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    N-benzoyl-N'-2,5-dihalo-4-perfluoroalkoxyphenylureas, pesticidal compositions containing them and their use in the control of pests
    1.
    发明授权
    N-benzoyl-N'-2,5-dihalo-4-perfluoroalkoxyphenylureas, pesticidal compositions containing them and their use in the control of pests 失效
    N-苯甲酰基-N'-2,5'-二卤代-4-全氟烷氧基苯基脲，含有它们的杀虫组合物及其在防治害虫中的应用

    公开(公告)号：US4925875A

    公开(公告)日：1990-05-15

    申请号：US218191

    申请日：1988-07-13

    Applicant: Jozef Drabek ,  Urs Siegrist

    Inventor： Jozef Drabek ,  Urs Siegrist

    IPC: A01N47/34 ,  C07C205/37 ,  C07C275/54

    CPC classification number: A01N47/34 ,  C07C205/37 ,  C07C275/54

    Abstract: Novel substituted N-benzoyl-N'-2,5-dihalo-4-perfluoroalkoxyphenylureas of formula I ##STR1## in which R.sub.1 is hydrogen, fluorine, chlorine or bromine; R.sub.2 is fluorine or chlorine; each of R.sub.3 and R.sub.4 is fluorine, chlorine or bromine; and n is 2, 3, 4, 5, 6, 7 or 8, processes and intermediates for their prepraration, their use in pest control, and pesticidal compositions that contain at least one compound of formula I as active ingredient, are disclosed. The preferred field of application is the control of pests in and on animals and plants.

    Abstract translation: 式I的新型取代的N-苯甲酰基-N'-2,5-二卤代-4-全氟烷氧基苯基脲其中R 1是氢，氟，氯或溴; R2是氟或氯; R3和R4各自为氟，氯或溴; 并且n是2,3,4,5,6,7或8，其制备方法和中间体，它们在害虫防治中的应用，以及含有至少一种式I化合物作为活性成分的杀虫组合物。 优选的应用领域是控制动物和植物中的有害生物。

    Process for the preparation of substituted aromatic amino compounds
    3.
    发明授权
    Process for the preparation of substituted aromatic amino compounds 有权
    取代芳香族氨基化合物的制备方法

    公开(公告)号：US06258982B1

    公开(公告)日：2001-07-10

    申请号：US09254586

    申请日：1999-03-10

    Applicant: Peter Baumeister ,  Urs Siegrist ,  Martin Studer

    Inventor： Peter Baumeister ,  Urs Siegrist ,  Martin Studer

    IPC: C07C23300

    CPC classification number: C07C221/00 ,  C07C209/36 ,  C07C227/04 ,  C07C211/45 ,  C07C225/22 ,  C07C229/44 ,  C07C229/60

    Abstract: The present invention relates to a hydrogenation process for the preparation of aromatic amino compounds containing directly on the aryl ring or in a side chain one or more entities that may also undergo hydrogenation, such as carbon multiple bonds, nitrile groups, imino groups or carbonyl groups. The preparation is carried out by catalytic hydrogenation of the corresponding aromatic nitro compounds in the presence of a phosphorus-modified noble metal catalyst. The invention relates also to the use of modified noble metal catalysts for the hydrogenation of aromatic nitro compounds containing carbon multiple bonds and/or substituted by nitrile, imino or carbonyl groups.

    Abstract translation: 本发明涉及一种用于制备直接在芳环或侧链上的芳族氨基化合物的氢化方法，一个或多个也可能进行氢化的实体，如碳多重键，腈基，亚氨基或羰基 。 在磷改性贵金属催化剂存在下，通过相应的芳族硝基化合物的催化氢化进行制备。 本发明还涉及改性贵金属催化剂用于氢化包含碳多重键和/或被腈，亚氨基或羰基取代的芳族硝基化合物的用途。

    Process for the production of aromatic halogen-amino compounds
    5.
    发明授权
    Process for the production of aromatic halogen-amino compounds 有权
    制备芳香族卤素 - 氨基化合物的方法

    公开(公告)号：US06197716B1

    公开(公告)日：2001-03-06

    申请号：US09185851

    申请日：1998-11-04

    Applicant: Peter Baumeister ,  Urs Siegrist ,  Martin Studer

    Inventor： Peter Baumeister ,  Urs Siegrist ,  Martin Studer

    IPC: B01J3100

    CPC classification number: C07D213/73 ,  C07C209/365

    Abstract: The present invention relates to a hydrogenation process for the production of aromatic halogen-amino compounds by means of catalytic hydrogenation on noble metal catalysts of corresponding aromatic halonitro compounds, characterised in that a rhodium, ruthenium, iridium, platinum or palladium catalyst which is modified with an inorganic or organic phosphorus compound with a degree of oxidation of less than V, is used, in the presence of a vanadium compound.

    Abstract translation: 本发明涉及通过在相应的芳族卤代硝酸化合物的贵金属催化剂上通过催化氢化生产芳族卤代 - 氨基化合物的氢化方法，其特征在于将铑，钌，铱，铂或钯催化剂改性为 在钒化合物的存在下，使用氧化度小于V的无机或有机磷化合物。

    Process for the preparation of 6-alkyl-4-(pyridin-3-yl-methyleneamino)-4,5-dihydro-1,2,4-triazin-3(2H)- one
    7.
    发明授权
    Process for the preparation of 6-alkyl-4-(pyridin-3-yl-methyleneamino)-4,5-dihydro-1,2,4-triazin-3(2H)- one 失效
    制备6-烷基-4-（吡啶-3-基 - 亚甲基氨基）-4,5-二氢-1,2,4-三嗪-3（2H） - 酮的方法

    公开(公告)号：US5606057A

    公开(公告)日：1997-02-25

    申请号：US194183

    申请日：1994-02-09

    Applicant: Thomas Pitterna ,  Urs Siegrist ,  Henry Szczepanski

    Inventor： Thomas Pitterna ,  Urs Siegrist ,  Henry Szczepanski

    IPC: A01N43/707 ,  B01J25/02 ,  C07B61/00 ,  C07D401/12 ,  C07D253/06

    CPC classification number: C07D401/12

    Abstract: A process for the preparation of 6-alkyl-4-(pyridin-3-yl-methyleneamino)-4,5-dihydro-1,2,4-triazin-3(2H)-one by the reaction of 4-amino-6-alkyl-3-oxo-2,3,4,5-tetrahydro-1,2,4-triazine with 3-cyanopyridine wherein the reaction is carried out under catalytic hydrogenation conditions in the presence of a Raney-nickel catalyst in an aqueous alcoholic medium, at a temperature between 0.degree. and 70.degree. C., at a pH of between 2 and 7, and in the presence of and a C.sub.1 -C.sub.6 -carboxylic acid or a C.sub.1 -C.sub.6 -carboxylic acid alkali metal salt or both, whereby the hydrogen pressure is between 0.1 and 10 bar.

    Abstract translation: 6-氨基-4-（吡啶-3-基 - 亚甲基氨基）-4,5-二氢-1,2,4-三嗪-3（2H） - 酮的制备方法， 6-烷基-3-氧代-2,3,4,5-四氢-1,2,4-三嗪与3-氰基吡啶反应，其中反应在催化氢化条件下在阮内镍催化剂存在下进行 水溶性醇介质，温度在0℃至70℃之间，pH为2-7，在C 1 -C 6羧酸或C 1 -C 6羧酸碱金属盐存在下，或 两者，由此氢压力在0.1和10巴之间。

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