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    CRYSTALLINE MATERIAL AND MEMBRANE COMPLEX
    1.
    发明申请
    CRYSTALLINE MATERIAL AND MEMBRANE COMPLEX 有权

    公开(公告)号：US20210340016A1

    公开(公告)日：2021-11-04

    申请号：US17305674

    申请日：2021-07-13

    申请人： NGK INSULATORS, LTD.

    发明人： Makoto MIYAHARA ,  Kenichi NODA

    IPC分类号： C01B37/04 ,  C01B37/08 ,  C01B37/06 ,  B01J20/18 ,  B01J20/02 ,  B01J20/28 ,  B01D71/02 ,  B01D69/14

    摘要： A crystalline material contains oxygen, aluminum and phosphorus, and has powder X-ray diffraction peaks shown below. When the peak at 2θ=14.17±0.2° is used as the reference peak and the intensity of the reference peak is set to 100, for example, the relative intensity of the peak at 2θ=8.65±0.2° is 1 to 15. The relative intensity of the peak at 2θ=9.99±0.2° is 1 to 15. The relative intensity of the peak at 2θ=16.52±0.2° is 5 to 80. The relative intensity of the peak at 2θ=17.37±0.2° is 1 to 15. The relative intensity of the peak at 2θ=21.81±0.2° is 10 to 80.

    Synthesis of SAPO-34 with essentially pure CHA framework
    2.
    发明授权
    Synthesis of SAPO-34 with essentially pure CHA framework 有权
    用基本纯CHA框架合成SAPO-34

    公开(公告)号：US07578987B2

    公开(公告)日：2009-08-25

    申请号：US11157102

    申请日：2005-06-20

    申请人： Stephen T. Wilson

    发明人： Stephen T. Wilson

    IPC分类号： C01B39/54 ,  C01B37/06 ,  C01B37/08

    CPC分类号： C07C1/20 ,  B01J29/84 ,  B01J29/85 ,  C01B39/54 ,  Y02P20/52 ,  Y02P30/42 ,  Y10S423/30 ,  C07C11/06 ,  C07C11/04 ,  C07C11/02

    摘要： A process for producing an ElAPO molecular sieve with essentially pure CHA framework having an average crystal size less than about 5 micrometers is disclosed. When El is silicon, the process allows for a broad range of silicon content, and produces a catalyst with a high selectivity for the conversion of methanol to olefins. The process includes making a crystalline metallo-aluminophosphate molecular sieve of the formula (ElxAlyPz)O2from a mixture comprising an aluminum source, a phosphorous source, water, an El source, a fluorine source and an organic template source wherein the molar ratio of the organic template source to phosphorous is less than about 0.5; crystallizing the molecular sieve at a temperature between 100 C and 250 C and calcining in air.

    摘要翻译： 公开了具有平均晶体尺寸小于约5微米的具有基本上纯CHA骨架的ElAPO分子筛的方法。 当El是硅时，该方法允许宽范围的硅含量，并产生具有高甲醇转化为烯烃的高选择性的催化剂。 该方法包括从包含铝源，磷源，水，El源，氟源和有机模板源的混合物制备式（ElxAlyPz）O 2的结晶金属铝磷酸盐分子筛，其中有机 模板源到磷小于约0.5; 在100℃和250℃之间的温度下使分子筛结晶并在空气中煅烧。

    Crystalline manganese phosphate compositions
    3.
    发明授权
    Crystalline manganese phosphate compositions 失效
    结晶磷酸锰组合物

    公开(公告)号：US5780003A

    公开(公告)日：1998-07-14

    申请号：US707986

    申请日：1996-08-23

    申请人： Gregory J. Lewis

    发明人： Gregory J. Lewis

    IPC分类号： B01J27/187 ,  C01B25/37 ,  C01B37/00 ,  C01B37/06 ,  C07C11/04 ,  C07C11/06 ,  C07C45/00 ,  C07D307/89 ,  B01J27/18 ,  B01J27/185

    CPC分类号： C01B37/065 ,  B01J27/187 ,  C01B37/002

    摘要： A new family of crystalline manganese phosphate compositions has been prepared. These compositions have an extended network which network can be a one-, two-, or three-dimensional network. The composition has an empirical formula of: (A.sup.a+).sub.v (Mn.sup.b+)(M.sup.c+).sub.x P.sub.y O.sub.z where A is a templating agent such as an alkali metal, M is a metal such as Al, Fe.sup.3+ and "b" is the average manganese oxidation state and varies from greater than 3.0 to about 4.0. These compositions can be used as adsorbents and as catalysts in the oxidation of hydrocarbons.

    摘要翻译： 已经制备了一种新的结晶磷酸锰组合物。 这些组合物具有扩展网络，其网络可以是一维，二维或三维网络。 该组合物具有以下经验式：（Aa +）v（Mnb +）（Mc +）xPyOz其中A为模板剂如碱金属，M为金属如Al，Fe3 +，“b”为平均锰氧化态， 从大于3.0到大约4.0。 这些组合物可用作烃的氧化中的吸附剂和催化剂。

    Synthesis of novel molecular sieves using a metal complex as a template
    5.
    发明授权
    Synthesis of novel molecular sieves using a metal complex as a template 失效
    使用金属络合物作为模板合成新的分子筛

    公开(公告)号：US5648058A

    公开(公告)日：1997-07-15

    申请号：US439415

    申请日：1995-05-11

    申请人： Kenneth J. Balkus, Jr. ,  Alexi G. Gabrielov

    发明人： Kenneth J. Balkus, Jr. ,  Alexi G. Gabrielov

    IPC分类号： B01J29/064 ,  B01J29/83 ,  C01B37/02 ,  C01B37/06 ,  C01B37/08

    CPC分类号： C01B37/08 ,  C01B37/02 ,  C01B37/06 ,  Y10S423/30

    摘要： The synthesis and characterization of novel molecular sieves containing bis(pentamethylcyclopentadienyl) cobalt(III) ion are described. Several types of molecular sieves were prepared using the cobalt metal complex as a template that was shown to be incorporated as a guest molecule within the molecular sieve. Molecular sieves prepared using bis(pentamethylcyclopentadienyl) cobalt(III) ion as template were characterized as having a pore size at least as large as 7 .ANG.. Other molecular sieves were also prepared using bis(cyclopentadienyl) cobalt(III) templates. The compounds are attractive as catalysts in a wide range of applications.

    摘要翻译： 描述了含有双（五甲基环戊二烯基）钴（III）离子的新型分子筛的合成和表征。 使用钴金属络合物作为模板制备了几种类型的分子筛，该模板显示作为客体分子掺入分子筛中。 使用双（五甲基环戊二烯基）钴（III）离子作为模板制备的分子筛的特征在于具有至少大于7安培的孔径。 其他分子筛也使用双（环戊二烯基）钴（III）模板制备。 该化合物在广泛的应用中作为催化剂是有吸引力的。

    Crystalline aluminophosphates compositions
    6.
    发明授权
    Crystalline aluminophosphates compositions 失效
    结晶磷酸铝组合物

    公开(公告)号：US5049366A

    公开(公告)日：1991-09-17

    申请号：US468307

    申请日：1990-01-22

    申请人： David M. Clark ,  Ronald J. Dogterom

    发明人： David M. Clark ,  Ronald J. Dogterom

    IPC分类号： B01J20/02 ,  B01J27/18 ,  B01J29/83 ,  B01J29/84 ,  B01J29/85 ,  C01B25/36 ,  C01B35/12 ,  C01B35/14 ,  C01B37/04 ,  C01B37/06 ,  C01B37/08 ,  C01B39/54

    CPC分类号： C01B37/08 ,  B01J29/83 ,  B01J29/84 ,  B01J29/85 ,  C01B35/1009 ,  C01B37/04 ,  C01B37/065

    摘要： Crystalline aluminophosphates and related compounds having in the as-synthesized anhydrous form the chemical composition:m'R(X.sub.n Al.sub.q P.sub.x)O.sub.2, wherein R represents ethylenediamine, X represents one or more elements which can be substituted for Al and/or P, whereinm'=0.01-0.33n=0-0.50q=0.30-0.60x=0.30-0.60and wherein n+q+x=1.The compounds can be prepared from a forming solution or gel comprising a source of aluminum, a source of phosphorus, ethylenediamine and optionally a source of at least one component X, which mixture is kept at elevated temperature for a period of time sufficient to produce a crystalline aluminophosphate or related compound followed by separating off the crystalline product obtained and drying, and which may subsequently be calcined.

    摘要翻译： 具有合成无水形式的结晶铝磷酸盐和相关化合物形成化学组成：m'R（XnAlqPx）O 2，其中R表示乙二胺，X表示可替代Al和/或P的一种或多种元素，其中m' = 0.01-0.33 n = 0-0.50 q = 0.30-0.60 x = 0.30-0.60，其中n + q + x = 1。 化合物可以由包含铝源，磷源，乙二胺和任选的至少一种组分X的源的成形溶液或凝胶制备，该混合物在高温下保持足以产生足够的时间 结晶磷酸铝或相关化合物，然后分离所得结晶产物并干燥，随后可煅​​烧。

    Quinary molecular sieve compositions
    8.
    发明授权
    Quinary molecular sieve compositions 失效
    五元分子筛组合物

    公开(公告)号：US4956164A

    公开(公告)日：1990-09-11

    申请号：US63791

    申请日：1987-06-22

    申请人： Brent M. T. Lok ,  Bonita K. Marcus ,  Edith M. Flanigen

    发明人： Brent M. T. Lok ,  Bonita K. Marcus ,  Edith M. Flanigen

    IPC分类号： B01J29/85 ,  C01B37/06 ,  C01B37/08 ,  C07C2/12 ,  C07C2/54 ,  C07C5/02 ,  C07C5/22 ,  C07C5/27 ,  C07C5/41

    CPC分类号： C07C5/41 ,  B01J29/85 ,  C01B37/06 ,  C01B37/08 ,  C07C2/12 ,  C07C2/54 ,  C07C5/02 ,  C07C5/224 ,  C07C5/2716 ,  C07C2527/173 ,  C07C2529/84 ,  Y10S423/30

    摘要： Molecular sieves having three-dimensional microporous framework structures of CoO.sub.2, MnO.sub.2, AlO.sub.2, PO.sub.2, and SiO.sub.2 tetrahedral oxide units are disclosed. These molecular sieves have an empirical chemical composition on an anhydrous basis are expressed by the formula:mR: (Co.sub.u Mn.sub.v Al.sub.x P.sub.y Si.sub.z)O.sub.2wherein "R" represents at least one organic templating agent present in the intracrystalline pore system; "m" represents the molar amount of "R" present per mole of (Co.sub.u Mn.sub.v Al.sub.x P.sub.y Si.sub.z)O.sub.2 ; and "u", "v", "x", "y" and "z" represent the mole fractions of cobalt, manganese, aluminum, phosphorus and silicon, respectively, present as tetrahedral oxides. Their use as adsorbents, catalysts, etc. is disclosed.

    摘要翻译： 公开了具有CoO 2，MnO 2，AlO 2，PO 2和SiO 2四面体氧化物单元的三维微孔骨架结构的分子筛。 这些分子筛具有无水基的经验化学组成由下式表示：mR：（CouMnvAlxPySiz）O 2，其中“R”表示存在于晶体内孔系统中的至少一种有机模板剂; “m”表示每摩尔（CouMnvAlxPySiz）O 2存在的“R”摩尔量; 和“u”，“v”，“x”，“y”和“z”分别表示作为四面体氧化物存在的钴，锰，铝，磷和硅的摩尔分数。 公开了它们作为吸附剂，催化剂等的用途。