PROCESS AND DEVICE FOR SIMULATED MOVING BED ADSORPTION AND SEPARATION WITH A REDUCED NUMBER OF CONTROL VALVES
    2.
    发明申请
    PROCESS AND DEVICE FOR SIMULATED MOVING BED ADSORPTION AND SEPARATION WITH A REDUCED NUMBER OF CONTROL VALVES 审中-公开
    用于模拟移动床吸附和分离与控制阀数量减少的过程和装置

    公开(公告)号:US20140224742A1

    公开(公告)日:2014-08-14

    申请号:US14131955

    申请日:2012-07-16

    IPC分类号: B01D15/18

    摘要: The present invention relates to a process for simulated moving bed (SMB) adsorption and separation with a reduced number of control valves, comprising separating the feedstocks comprising isomers by SMB adsorption, said SMB comprising m beds of adsorbent, each of which is equipped with grids, each of the grids being equipped with the materials charging and discharging pipeline of the bed, the materials charged into and discharged from SMB at least comprising adsorption feedstocks, desorbent, extract, raffinate and the flushing liquids charged from different beds, wherein the to extract is enriched with the target product; there are at least two streams of said flushing liquid selected from any one of the adsorption feedstock, desorbent, extract and raffinate; there are altogether n streams of materials charged to and discharged from the SMB, wherein there are s types of materials having the same composition and flow direction; p sets of on-off valves are used to control n streams of materials is charged to and discharged from the beds of adsorbent, wherein at least one group of materials composed of two streams of materials having the composition and flow direction is controlled by one set of valves, with s≦p

    摘要翻译: 本发明涉及一种具有减少数量的控制阀的模拟移动床(SMB)吸附和分离方法,包括通过SMB吸附分离包含异构体的原料,所述SMB包括多个吸附剂床,每个床装有栅格 每个网格配备有床的材料充放电管线,至少包含吸附原料,解吸剂,提取物,提余液和从不同床装入的冲洗液体的SMB中排出的材料,其中提取 富含目标产品; 从吸附原料,解吸剂,萃取液和萃余液中的任一种中选出至少两股所述冲洗液; 总共有N条物料流充入和排出SMB,其中有类型的材料具有相同的组成和流动方向; p组开关阀用于控制n个物料流从吸附剂床排出并排出,其中由具有组成和流动方向的两股材料组成的至少一组材料由一组控制 阀门,s≦̸ p

    Reduction In Flushing Volume In An Adsorptive Separation System
    3.
    发明申请
    Reduction In Flushing Volume In An Adsorptive Separation System 有权
    在吸附分离系统中减少冲洗量

    公开(公告)号:US20140031601A1

    公开(公告)日:2014-01-30

    申请号:US14045094

    申请日:2013-10-03

    发明人: John R. Porter

    IPC分类号: C07C7/13 B01D15/02

    摘要: A process for separating a product from a multicomponent feedstream to an adsorption apparatus or system is described. The apparatus or system may comprise a moving-bed or a simulated moving-bed adsorption means. The product comprises at least one organic compound, such as an aryl compound with alkyl substitutes. In embodiments the conduits used to supply the feedstream to the apparatus or system are flushed with media of multiple grades. The improvement is a more efficient use of the desorbent. In embodiments the process achieves improvements in one or more of efficiency of adsorption separation, capacity of adsorption apparatus systems, and purity of product attainable by adsorption process.

    摘要翻译: 描述了将产物从多组分进料流分离到吸附装置或系统的方法。 该装置或系统可包括移动床或模拟移动床吸附装置。 产物包含至少一种有机化合物,例如具有烷基取代基的芳基化合物。 在实施例中,用于将进料流供应到设备或系统的管道用多个等级的介质冲洗。 改进是更有效地使用解吸剂。 在实施方案中,该方法实现了吸附分离效率,吸附装置系统的容量和通过吸附过程可获得的产物的纯度中的一种或多种的改进。

    Flushing apparatus in a simulated mobile bed adsorption unit comprising two fluid distribution lines, and the use thereof
    6.
    发明授权
    Flushing apparatus in a simulated mobile bed adsorption unit comprising two fluid distribution lines, and the use thereof 失效
    包括两个流体分配管线的模拟移动床吸附单元中的冲洗装置及其用途

    公开(公告)号:US06284200B1

    公开(公告)日:2001-09-04

    申请号:US08985704

    申请日:1997-12-05

    申请人: Gerard Hotier

    发明人: Gerard Hotier

    IPC分类号: B01D5000

    CPC分类号: B01D15/1835 B01D15/1842

    摘要: A simulated moving bed flushing apparatus and its use are described. The adsorber comprises a plurality of beds (10, 11) of adsorbent, each bed being connected to a distribution means (5) comprising two fluid distribution lines (2,1,) the first distribution line (2) of each distribution means being connected to at least one inlet (7) for feed and to at least one raffmate outlet (8), the other line 1 being connected to at least one solvent inlet (3) and to at least one extract outlet (4), each inlet and outlet comprising an on-off valve (7a, 8a, 3a, 4a), the first distribution line (2) comprising a flushing valve (9), and all of the flushing valves (9) relating to all of the distribution lines (2) are connected to means (100, 102) for circulating a fluid to be displaced. FIG. 1 to be published.

    摘要翻译: 描述了一种模拟移动式床冲洗装置及其用途。 吸附器包括多个吸附剂床(10,11),每个床连接到分配装置(5),分配装置(5)包括两个流体分配管线(2,1),每个分配装置的第一分配管线(2)连接 至少一个用于进料的入口(7)和至少一个熔体出口(8),另一条管线1连接到至少一个溶剂入口(3)和至少一个提取物出口(4),每个入口和 出口包括开关阀(7a,8a,3a,4a),第一分配管线(2)包括冲洗阀(9),以及与所有分配管线(2)相关的所有冲洗阀(9) )连接到用于使待移动的流体循环的装置(100,102)。 1发表。

    Desorption technique
    7.
    发明授权
    Desorption technique 失效
    解吸技术

    公开(公告)号:US4461649A

    公开(公告)日:1984-07-24

    申请号:US490594

    申请日:1983-05-02

    摘要: This is a separation process employing a column of adsorbent which is divided sequentially into at least three zones, adsorption, purification and desorption zones. A net fluid flow is maintained through the column with the adsorbent moving actually or in a simulated manner countercurrent with respect to the fluid. The feedstock contains the components to be separated with one component being more selectively adsorbed in the adsorption zone by the adsorbent than the other components. A desorbent fluid effects desorption of the more selectively adsorbed component in the desorption zone, however, if carried over into the adsorption zone with the moving adsorbent the desorbent impedes adsorption. The process employs a flush stream introduced at the upstream boundary of the desorption zone, with the desorbent introduced between the upstream and downstream boundaries of that zone, which flushes the desorbent from the adsorbent prior to its movement into the adsorption zone.

    摘要翻译: 这是使用吸附塔的分离方法,该吸附塔依次分成至少三个区域,即吸附,净化和解吸区域。 通过柱子维持净流体流动,吸附剂实际上或以相对于流体逆流的模拟方式移动。 原料包含待分离的组分,一种组分通过吸附剂被选择性地吸附在吸附区中而不是其它组分。 解吸流体对脱附区中更多选择性吸附的组分进行解吸,然而,如果移动的吸附剂被吸附到吸附区,则解吸剂阻止吸附。 该方法使用在解吸区的上游边界处引入的冲洗流,其中解吸剂引入该区的上游和下游边界之间,其在吸附剂移动到吸附区之前从吸附剂上冲洗脱附剂。

    CONTINUOUS PROCESS FOR SEPARATION OF PROTEINS
    9.
    发明申请
    CONTINUOUS PROCESS FOR SEPARATION OF PROTEINS 有权
    分离蛋白质的连续方法

    公开(公告)号:US20170065906A1

    公开(公告)日:2017-03-09

    申请号:US14848196

    申请日:2015-09-08

    摘要: Disclosed is a continuous process for separating or extracting proteins from a low grade mixture of a protein of interest, other proteins, impurities, and salts in a continuous simulated moving bed separation process. The invention provides for direct extraction of heme protein and plant protein from a crude mixture of such proteins, other proteins, impurities and salts using the chromatographic technique of simulated moving bed (SMB) continuous chromatography. The SMB process combines the steps of feed loading, adsorbent washing, product elution, adsorbent regeneration, and adsorbent equilibration. The novel strong anion exchange resin adsorbent is a quaternary amine cross-linked microcellulose wherein the microcellulose is cross-linked with epichlorohydrin and the quaternary amine is 2,3-epoxypropyltrimethyl-ammonium chloride which exhibits selective adsorption of proteins and complete regeneration. Purified protein separated in this manner may provide human health benefits by providing greater medicinal and nutrition opportunities from low quality protein sources.

    摘要翻译: 公开了在连续模拟移动床分离过程中从目的蛋白质,其它蛋白质,杂质和盐的低级混合物中分离或提取蛋白质的连续方法。 本发明提供使用模拟移动床(SMB)连续层析的色谱技术从这种蛋白质,其他蛋白质,杂质和盐的粗混合物中直接提取血红素蛋白和植物蛋白。 SMB方法结合了进料负载,吸附剂洗涤,产物洗脱,吸附剂再生和吸附剂平衡的步骤。 新型强阴离子交换树脂吸附剂是季铵交联微纤维素,其中微纤维素与表氯醇交联,季胺是显示出蛋白质选择性吸附和完全再生的2,3-环氧丙基三甲基氯化铵。 以这种方式分离的纯化蛋白质可以通过从低质量蛋白质来源提供更大的药物和营养机会来提供人类健康益处。

    PRODUCT RECOVERY FROM ADSORPTION-SEPARATION PURGE FLUIDS
    10.
    发明申请
    PRODUCT RECOVERY FROM ADSORPTION-SEPARATION PURGE FLUIDS 审中-公开
    产品从吸收分离浆液中回收

    公开(公告)号:US20140371510A1

    公开(公告)日:2014-12-18

    申请号:US14476903

    申请日:2014-09-04

    申请人: UOP LLC

    IPC分类号: C07C7/12

    摘要: Purge fluid from a vessel head in an adsorption process is distributed to recovery processes according to the purity of product contained in the fluid. Extract-rich fluid thus is routed directly to recovery of the extract product. Distribution preferably is determined by internal positioning of feed, desorbent and product streams in the adsorption vessel.

    摘要翻译: 根据流体中含有的产品的纯度将吸附过程中的容器头部的流体分配到回收过程中。 因此,提取物富含的流体直接路由到萃取产物的回收。 分布优选通过进料,解吸剂和产物流在吸附容器中的内部定位来确定。