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    Hydrosilylation process
    1.
    发明授权
    Hydrosilylation process 有权
    氢化硅烷化过程

    公开(公告)号：US07208619B2

    公开(公告)日：2007-04-24

    申请号：US10484413

    申请日：2002-07-18

    申请人： Timothy Rex Bunce ,  Avril Surgenor ,  Stephen Westall

    发明人： Timothy Rex Bunce ,  Avril Surgenor ,  Stephen Westall

    IPC分类号： C07F7/08

    CPC分类号： C08G77/045 ,  C07F7/0879 ,  C08G77/38

    摘要： A silane or siloxane containing at least one organic group is prepared by a hydrosilylation reaction between a silane or siloxane (A) containing at least one Si—H group and an allyl compound (B) in the presence of a noble metal catalyst. The silane or siloxane (A) and the allyl compound (B) are fed continuously through a reaction zone which is maintained at a temperature in the range 115–200° C. and which is provided with heat exchanger means to dissipate the heat from the exothermic hydrosilylation reaction. The residence time of (A) and (B) in the reaction zone is less than 20 minutes.

    摘要翻译： 含有至少一个有机基团的硅烷或硅氧烷是在贵金属催化剂存在下，通过含有至少一个Si-H基团和烯丙基化合物（B）的硅烷或硅氧烷（A）之间的氢化硅烷化反应来制备的。 将硅烷或硅氧烷（A）和烯丙基化合物（B）连续进料通过保持在115-200℃范围内的温度的反应区，并且设置有热交换器装置以从 放热氢化硅烷化反应。 反应区中（A）和（B）的停留时间少于20分钟。

    Polysiloxanes and their preparation
    3.
    发明授权
    Polysiloxanes and their preparation 有权
    聚硅氧烷及其制备方法

    公开(公告)号：US07238768B2

    公开(公告)日：2007-07-03

    申请号：US11602559

    申请日：2006-11-21

    申请人： Peter Cheshire Hupfield ,  Avril Surgenor ,  Stephen Westall

    发明人： Peter Cheshire Hupfield ,  Avril Surgenor ,  Stephen Westall

    IPC分类号： C08G77/26

    CPC分类号： C08G77/26 ,  C08G77/08

    摘要： An amino-functional polysiloxane is prepared by reacting an aminosilane (A) which contains an aminoalkyl group and at least one alkoxy group bonded to Si with a carboxylic acid and a silanol-functional polysiloxane (B). The aminosilane (A) is partially converted into its carboxylate salt which acts as a catalyst for the siloxane condensation polymerization reaction between (A) and (B).

    摘要翻译： 通过使包含氨基烷基的氨基硅烷（A）和至少一个与Si结合的烷氧基与羧酸和硅烷醇官能聚硅氧烷（B）反应制备氨基官能聚硅氧烷。 氨基硅烷（A）部分转化成其羧酸盐，其用作（A）和（B）之间的硅氧烷缩聚反应的催化剂。

    Process for the production of organosilicon compounds
    4.
    发明授权
    Process for the production of organosilicon compounds 失效
    生产有机硅化合物的方法

    公开(公告)号：US5109094A

    公开(公告)日：1992-04-28

    申请号：US473073

    申请日：1990-01-31

    申请人： Sian B. Rees ,  Stephen Westall

    发明人： Sian B. Rees ,  Stephen Westall

    IPC分类号： C08G77/08

    CPC分类号： C08G77/08

    摘要： A process for the production of an organosilicon condensation product which comprises contacting (A) at least one organosilicon compound having in the molecule at least one silicon-bonded hydroxyl group, the organic substituents being selected from monovalent hydrocarbon groups having from 1 to 14 carbon atoms and monovalent substituted hydrocarbon groups having from 1 to 10 carbon atoms in which the substituents are selected from amino, halogen, mercapto, hydroxyl, amido and ester, with (B) a hydroxide selected from the group consisting of magnesium, calcium, strontium and barium hydroxides.

    Process for producing organosilicon products
    5.
    发明授权
    Process for producing organosilicon products 失效
    生产有机硅产品的方法

    公开(公告)号：US5109093A

    公开(公告)日：1992-04-28

    申请号：US473080

    申请日：1990-01-31

    申请人： Sian B. Rees ,  Stephen Westall

    发明人： Sian B. Rees ,  Stephen Westall

    IPC分类号： C08G77/38 ,  C08G77/08 ,  C08G77/18 ,  C08G77/20 ,  C08G77/22

    CPC分类号： C08G77/18 ,  C08G77/08 ,  C08G77/20 ,  C08G77/22

    摘要： A process for the preparation of an organosilicon condensation product which comprises reacting together at a temperature of at least 50.degree. C. (A) an organosilicon compound having in the molecule at least one silicon-bonded hydroxyl group; and (B) an organosilicon compound having in the molecule at least one silicon-bonded --OX group, in which X respresents an alkyl group having from 1 to 8 carbon atoms or an alkoxyalkyl group having from 2 to 8 carbon atoms, in the presence of a catalytic substance which is selected from strontium hydroxide and barium hydroxide.

    Organosiloxane-oxyalkylene copolymers
    8.
    发明授权
    Organosiloxane-oxyalkylene copolymers 失效
    有机硅氧烷 - 氧化烯共聚物

    公开(公告)号：US4631208A

    公开(公告)日：1986-12-23

    申请号：US791956

    申请日：1985-10-28

    申请人： Stephen Westall

    发明人： Stephen Westall

    IPC分类号： D06M15/643 ,  C08G77/00 ,  C08G77/22 ,  C08G77/38 ,  C08G77/46 ,  C08G77/50 ,  C11D3/37 ,  D06M15/647 ,  B05D3/02

    CPC分类号： C11D3/3738 ,  C08G77/46 ,  C08G77/50 ,  D06M15/647

    摘要： Organosiloxane-oxyalkylene copolymers in which a silicon atom of at least one organosiloxane unit has attached thereto the group--X(OR).sub.n OSiR'.sub.a (OR").sub.3-awherein X represents a divalent hydrocarbon group, R represents an alkylene group having 2 to 4 carbon atoms, n is an integer of at least 2, R' represents alkyl, vinyl, allyl or phenyl, R" represents alkyl or alkoxyalkyl and a has a value of 1 or 2, at least 40% of the total substituents in the copolymer being methyl.The copolymers are film forming and are particularly suitable for the treatment of textile fibres to facilitate the removal of oily stains during laundering.

    摘要翻译： 至少一个有机硅氧烷单元的硅原子连接基团-X（OR）nOSiR'a（OR“）3-a的有机硅氧烷 - 氧化烯共聚物，其中X表示二价烃基，R表示具有 2至4个碳原子，n为至少2的整数，R'表示烷基，乙烯基，烯丙基或苯基，R“表示烷基或烷氧基烷基，a为1或2，至少为总数的40％ 共聚物中的取代基是甲基。 共聚物是成膜的，特别适用于纺织纤维的处理，以便于洗涤期间除去油性污渍。

    Method of making siloxane compositions
    10.
    发明授权
    Method of making siloxane compositions 失效
    制造硅氧烷组合物的方法

    公开(公告)号：US5210129A

    公开(公告)日：1993-05-11

    申请号：US844054

    申请日：1992-03-02

    申请人： Jean de la Croi Habimana ,  Stephen Westall

    发明人： Jean de la Croi Habimana ,  Stephen Westall

    IPC分类号： C08G77/08 ,  C08J3/09

    CPC分类号： C08J3/098 ,  C08G77/08 ,  C08J2383/04

    摘要： A method of making a dispersion of a high viscosity siloxane in a volatile, especially cyclic siloxane, comprises first dispersing organopolysiloxanes having at least 2 Si--OR groups, wherein R is H or alkyl in a volatile siloxane and adding a catalyst which is either a phosphonitrile halide having the general formula [X(PX.sub.2 .dbd.N).sub.n PX.sub.3 ].sup.+ [MX.sub.(v-t+1) R.sub.t ].sup.-, or a heterogeneous catalyst selected from Li, Mg, Ca, Sr or Ba hydroxide, Na or K borate or phosphate, Rb or Cs carbonate or carboxylates of Rb or Cs wherein M is an element having an electronegativity of from 1.0 to 2.0, R is alkyl, X is halide, n is 1 to 6, v is the valence of M and t is from 0 to (v-1).

    摘要翻译： 制备高粘度硅氧烷在挥发性，特别是环状硅氧烷中的分散体的方法包括首先分散具有至少2个Si-OR基团的有机聚硅氧烷，其中R是H或烷基在挥发性硅氧烷中，并加入催化剂 具有通式[X（PX2 = N）nPX3] + [MX（v-t + 1）Rt] - 的磷腈卤化物，或选自Li，Mg，Ca，Sr或氢氧化钡，Na或K硼酸盐的多相催化剂 或磷酸盐，Rb或Cs碳酸盐或Rb或Cs的羧酸盐，其中M是电负性为1.0至2.0的元素，R为烷基，X为卤化物，n为1至6，v为M的化合价，t为 从0到（v-1）。