再次用于制造聚对苯二甲酸丁二醇酯。
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Patent Agency Ranking
公开(公告)号：US4128730A
公开(公告)日：1978-12-05
申请号：US759802
申请日：1977-01-14
Applicant: Manfred Reich
Inventor： Manfred Reich
CPC classification number: C07C45/002 , B01J23/755 , B01J23/868 , C07C27/22 , C07C45/54 , B01J21/08 , B01J37/0201 , B01J37/18
Abstract: The amount of formic acid ester produced by the Oxo Process is reduced and the amount of alcohol is increased when the reaction product of said process, in contact with a copper/nickel supported catalyst, is subjected to elevated temperatures. Such catalysts are also useful for the conversion, by hydrogenation, of formyl esters to their corresponding alcohols.
Abstract translation: 当所述方法与铜/镍负载的催化剂接触的反应产物经受高温时，由Oxo工艺生产的甲酸酯的量减少并且醇的量增加。 这样的催化剂也可用于通过氢化甲酰基酯与其相应的醇的转化。
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公开(公告)号：US4105701A
公开(公告)日：1978-08-08
申请号：US572238
申请日：1975-04-28
Applicant: Donald R. Larkin
Inventor： Donald R. Larkin
Abstract: A liquid contaminated with a carbonyl compound, especially an aldehyde, is purified by being contacted with a bed of solid polyvinyl alcohol particles or fibers. The carbonyl compound is adsorbed or chemisorbed onto the solid polyvinyl alcohol surface with resulting reaction in the carbonyl content of the liquid.
Abstract translation: 被羰基化合物，特别是醛污染的液体通过与固体聚乙烯醇颗粒或纤维床接触来纯化。 羰基化合物被吸附或化学吸附到固体聚乙烯醇表面上，导致液体羰基含量的反应。
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公开(公告)号：US4083931A
公开(公告)日：1978-04-11
申请号：US716555
申请日：1976-08-23
Applicant: Fu-Ming Lee
Inventor： Fu-Ming Lee
CPC classification number: C07C29/88
Abstract: A process for treating and recovering components from aldol-condensation polyol waste liquor containing sodium formate, water, polyol, and organic by-products comprising A. vacuum crystallizing and removing sodium formate; B. introducing methanol and sulfuric acid; C. distilling to remove and recover methyl formate; D. increasing the pH to about 6.5 to 7.0; E. cooling to precipitate Glauber's salt, polyol and organics; and F. adding water to dissolve and separate the Glauber's salt and recover substantially pure polyol and organics.
Abstract translation: 一种从含有甲酸钠，水，多元醇和有机副产物的醛醇缩合多元醇废液中处理和回收组分的方法，包括A.真空结晶和除去甲酸钠; B.引入甲醇和硫酸; 蒸馏除去并回收甲酸甲酯; D.将pH值提高至约6.5-7.0; E.冷却以沉淀芒硝，多元醇和有机物; 和F.加水以溶解并分离芒硝的盐并回收基本上纯的多元醇和有机物。
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公开(公告)号：US4062900A
公开(公告)日：1977-12-13
申请号：US705718
申请日：1976-07-15
Applicant: Yasuo Tanabe , Jun Toriya , Masato Sato , Ken Shiraga
Inventor： Yasuo Tanabe , Jun Toriya , Masato Sato , Ken Shiraga
IPC: C07C27/26 , C07C27/00 , C07C27/02 , C07C29/74 , C07C29/92 , C07C31/18 , C07C31/20 , C07C33/035 , C07C67/00 , C07C29/24
CPC classification number: C07C31/18
Abstract: Butanediol and/or butenediol are prepared by hydrolyzing diacetoxybutane and/or diacetoxybutene in the presence of a cation-exchange resin and recovered by fractional distillation. By the treatment of the hydrolyzed product with an anion exchange resin at any stage before the butanediol and/or butenediol are fractionated, butanediol and/or butenediol are recovered in high yield.
Abstract translation: 丁二醇和/或丁烯二醇通过在阳离子交换树脂的存在下水解二乙酰氧基丁烷和/或二乙酰氧基丁烯并通过分馏回收来制备。 通过在丁二醇和/或丁烯二醇分馏之前的任何阶段用阴离子交换树脂处理水解产物，以高收率回收丁二醇和/或丁烯二醇。
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10.发明授权Recovery of alkylene glycols by azeotropic distillation with 1,2,3-trimethyl benzene 失效用1,2,3-三甲基苯共沸蒸馏回收亚烷基二醇
公开(公告)号：US4021311A
公开(公告)日：1977-05-03
申请号：US612826
申请日：1975-09-12
Applicant: Mitchell Becker
Inventor： Mitchell Becker
CPC classification number: C07C29/82
Abstract: Ethylene glycol or 1,2-propylene glycol contained in mixtures with lower carboxylate esters of the glycol is recovered by azeotropic distillation of the mixtures with 1,2,3-trimethyl benzene.
Abstract translation: 通过与1,2,3-三甲基苯共混蒸馏回收与二醇的低级羧酸酯的混合物中所含的乙二醇或1,2-丙二醇。
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