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公开(公告)号：US4059414A
公开(公告)日：1977-11-22
申请号：US691118
申请日：1976-05-28
申请人： Hans D. Holtz , Benedict R. Bonazza
发明人： Hans D. Holtz , Benedict R. Bonazza
IPC分类号： C10L1/24
CPC分类号： C10L1/2437 , C10M1/08 , C10M2219/044
摘要： A long chain monocarboxylic acid is reacted with a trialkanolamine to produce an ester and this ester is then treated with sulfonic acid to produce a sulfonate to provide compounds which are suitable as ashless detergent additives and the method for producing these compounds are provided. In a preferred embodiment the ashless fuel detergent additives are combined with hydrocarbons suitable as fuel in an internal combustion engine to provide ashless fuel and lubricant detergent compositions.
摘要翻译： 将长链一元羧酸与三烷醇胺反应以产生酯，然后用磺酸处理该酯以产生磺酸盐，以提供适合作为无灰洗涤剂添加剂的化合物，并提供制备这些化合物的方法。 在优选实施方案中，无灰燃料洗涤剂添加剂与适合作为内燃机燃料的烃组合，以提供无灰燃料和润滑剂洗涤剂组合物。
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公开(公告)号：US4125383A
公开(公告)日：1978-11-14
申请号：US676257
申请日：1976-04-12
申请人： Hans D. Holtz
发明人： Hans D. Holtz
IPC分类号： C10L1/22 , C10L1/24 , C07C102/04
CPC分类号： C10L1/2493 , C10L1/221
摘要： A long chain monocarboxylic acid, a polyamine, and an isocyanate containing about 12 to 18 carbon atoms are reacted to provide compounds which are suitable as ashless detergent additives. Optionally, these compounds can be further reacted with hydrocarbyl sulfonic acid. The method for producing these compounds is also provided. In a preferred embodiment the ashless fuel detergent additives are combined with hydrocarbons suitable as fuel in an internal combustion engine to provide ashless fuel detergent compositions.
摘要翻译： 使长链单羧酸，多胺和含有约12至18个碳原子的异氰酸酯反应以提供适合作为无灰洗涤剂添加剂的化合物。 任选地，这些化合物可以进一步与烃基磺酸反应。 也提供了这些化合物的制造方法。 在优选的实施方案中，无灰燃料洗涤剂添加剂与内燃机中适合作为燃料的烃组合以提供无灰燃料洗涤剂组合物。
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公开(公告)号：US4088823A
公开(公告)日：1978-05-09
申请号：US620465
申请日：1975-10-07
申请人： Hans D. Holtz , Lloyd E. Gardner
发明人： Hans D. Holtz , Lloyd E. Gardner
CPC分类号： C07C29/095 , C07C45/36 , C07C67/035
摘要： A process is provided for oxygenating alkyl-substituted aromatic compounds. In the process alkyl-substituted aromatic compounds are contacted with molecular oxygen in the presence of a suitable monocarboxylic acid, a soluble copper, cobalt, or iron compound, and an inorganic bromine compound. Optionally present are inorganic nitrates, acetic anhydride, or water. In an embodiment of the invention the process is carried out in two distinct steps with contact of the alkyl-substituted aromatic compounds and oxygen in the presence of the essential components produce an ester comprising both an aromatic alcohol and the carboxylic acid with subsequent hydrolyzing of this ester to produce an aromatic alcohol with regeneration of the carboxylic acid.
摘要翻译： 提供了对烷基取代的芳族化合物进行加氧的方法。 在该方法中，在合适的一元羧酸，可溶性铜，钴或铁化合物和无机溴化合物的存在下，使烷基取代的芳族化合物与分子氧接触。 任选存在无机硝酸盐，乙酸酐或水。 在本发明的一个实施方案中，该方法在两个不同的步骤中进行，其中烷基取代的芳族化合物和氧在必要组分存在下接触产生包含芳族醇和羧酸的酯，随后水解该 酯以产生具有羧酸再生的芳族醇。
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公开(公告)号：US4065511A
公开(公告)日：1977-12-27
申请号：US399491
申请日：1973-09-21
申请人： Hans D. Holtz
发明人： Hans D. Holtz
IPC分类号： C07C35/06 , C07C29/00 , C07C67/00 , C07C121/34
CPC分类号： C07C35/06
摘要： Selected organic peroxides are converted to the corresponding alcohols when contacted with a triorganophosphine in a reaction medium comprising water and an organic solvent miscible with water. In one embodiment, diene polyperoxides are converted to the novel diols.
摘要翻译： 当在包含水和与水混溶的有机溶剂的反应介质中与三有机膦接触时，选择的有机过氧化物被转化为相应的醇。 在一个实施方案中，将二烯聚过氧化物转化为新型二醇。
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5.发明授权
公开(公告)号：US4110252A
公开(公告)日：1978-08-29
申请号：US748085
申请日：1976-12-06
申请人： Clifford E. Smith , Hans D. Holtz
发明人： Clifford E. Smith , Hans D. Holtz
摘要： A catalytically active composition is provided that is an intercalate of graphite, aluminum halide, and a Group VA metal halide. A process for preparing an intercalate of graphite, aluminum halide, and a Group VA metal halide is also provided.
摘要翻译： 提供了催化活性组合物，其是石墨，卤化铝和VA族金属卤化物的插层。 还提供了制备石墨，卤化铝和VA族金属卤化物的插层的方法。
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公开(公告)号：US3931236A
公开(公告)日：1976-01-06
申请号：US351980
申请日：1973-04-17
申请人： Hans D. Holtz , John E. Mahan
发明人： Hans D. Holtz , John E. Mahan
IPC分类号： C07D315/00 , C07D309/30
CPC分类号： C07D315/00
摘要： A halotetrahydropyran is oxidized and dehydrohalogenated employing oxygen and a free radical initiator.4-Chlorotetrahydropyran is converted to 5,6-dihydro-1,2-pyrone using 2,2'-azobis(2-methylpropionitrile) under elevated oxygen pressure and at a temperature of the order of about 170.degree.F.
摘要翻译： 使用氧和自由基引发剂将卤代四氢吡喃氧化并脱卤化氢。
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7.发明授权Alkylation of olefins with paraffins utilizing aluminum halide and group VA metal halide intercalated in graphite 失效使用铝卤化物和插入石墨的VA族金属卤化物的链烷烃进行烷基化
公开(公告)号：US4128596A
公开(公告)日：1978-12-05
申请号：US879571
申请日：1978-02-21
申请人： Clifford E. Smith , Hans D. Holtz
发明人： Clifford E. Smith , Hans D. Holtz
摘要： A catalytically active composition is provided that is an intercalate of graphite, aluminum halide, and a Group VA metal halide. A process for preparing an intercalate of graphite, aluminum halide, and a Group VA metal halide is also provided.
摘要翻译： 提供了催化活性组合物，其是石墨，卤化铝和VA族金属卤化物的插层。 还提供了制备石墨，卤化铝和VA族金属卤化物的插层的方法。
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公开(公告)号：US4082518A
公开(公告)日：1978-04-04
申请号：US571901
申请日：1975-04-28
IPC分类号： C08C19/00 , C10L1/236 , C10M149/08 , C10L1/22
CPC分类号： C10L1/2362 , C08C19/00 , C10M149/08 , C10M2215/16
摘要： Improved additives for motor fuels and lubricants are provided comprising low molecular weight hydrogenated liquid polymers containing low levels of combined nitrogen. More specifically, hydrogenated adducts formed from normally liquid low molecular weight polydiolefins and acrylonitrile are excellent additives for motor fuels and lubricants. Motor fuels and lubricating oil compositions containing said additives are also provided.
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公开(公告)号：US4059535A
公开(公告)日：1977-11-22
申请号：US691119
申请日：1976-05-28
申请人： Albert N. De Vault , Hans D. Holtz
发明人： Albert N. De Vault , Hans D. Holtz
CPC分类号： C10M1/08 , C10L1/2437 , C10M2219/044
摘要： A long chain monocarboxylic acid is reacted with a multi-amine to produce an amide and the amide is then treated with sulfonic acid to produce a sulfonate to provide compounds which are suitable as ashless detergent additives and the method for producing these compounds are provided. In a preferred embodiment the detergent additives are combined with hydrocarbons suitable as fuel in an internal combustion engine and with oil formulations to provide ashless fuel detergent compositions and lubricant detergent compositions.
摘要翻译： 将长链单羧酸与多胺反应以产生酰胺，然后用磺酸处理酰胺以产生磺酸盐以提供适合作为无灰洗涤剂添加剂的化合物，并且提供这些化合物的制备方法。 在优选的实施方案中，洗涤剂添加剂与内燃机中适合作为燃料的烃和油配方混合以提供无灰燃料洗涤剂组合物和润滑剂洗涤剂组合物。
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公开(公告)号：US4000068A
公开(公告)日：1976-12-28
申请号：US603974
申请日：1975-08-12
申请人： William T. Nelson , Hans D. Holtz
发明人： William T. Nelson , Hans D. Holtz
摘要： Organically polluted waters are purified by contacting such waters with a water soluble copper salt catalyst in the liquid phase under oxidizing conditions. In one embodiment, an aqueous stream obtained from the effluent of an oxidative dehydrogenation process containing contaminating oxygen-containing organic materials is subjected to liquid phase oxidizing conditions in the presence of cupric nitrate under conditions providing sufficient cupric ion concentration to convert the water to a potable aqueous product.
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