Process for preparing substituted aminoanthraquinones
    1.
    发明授权
    Process for preparing substituted aminoanthraquinones 失效
    制备取代氨基蒽醌的方法

    公开(公告)号:US5017713A

    公开(公告)日:1991-05-21

    申请号:US433784

    申请日:1989-11-08

    CPC classification number: C09B1/36 C09B1/26 C09B1/28

    Abstract: Substituted aminoanthraquinone compounds, which are used for dye stuffs or intermediate thereof, represented by the formula (II) ##STR1## wherein R.sub.3 represents a C.sub.1 -C.sub.6 alkyl group which may be substituted, X represents a hydrogen atom, --COR.sub.1 or --SO.sub.2 R.sub.2 wherein R.sub.1 and R.sub.2 each represents a substituted or unsubstituted C.sub.1 -C.sub.4 alkyl or C.sub.6 -C.sub.12 aryl group, and Y and Z represent independently a hydrogen atom, a halogen atom, a nitro group or a C.sub.1 -C.sub.4 alkyl group, is prepared by allowing anthraquinone compounds represented by the formula ##STR2## wherein X, Y and Z are as defined above, to react with alkylating agents in organic solvents in the presence of organic quaternary ammonium salts and alkalies.

    Process for the manufacture of aminoanthraquinones
    3.
    发明授权
    Process for the manufacture of aminoanthraquinones 失效
    制备氨基蒽醌的方法

    公开(公告)号:US4076735A

    公开(公告)日:1978-02-28

    申请号:US612811

    申请日:1975-09-12

    Applicant: Zdenek Seha

    Inventor: Zdenek Seha

    CPC classification number: C09B1/28 C09B1/303

    Abstract: A process for the manufacture of aminoanthraquinones, wherein nitroanthraquinones are reacted in dipolar aprotic solvents which contain --SO.sub.2 -- or --SO-- groups and are inert to the reactants, with aliphatic, aliphatic-aromatic, cycloaliphatic, substituted or unsubstituted primary or secondary amines of the formulae R--NH.sub.2 or R--R'--NH, in which R and R' are radicals that are the same or different, such as alkyl, aralkyl, cycloalkyl, hydroxyalkyl radicals of 1 to 8 carbon atoms.

    Abstract translation: 制备氨基蒽醌的方法,其中硝基蒽醌在含有-SO 2 - 或-SO-基团并对反应物惰性的偶极非质子溶剂中与脂族,脂族 - 芳族,脂环族,取代或未取代的伯或仲胺反应 式R-NH 2或R-R'-NH,其中R和R'是相同或不同的基团,例如具有1至8个碳原子的烷基,芳烷基,环烷基,羟基烷基。

    Process for the preparation of dyestuff compositions

    公开(公告)号:US4061464A

    公开(公告)日:1977-12-06

    申请号:US620385

    申请日:1975-10-07

    Abstract: A process for the preparation of new dyestuff compositions which contain one or more basic dyestuffs in the form of dyestuff bases from the series of the triarylmethane, indoldiarylmethane, azine, oxazine, thiazine or xanthene dyestuffs or one or more basic dyestuffs of the series of the azo, anthraquinone, phthalocyanine, styryl, quinophthalone, benzoxanthene, naphthoylene-benzimidazole, naphthalimide or nitro series, carrying a primary, secondary or tertiary amino group or a guanidino or hydrazino group, as well as one or more non-ionic or slightly cationic surface-active agents and, optionally, water and/or an organic solvent miscible with water, which process comprises synthesizing the dyestuff in the surface-active agent optionally containing water and/or an organic solvent miscible with water, and then adding, if necessary, water and/or a solvent miscible with water and a further surface-active agent, this process of the invention having the advantage that an intermediate isolation, drying or grinding of the dyestuffs contained in the dyestuff compositions defined above is not necessary, so that the dyestuffs need not be introduced as substance into the surface-active agent and the solvent in a process wherein compositions of this type are prepared by a usual mixing, kneading or melting process; moreover, higher dyestuff yields are obtained in the dyestuff synthesis, and it allows to prepare dyestuff compositions from dyestuffs which are difficult to be isolated in substance after synthesis and often precipitate as oily or smeary products. The dyestuff compositions obtained according to the process of the invention, which are pastes or liquids, have a high stability upon storage. After being diluted with an aqueous solution of an amount at least equivalent to the dyestuff of an inorganic or organic acid, as well as, optionally, after the addition of dyeing and/or printing auxiliaries, the novel dyestuff compositions are suitable for dyeing or printing textile material containing acid groups.

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