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    Device for optical and electrochemical measurements in microliter size samples
    4.
    发明授权
    Device for optical and electrochemical measurements in microliter size samples 有权
    用于在微升尺寸样品中进行光学和电化学测量的装置

    公开(公告)号：US6043878A

    公开(公告)日：2000-03-28

    申请号：US147986

    申请日：1999-07-09

    申请人： Miklos Gratzl ,  Andrea Cserey ,  Kwong Yue Hui

    发明人： Miklos Gratzl ,  Andrea Cserey ,  Kwong Yue Hui

    IPC分类号： B01F13/00 ,  B01F13/02 ,  B01L3/00 ,  G01N21/79 ,  G01N27/403 ,  G01N35/00 ,  G01N35/10 ,  G01N1/10

    CPC分类号： B01F13/0272 ,  B01F13/0071 ,  B01F13/0093 ,  B01L3/5088 ,  G01N21/79 ,  B01F13/0084 ,  B01L2300/0645 ,  B01L2400/0472 ,  B01L3/5027 ,  G01N2035/00237 ,  G01N2035/00287 ,  G01N2035/1034

    摘要： A small liquid sample (24) to be tested is contained within an annulus (18) on the upper surface (14) of a substrate (12). In one embodiment, a reagent diffuses into the sample through a membrane (28) in a junction hole (26), the junction hole connecting upper (14) and lower (16) surfaces of the substrate. Optical measuring equipment (70, 72) detects a measurable change in an optical property of the sample. In an alternate embodiment, a flow of gas (30), directed at the small liquid sample (24), causes the sample to flow in a controlled manner over the surface of an electrode (20), disposed on the substrate surface (14). In another alternate embodiment, a special averaging electrode (20) is disposed in a non-homogeneous sample (24). Highly reproducible and accurate hydrodynamic electrochemical studies and analyses of microliter size samples are thus achievable, without the need for moving mechanical parts.

    摘要翻译： PCT No.PCT / US97 / 17067 Sec。 371日期1999年7月9日 102（e）日期1999年7月9日PCT 1997年9月24日PCT公布。 第WO98 / 13675号公报 日期1998年4月2日待测试的小液体样品（24）被包含在衬底（12）的上表面（14）上的环形空间（18）中。 在一个实施方案中，试剂通过连接孔（26）中的膜（28）扩散到样品中，连接孔连接衬底的上部（14）和下部（16）表面。 光学测量设备（70,72）检测样品的光学特性的可测量的变化。 在替代实施例中，指向小液体样品（24）的气体流（30）使得样品以受控的方式流过设置在基底表面（14）上的电极（20）的表面， 。 在另一替代实施例中，特殊平均电极（20）设置在非均匀样品（24）中。 因此，可以实现高度可重复和准确的微动态电化学研究和微升尺寸样品的分析，而不需要移动机械部件。

    CHEMICAL ANALYZER
    6.
    发明申请
    CHEMICAL ANALYZER 失效
    化学分析仪

    公开(公告)号：US20130121883A1

    公开(公告)日：2013-05-16

    申请号：US13738555

    申请日：2013-01-10

    申请人： HITACHI HIGH-TECHNOLOGIES CORPORATION

    发明人： Hironobu YAMAKAWA ,  Yoichi ARUGA ,  Takenori OKUSA ,  Taisaku SEINO

    IPC分类号： G01N33/50

    CPC分类号： G01L9/00 ,  B01F13/0272 ,  B01L3/508 ,  B01L3/5085 ,  B01L99/00 ,  B01L2300/0636 ,  B01L2300/0822 ,  B01L2300/0829 ,  B08B9/035 ,  B08B9/0817 ,  G01L9/0041 ,  G01N33/50 ,  G01N35/025 ,  G01N2035/00544 ,  G01N2035/0437 ,  Y10T436/2575

    摘要： An automatic chemical analyzer in which a reaction solution is stirred by air ejected from an air ejection hole placed above a reaction container. The reaction region can be washed and cleaned sufficiently without causing damage, such as exfoliation of a coating reagent. A reaction container disk is provided with a pore and a pressure detector connected with the pore. Before and after the stirring operation, the ejection hole (nozzle) ejecting air is moved and the output value of the pressure detector is compared with a previously measured normal value. With a discharge pipe and a suction pipe inserted to the opening of the reaction container to be close to both ends of the opening and the side wall of the container, the reaction region at the bottom of the container is washed by continuous discharge and suction of cleaning fluid.

    摘要翻译： 一种自动化学分析仪，其中反应溶液被从放置在反应容器上方的空气喷射孔喷出的空气搅拌。 可以充分洗涤和清洁反应区域而不会引起诸如涂层试剂剥落的损伤。 反应容器盘设置有孔和与孔相连的压力检测器。 在搅拌操作之前和之后，移动喷射孔（喷嘴）喷射空气，并将压力检测器的输出值与先前测量的正常值进行比较。 通过将排出管和吸入管插入反应容器的开口以接近容器的开口和侧壁的两端，容器底部的反应区域通过连续排出和抽吸 清洗液

    CHEMICAL ANALYZER
    7.
    发明申请
    CHEMICAL ANALYZER 有权
    化学分析仪

    公开(公告)号：US20120107180A1

    公开(公告)日：2012-05-03

    申请号：US13201491

    申请日：2010-02-22

    申请人： Hironobu Yamakawa ,  Yoichi Aruga ,  Takenori Okusa ,  Kenichi Takahashi ,  Taisaku Seino

    发明人： Hironobu Yamakawa ,  Yoichi Aruga ,  Takenori Okusa ,  Kenichi Takahashi ,  Taisaku Seino

    IPC分类号： G01N33/50

    CPC分类号： G01L9/00 ,  B01F13/0272 ,  B01L3/508 ,  B01L3/5085 ,  B01L99/00 ,  B01L2300/0636 ,  B01L2300/0822 ,  B01L2300/0829 ,  B08B9/035 ,  B08B9/0817 ,  G01L9/0041 ,  G01N33/50 ,  G01N35/025 ,  G01N2035/00544 ,  G01N2035/0437 ,  Y10T436/2575

    摘要： An automatic chemical analyzer in which a reaction solution is stirred by air ejected from an air ejection hole placed above a reaction container. The reaction region can be washed and cleaned sufficiently without causing damage, such as exfoliation of a coating reagent. A reaction container disk 161 is provided with a pore 240 and a pressure detector 241 connected with the pore. Before and after the stirring operation, the ejection hole (nozzle) 170 ejecting air is moved and the output value of the pressure detector is compared with a previously measured normal value. With a discharge pipe 1101 and a suction pipe 1102 inserted to the opening of the reaction container 1140 to be close to both ends of the opening and the side wall of the container, the reaction region 1150 at the bottom of the container is washed by continuous discharge and suction of cleaning fluid.

    摘要翻译： 一种自动化学分析仪，其中反应溶液被从放置在反应容器上方的空气喷射孔喷出的空气搅拌。 可以充分洗涤和清洁反应区域而不会引起诸如涂层试剂剥落的损伤。 反应容器盘161设置有与孔连通的孔240和压力检测器241。 在搅拌操作之前和之后，喷射空气的喷射孔（喷嘴）170移动，并将压力检测器的输出值与先前测量的正常值进行比较。 通过将排出管1101和吸入管1102插入到反应容器1140的开口中以接近容器的开口和侧壁的两端，容器底部的反应区域1150被连续地洗涤 清洗液的排放和抽吸。

    Fluidized bed systems and methods including micro-jet flow
    8.
    发明授权
    Fluidized bed systems and methods including micro-jet flow 有权
    流化床系统和方法包括微喷流

    公开(公告)号：US08118243B2

    公开(公告)日：2012-02-21

    申请号：US11937736

    申请日：2007-11-09

    申请人： Robert Pfeffer ,  Jose A. Quevedo ,  Juergen Flesch

    发明人： Robert Pfeffer ,  Jose A. Quevedo ,  Juergen Flesch

    IPC分类号： B02C19/00

    CPC分类号： B01J8/32 ,  B01F3/18 ,  B01F13/02 ,  B01F13/0272 ,  B01J8/1818 ,  B01J8/1872 ,  B82Y15/00 ,  B82Y30/00

    摘要： Methods and systems for enhancing fluidization of nanoparticle and/or nanoagglomerates are provided. A fluidization chamber is provided with a fluidizing medium directed in a first fluidizing direction, e.g., upward into and through a bed containing a volume of nanoparticles and/or nanopowders. A second source of air/gas flow is provided with respect to the fluidization chamber, the secondary air/gas flow generally being oppositely directed relative to the fluidizing medium. Turbulence created by the secondary gas flow is advantageously effective to aerate the agglomerates and the shear generated by the jet is advantageously effective to break apart nanoagglomerates and/or reduce the tendency for nanoagglomerates to form or reform. A downwardly directed source of secondary gas flow located near the main gas distributor leads to full fluidization of the entire amount of powder in the column. The oppositely directed fluid flow facilitates powder circulation within the fluidization chamber, thereby enhancing fluidization results.

    摘要翻译： 提供了用于增强纳米颗粒和/或纳米团聚体的流化的方法和系统。 流化室设置有以第一流化方向（例如向上）流入并穿过含有一定体积纳米颗粒和/或纳米粉末的床的流化介质。 相对于流化室提供第二气/气流源，二次空气/气流通常相对于流化介质相反地定向。 由二次气流产生的湍流有利于使附聚物充气，并且由射流产生的剪切有利于有效地分离纳米颗粒和/或降低纳米颗粒形成或改性的倾向。 位于主气体分配器附近的向下定向的二次气流源导致柱中全部粉末的充分流化。 相反导向的流体流动促进流化室内的粉末循环，从而增强流化结果。

    Fluidized Bed Systems And Methods Including Micro-Jet Flow
    10.
    发明申请
    Fluidized Bed Systems And Methods Including Micro-Jet Flow 有权
    流化床系统和包括微喷流的方法

    公开(公告)号：US20080179433A1

    公开(公告)日：2008-07-31

    申请号：US11937736

    申请日：2007-11-09

    申请人： Robert Pfeffer ,  Jose A. Quevedo ,  Juergen Flesch

    发明人： Robert Pfeffer ,  Jose A. Quevedo ,  Juergen Flesch

    IPC分类号： B02C19/06

    CPC分类号： B01J8/32 ,  B01F3/18 ,  B01F13/02 ,  B01F13/0272 ,  B01J8/1818 ,  B01J8/1872 ,  B82Y15/00 ,  B82Y30/00

    摘要： Methods and systems for enhancing fluidization of nanoparticle and/or nanoagglomerates are provided. A fluidization chamber is provided with a fluidizing medium (e.g., a fluidizing gas) directed in a first fluidizing direction, e.g., upward into and through a bed containing a volume of nanoparticles and/or nanopowders. A second source of air/gas flow is provided with respect to the fluidization chamber, the secondary air/gas flow generally being oppositely (or substantially oppositely) directed relative to the fluidizing medium. Turbulence created by the secondary gas flow, e.g., a jet from a micro-jet nozzle, is advantageously effective to aerate the agglomerates and the shear generated by the jet is advantageously effective to break apart nanoagglomerates and/or reduce the tendency for nanoagglomerates to form or reform. A downwardly directed source of secondary gas flow located near the main gas distributor leads to full fluidization of the entire amount of powder in the column. In addition, the oppositely directed fluid flow facilitates powder circulation within the fluidization chamber, thereby enhancing fluidization results. Use of oppositely directed fluid flow is believed to transition a bed that is exhibiting agglomerate bubbling fluidization (ABF) behavior into a bed that exhibits agglomerate particulate fluidization (APF) behavior

    摘要翻译： 提供了用于增强纳米颗粒和/或纳米团聚体的流化的方法和系统。 流化室设置有以第一流化方向（例如向上）引导入并穿过含有一定体积的纳米颗粒和/或纳米粉末的床的流化介质（例如，流化气体）。 相对于流化室设置第二气/气流源，二次空气/气体流通常相对于流化介质相反（或大致相反地）流动。 由次级气流产生的湍流，例如来自微喷嘴的射流，有利于使附聚物充气，并且由射流产生的剪切有利于有效地分离纳米团聚体和/或降低纳米颗粒形成的趋势 或改革。 位于主气体分配器附近的向下定向的二次气流源导致柱中全部粉末的充分流化。 此外，相反导向的流体流动促进流化室内的粉末循环，从而增强流化结果。 认为使用相反导向的流体流动将使附聚发泡流化（ABF）行为的床转变为显示附聚颗粒流化（APF）行为的床