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1.发明授权Azeotropic distillation process for recovery of diamondoid compounds from hydrocarbon streams 失效用于从油气回收回收二氧化钛化合物的AZOOPOPIC蒸馏工艺
公开(公告)号：US5139621A
公开(公告)日：1992-08-18
申请号：US535633
申请日：1990-06-11
摘要： An azeotropic distillation method for separating diamondoids from a near-boiling solvent. The method is particularly useful for recovering diamondoids extracted from a produced natural gas stream via hydrocarbon solvent injection.
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公开(公告)号：US5106514A
公开(公告)日：1992-04-21
申请号：US521957
申请日：1990-05-11
申请人： Richard A. Alexander
发明人： Richard A. Alexander
CPC分类号： B04C5/14 , B01D17/0214 , B04C5/081 , B04C5/103 , B04C5/13
摘要： A material extraction nozzle for separating a mixture of materials having different densities, comprising: a nozzle body shell having an outer surface with a tangentially located material inlet at an upper portion thereof and an inner surface defining in part a frustrum of a cone; a substantially conical diffuser section having an outer surface terminating in an apex, the diffuser section axially aligned within the nozzle body shell in a spaced relation therewith so as to form an extraction chamber with the inner surface of the nozzle body shell and the outer surface of the substantially conical diffuser section; an extracted material outlet port positioned axially through the substantially conical diffuser section; and at least one rejected material capillary outlet located below the apex of the diffuser section.
摘要翻译： 一种用于分离具有不同密度的材料的混合物的材料提取喷嘴，包括：喷嘴体外壳，其具有在其上部具有切向定位的材料入口的外表面和部分限定锥体的内表面; 基本上圆锥形的扩散器部分具有终止于顶点的外表面，扩散器部分在喷嘴主体壳体内以间隔开的方式轴向地对齐，以形成具有喷嘴主体壳体的内表面的提取室， 大致圆锥形的扩散器部分; 提取的材料出口端口轴向地定位穿过基本上圆锥形的扩散器部分; 以及位于扩散器部分的顶点下方的至少一个排出材料毛细管出口。
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公开(公告)号：US4952747A
公开(公告)日：1990-08-28
申请号：US358759
申请日：1989-05-26
摘要： According to this invention, substantially hydrocarbonaceous fractions comprising diamondoid compounds are peculiarly suitable for separation by a thermal gradient diffusion process. Applicability of this process to this service is dependent upon the fact that the diamondoid compounds exhibit a large change in viscosity relative to temperature, that is, their viscosity goes down significantly per degree of increase in temperature.
摘要翻译： 根据本发明，包含类金刚石化合物的基本上含烃部分特别适用于通过热梯度扩散方法进行分离。 该方法对该方法的适用性取决于金刚石类化合物相对于温度表现出大的粘度变化的事实，也就是说，它们的粘度随着温度的升高而显着下降。
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公开(公告)号：US07088447B1
公开(公告)日：2006-08-08
申请号：US11141453
申请日：2005-05-31
IPC分类号： G01N21/00
CPC分类号： G01N15/1459 , G01N15/1434 , G01N2015/1486
摘要： A particle measurement system using a single component light collecting system with an aperture having a portion within direct view of the light detector. An aperture assembly extending into a sample may be self-concealing by having an extended portion to block light from directly illuminating the light detector. Alternatively, a smooth, reflective inside surface of the aperture assembly provides for self-concealment by causing spontaneous emitted light to have low angles of reflection. In either case, spontaneously emitted light is substantially prevented from reflecting directly into the light detector, thereby reducing light noise to the level of molecular noise.
摘要翻译： 一种使用单分量光收集系统的粒子测量系统，其具有孔，其具有在光检测器的直视下的部分。 延伸到样品中的孔组件可以通过具有延伸部分来阻挡来自直接照射光检测器的光而自我隐藏。 或者，孔组件的光滑的反射内表面通过使自发发射的光具有低的反射角来提供自我隐藏。 在任一情况下，基本上防止了自发发射的光直接反射到光检测器中，从而将光噪声降低到分子噪声的水平。
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公开(公告)号：US4982049A
公开(公告)日：1991-01-01
申请号：US358761
申请日：1989-05-26
IPC分类号： C07C13/615 , C10G21/00 , C10G25/00 , C10L3/00
CPC分类号： C10G25/00 , C07C13/615 , C10G21/00 , C10L3/00
摘要： A process for recovering diamondoid compounds from hydrocarbonaceous minerals and/or from deposits left by such minerals in equipment or otherwise, which comprises dissolving diamondoid compounds in an aromatic distillate fuel oil; extracting aromatics from the solution; and separating diamondoid compounds from the raffinate of the extraction.
摘要翻译： 从设备或其他方法中从含烃矿物和/或由这些矿物质留下的沉积物中回收金刚石类化合物的方法，其包括将金刚石类化合物溶解在芳族馏分燃料油中; 从溶液中萃取芳烃; 并从萃取液的萃余液中分离金刚石类化合物。
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公开(公告)号：US4952748A
公开(公告)日：1990-08-28
申请号：US405119
申请日：1989-09-07
摘要： A process is disclosed for extracting diamondoid compounds from a hydrocarbon gas stream. The process includes two stages, each of which alone is effective to remove diamondoids from a hydrocarbon gas stream. The first stage comprises contacting the diamondoid-laden hydrocarbon gas with a suitable solvent to preferentially dissolve the diamondoids into the solvent. Diesel fuel is the preferred solvent for this first stage. The second stage comprises sorbing diamondoids from the diamonoid-laden hydrocarbon gas with silica gel. The most preferred embodiment of the invention is a serial process in which a diamondoid-laden gas is first treated in the solvation stage and the partially purified gas is further resolved in the silica gel sorption stage. The invention still further includes a process for segregating adamantane and diamantane when both are separated from a hydrocarbon gas stream.
摘要翻译： 公开了从烃气流中提取金刚石类化合物的方法。 该方法包括两个阶段，其中每个阶段单独有效地从烃气流中除去金刚石。 第一阶段包括将含有金刚石的载体烃与合适的溶剂接触以优先将金刚石溶解到溶剂中。 柴油燃料是第一阶段的首选溶剂。 第二阶段包括用含硅胶的含二氧化碳的烃气体吸附金刚石。 本发明的最优选实施方案是在溶剂化阶段首先处理载有类金刚石的气体并且部分纯化的气体在硅胶吸附阶段进一步分解的连续方法。 本发明还包括当两者与烃气流分离时分离金刚烷和金刚烷的方法。
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7.发明授权Material extraction nozzle coupled with distillation tower and vapors separator 失效材料提取喷嘴与蒸馏塔和蒸汽分离器相结合
公开(公告)号：US5246575A
公开(公告)日：1993-09-21
申请号：US825342
申请日：1992-01-24
申请人： Richard A. Alexander
发明人： Richard A. Alexander
摘要： A material extraction nozzle for separating a mixture of materials having different densities, comprising: a nozzle body shell having an outer surface with a tangentially located material inlet at an upper portion thereof and an inner surface defining in part a frustrum of a cone; a substantially conical diffuser section having an outer surface terminating in an apex, the diffuser section axially aligned within the nozzle body shell in a spaced relation therewith so as to form an extraction chamber with the inner surface of the nozzle body shell and the outer surface of the substantially conical diffuser section; an extracted material outlet port positioned axially through the substantially conical diffuser section; and at least one rejected material capillary outlet located below the apex of the diffuser section.
摘要翻译： 一种用于分离具有不同密度的材料的混合物的材料提取喷嘴，包括：喷嘴体外壳，其具有在其上部具有切向定位的材料入口的外表面和部分限定锥体的内表面; 基本上圆锥形的扩散器部分具有终止于顶点的外表面，扩散器部分在喷嘴主体壳体内以间隔开的方式轴向地对齐，以形成具有喷嘴主体壳体的内表面的提取室， 大致圆锥形的扩散器部分; 提取的材料出口端口轴向地定位穿过基本上圆锥形的扩散器部分; 以及位于扩散器部分的顶点下方的至少一个排出材料毛细管出口。
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公开(公告)号：US4952749A
公开(公告)日：1990-08-28
申请号：US358760
申请日：1989-05-26
IPC分类号： C10G25/00
CPC分类号： C10G25/00
摘要： A process for recovering diamondoid compounds from a fluid mixture thereof with other hydrocarbonaceous compounds which comprises contacting said mixture with a porous solid, for example, a zeolite, having pore opening large enough to admit said diamondoid compounds thereinto and small enough so that at least 50% of the external atoms of said diamondoid compounds are capable of simultaneously contacting the internal walls of the pores of said solid under conditions conducive to absorption of diamondoid compounds by said solid; and then desorbing the absorbate comprising diamondoid compounds from said solid absorbant.
摘要翻译： 一种从其与其它烃类化合物的流体混合物中回收金刚石类化合物的方法，其包括使所述混合物与多孔固体例如沸石接触，所述多孔固体具有足够大的孔隙以允许所述类金刚石化合物进入其中并且足够小以使得至少50 所述金刚石化合物的外部原子的％能够在有助于所述固体吸收金刚石类化合物的条件下同时接触所述固体的孔的内壁; 然后从所述固体吸收剂中解吸包含类金刚石化合物的吸收剂。
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