Abstract:
The invention concerns a process for the spheroidisation, densification and purification of powders through the combined action of plasma processing, and ultra-sound treatment of the plasma-processed powder. The ultra-sound treatment allows for the separation of the nanosized condensed powder, referred to as ‘soot’, from the plasma melted and partially vaporized powder. The process can also be used for the synthesis of nanopowders through the partial vaporization of the feed material, followed by the rapid condensation of the formed vapour cloud giving rise to the formation of a fine aerosol of nanopowder. In the latter case, the ultra-sound treatment step serves for the separation of the formed nanopowder form the partially vaporized feed material.
Abstract:
A process and apparatus for the synthesis of metal oxide nanopowder from a metal compound vapour is presented. In particular a process and apparatus for the synthesis of TiO2 nanopowder from TiCl4 is disclosed. The metal compound vapour is reacted with an oxidizing gas in electrically induced RF frequency plasma thus forming a metal oxide vapour. The metal oxide vapour is rapidly cooled using a highly turbulent gas quench zone which quickly halts the particle growth process, yielding a substantial reduction in the size of metal oxide particles formed compared with known processes. The metal compound vapour can also react with a doping agent to create a doped metal oxide nanopowder. Additionally, a process and apparatus for the inline synthesis of a coated metal oxide is disclosed wherein the metal oxide particles are coated with a surface agent after being cooled in a highly turbulent gas quench zone.
Abstract:
A process and apparatus for preparing a nanopowder are presented. The process comprises feeding a reactant material into a plasma reactor in which is generated a plasma flow having a temperature sufficiently high to vaporize the material; transporting the vapour by means of the plasma flow into a quenching zone; injecting a preheated quench gas into the plasma flow in the quenching zone to form a renewable gaseous condensation front; and forming a nanopowder at the interface between the renewable controlled temperature gaseous condensation front and the plasma flow.
Abstract:
An induction plasma torch comprises a tubular torch body, a gas distributor head located at the proximal end of the torch body for supplying at least one gaseous substance into the chamber within the torch body, a higher frequency power supply connected to a first induction coil mounted coaxial to the tubular torch body, a lower frequency solid state power supply connected to a plurality of second induction coils mounted coaxial to the tubular torch body between the first induction coil and the distal end of this torch body. The first induction coil provides the inductive energy necessary to ignite the gaseous substance to form a plasma. The second induction coils provide the working energy necessary to operate the plasma torch. The second induction coils can be connected to the solid state power supply in series and/or in parallel to match the impedance of this solid state power supply.
Abstract:
An induction plasma torch comprises a tubular torch body, a gas distributor head located at the proximal end of the torch body for supplying at least one gaseous substance into the chamber within the torch body, a higher frequency power supply connected to a first induction coil mounted coaxial to the tubular torch body, a lower frequency solid state power supply connected to a plurality of second induction coils mounted coaxial to the tubular torch body between the first induction coil and the distal end of this torch body. The first induction coil provides the inductive energy necessary to ignite the gaseous substance to form a plasma. The second induction coils provide the working energy necessary to operate the plasma torch. The second induction coils can be connected to the solid state power supply in series and/or in parallel to match the impedance of this solid state power supply.
Abstract:
The method and apparatus treat a surface of natural rock or artificial stone-like material to give to this surface an attractive finish. A high temperature jet of plasma and a high speed jet of cooling fluid are projected onto the surface to be treated. The two jets are moved on the surface at a given speed with the jet of cooling fluid following the plasma jet. The speed of movement is selected so that the high temperature plasma jet heats only a thin superficial layer of rock or stone-like material. As the jet of cooling fluid follows the jet of plasma, it suddenly cools the thin superficial layer just heated by the plasma jet to cause a thermal shock which bursts particles of rock or stone-like material at the surface thereof, and blows these particles off the rock surface.
Abstract:
A process and apparatus for synthesizing a nanopowder is presented. In particular, a process for the synthesis of nanopowders of various materials such as metals, alloys, ceramics and composites by induction plasma technology, using organometallic compounds, chlorides, bromides, fluorides, iodides, nitrites, nitrates, oxalates and carbonates as precursors is disclosed. The process comprises feeding a reactant material into a plasma torch in which is generated a plasma flow having a temperature sufficiently high to yield a superheated vapour of the material; transporting said vapour by means of the plasma flow into a quenching zone; injecting a cold quench gas into the plasma flow in the quenching zone to form a renewable gaseous cold front; and forming a nanopowder at the interface between the renewable gaseous cold front and the plasma flow.
Abstract:
The present invention relates to a solid oxide fuel cell comprising a reformer for supporting the solid oxide fuel cell, an anode, an electrolyte, and a cathode. The reformer includes an electroconductive mixture of active material and a polymeric ceramic material shaped to constitute a slab having an upper surface and a lower surface and grooves along at least one of the upper surface and the lower surface and flat regions along the periphery of the grooved surface.
Abstract:
The invention relates to a process and an apparatus for the plasma deposition of protective coatings and near net shape bodies using induction plasma technology. The apparatus comprises an induction plasma torch in which the particulate material to be deposited is accelerated and injected axially into the discharge. As the particles traverse the plasma they are heated and melted before being deposited by impaction on the substrate placed at the downstream end of the plasma torch facing the plasma jet.
Abstract:
The solid oxide fuel cell can comprise: an electroconductive and porous reformer including a catalytically active material and shaped to constitute a solid slab having a first surface and a second surface opposite the first surface, and a plurality of adjacent grooves along the first surface, and flat regions adjacent the plurality of grooves; an anode layer covering the plurality of grooves of the reformer slab and having a corresponding grooved shape; an electrolyte layer covering the anode layer over the plurality of grooves of the reformer slab and having a corresponding grooved shape, and extending over the flat regions; and a cathode layer covering the electrolyte layer over the grooves of the reformer slab and having a corresponding grooved shape.