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公开(公告)号：US10113978B2
公开(公告)日：2018-10-30
申请号：US15221889
申请日：2016-07-28
IPC分类号： G01N21/64 , G01N27/416 , G01N21/956 , G01N21/91
摘要： An interfacial electric field intensity of a surface is measured by covalently binding a monolayer of a voltage sensitive chromophore to the surface and irradiating it with actinic radiation while it is in contact with a liquid and measuring a first fluorescence emission spectrum. A solution of the voltage sensitive chromophore dissolved in a sample of the liquid is also irradiated with actinic radiation and a second fluorescence emission spectrum is measured. The first and second fluorescence emission spectra are compared to determine the interfacial electric field intensity.
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公开(公告)号：US09963614B2
公开(公告)日：2018-05-08
申请号：US14714422
申请日：2015-05-18
IPC分类号： C09D133/24 , C08F220/38 , C08K5/00 , C09D133/14 , C09D135/00
CPC分类号： C09D133/02 , C08F220/06 , C08F220/20 , C08F220/38 , C08F220/58 , C08K5/00 , C09D133/14 , C09D135/00 , C08F2220/382 , C08F2220/303 , C08F2220/585 , C08F212/14
摘要： A water-soluble composition includes reducible copper ions or copper nanoparticles complexed with a reactive polymer. The reactive polymer can be crosslinked using suitable irradiation to provide copper-containing water-insoluble complexes. The water-soluble composition can be used to provide various articles and electrically-conductive materials that can be assembled in electronic devices. The reactive polymer has greater than 1 mol % of recurring units comprising sulfonic acid or sulfonate groups, at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally at least 1 mol % of recurring units comprising a pendant amide, amine, hydroxyl, lactam, phosphonic acid, or carboxylic acid group.
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公开(公告)号：US20170145233A1
公开(公告)日：2017-05-25
申请号：US15218144
申请日：2016-07-25
IPC分类号： C09D11/322 , C09D11/037 , B41J2/01 , C09D11/107 , C09D17/00 , C09D135/02 , C09D11/40 , C09D11/033
CPC分类号： C09D11/322 , B41J2/01 , B41J2/2107 , B41J2/2117 , C08F224/00 , C08F2800/10 , C08J3/05 , C08J2337/00 , C09D11/03 , C09D11/033 , C09D11/037 , C09D11/107 , C09D11/38 , C09D11/40 , C09D17/001 , C09D17/008 , C09D135/02
摘要： An aqueous dispersion contains pigment colorant particles that are present in an amount of at least 5 weight % and up to and including 80 weight %; a dispersing polymer that is a hexyloxy benzoic acid polymer; and an aqueous medium. The weight ratio of the pigment colorant particles to the dispersing polymer is from 19:1 to and including 2:1. Such aqueous dispersions can be incorporated into aqueous inkjet ink compositions that can be used for forming opaque images such as white images using inkjet printing methods.
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公开(公告)号：US09644112B1
公开(公告)日：2017-05-09
申请号：US15133583
申请日：2016-04-20
摘要： Articles are designed with a substrate and have either a uniform layer or pattern of electrically-conductive polyaniline on one or both supporting sides of the substrate. The electrically-conductive polyaniline is disposed either within, on top of, or both within and on top of, a uniform or pattern of a crosslinked polymer that is derived from a photocurable composition comprising water-soluble reactive polymer comprising (a) greater than 40 mol % of recurring units comprising sulfonic acid or sulfonate groups, (b) at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally (c) at least 1 mol % of recurring units comprising a pendant amide, hydroxyl, lactam, phosphonic acid, phosphonate, carboxylic acid, or carboxylate group, all amounts based on the total recurring units in the water-soluble reactive polymer.
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公开(公告)号：US10060853B2
公开(公告)日：2018-08-28
申请号：US15221978
申请日：2016-07-28
IPC分类号： G01N21/64 , G01N27/416
CPC分类号： G01N21/6428 , G01N21/643 , G01N21/6456 , G01N21/8851 , G01N27/4166 , G01N2021/6421 , G01N2021/6439 , G01N2201/129 , Y10T436/145555
摘要： A characteristic difference between first and second liquids is measured using a surface having a monolayer of a voltage sensitive chromophore that is covalently bound to the surface. The first liquid is brought into contact with the surface and it is irradiated with actinic radiation to measure a first fluorescence emission spectrum. The second liquid is also brought into contact with the surface and it is irradiated with actinic radiation to measure a second fluorescence emission spectrum. The first and second fluorescence emission spectra are compared to characterize a difference between the first and second fluids.
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公开(公告)号：US09718935B1
公开(公告)日：2017-08-01
申请号：US15133336
申请日：2016-04-20
IPC分类号： G03F7/027 , C08J7/16 , H01B1/12 , C08F212/14 , C08J7/04 , C08J7/12 , C08G73/02 , B05D7/04 , B05D3/06 , B05D3/10 , B05D7/00 , H05K3/02 , H05K3/10 , G03F7/20 , G03F7/32
CPC分类号： C08J7/16 , B05D3/067 , B05D3/101 , B05D7/04 , B05D7/544 , B05D7/584 , C08F12/30 , C08F212/14 , C08G73/0266 , C08J7/047 , C08J7/123 , C08J2367/02 , C08J2425/08 , C09D125/18 , G03F7/038 , G03F7/405 , H01B1/128 , H05K1/095 , H05K3/02 , H05K3/105 , H05K3/1283 , C08F2220/302 , C08F220/06
摘要： A method is used to provide an electrically-conductive polyaniline patterns on a substrate. A photocurable composition is applied as a pattern, comprising a water-soluble reactive polymer comprising (a) greater than 40 mol % of recurring units comprising sulfonic acid or sulfonate groups, (b) at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition. The pattern is exposed to radiation sufficient to cause crosslinking via [2+2] photocycloaddition of the (b) recurring units to form a pattern of crosslinked polymer. The crosslinked polymer is contacted with an aniline reactive composition comprising an aniline monomer and up to 0.5 molar of an aniline oxidizing agent, in a molar ratio of from 1:0.5 to 1:1.5 of the aniline monomer to the aniline oxidizing agent. A pattern of electrically-conductive polyaniline disposed within, on top of, or both within and on top of, the crosslinked polymer only.
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公开(公告)号：US09519219B2
公开(公告)日：2016-12-13
申请号：US14661235
申请日：2015-03-18
CPC分类号： G03F7/06 , B05D7/04 , C08F8/42 , C08K2003/0806 , C09D5/14 , C09D7/67 , C09D7/68 , C23C18/1608 , C23C18/1851 , C23C18/1889 , C23C18/1893 , C23C18/2006 , C23C18/208 , C23C18/2086 , C23C18/30 , C23C18/36 , C23C18/38 , C23C18/40 , C23C18/44 , G03F7/0388 , G03F7/20 , G03F7/40
摘要： Silver-containing compositions contain a water-soluble complex of a reactive polymer with either reducible silver ions or silver nanoparticles, the reactive polymer comprising: (a) greater than 1 mol % of recurring units comprising sulfonic acid or sulfonate groups, (b) at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally (c) at least 1 mol % of recurring units comprising a pendant amide, hydroxyl, lactam, phosphonic acid, or carboxylic acid group, all amounts based on the total recurring units in the reactive polymer. Other silver-containing compositions contain a water-insoluble complex of a reacted polymer with either reducible silver ions or silver nanoparticles. The reacted polymers are derived from the reactive polymers.
摘要翻译： 含银组合物含有反应性聚合物与可还原银离子或银纳米颗粒的水溶性络合物，反应性聚合物包含：（a）大于1mol％的包含磺酸或磺酸盐基团的重复单元，（b） 至少5摩尔％的包含能够通过[2 + 2]光环加成交联的侧基的重复单元和任选地（c）至少1摩尔％的包含酰胺，羟基，内酰胺，膦酸或羧酸的重复单元的重复单元 组，基于反应性聚合物中的总重复单元的所有量。 其它含银组合物含有反应聚合物与可还原银离子或银纳米颗粒的水不溶性络合物。 反应的聚合物衍生自反应性聚合物。
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公开(公告)号：US20160340540A1
公开(公告)日：2016-11-24
申请号：US14714422
申请日：2015-05-18
IPC分类号： C09D133/24
CPC分类号： C09D133/02 , C08F220/06 , C08F220/20 , C08F220/38 , C08F220/58 , C08K5/00 , C09D133/14 , C09D135/00 , C08F2220/382 , C08F2220/303 , C08F2220/585 , C08F212/14
摘要： A water-soluble composition includes reducible copper ions or copper nanoparticles complexed with a reactive polymer. The reactive polymer can be crosslinked using suitable irradiation to provide copper-containing water-insoluble complexes. The water-soluble composition can be used to provide various articles and electrically-conductive materials that can be assembled in electronic devices. The reactive polymer has greater than 1 mol % of recurring units comprising sulfonic acid or sulfonate groups, at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally at least 1 mol % of recurring units comprising a pendant amide, amine, hydroxyl, lactam, phosphonic acid, or carboxylic acid group.
摘要翻译： 水溶性组合物包括可还原的铜离子或与反应性聚合物络合的铜纳米颗粒。 反应性聚合物可以使用合适的照射进行交联以提供含铜的水不溶性络合物。 水溶性组合物可用于提供可组装在电子设备中的各种制品和导电材料。 反应性聚合物具有大于1摩尔％的包含磺酸或磺酸盐基团的重复单元，至少5摩尔％的包含能够通过[2 + 2]光环加成交联的侧基的重复单元和任选至少1摩尔％ 包含酰胺，胺，羟基，内酰胺，膦酸或羧酸基的重复单元。
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公开(公告)号：US20160338358A1
公开(公告)日：2016-11-24
申请号：US14714409
申请日：2015-05-18
IPC分类号： A01N59/20 , A01N25/34 , C08F226/08 , C08L33/14 , C08F228/02 , C08F222/06
CPC分类号： A01N59/20 , C08F2/48 , C08F220/38 , C08L33/14 , C08F2220/382 , C08F2220/1858 , C08F220/06 , C08F2220/1875 , C08F220/20 , C08F226/10 , C08F222/06 , A01N25/10
摘要： A water-soluble composition includes reducible copper ions or copper nanoparticles complexed with a reactive polymer. The reactive polymer can be crosslinked using suitable irradiation to provide copper-containing water-insoluble complexes. The water-soluble composition can be used to provide various articles and electrically-conductive materials that can be assembled in electronic devices. The reactive polymer has greater than 1 mol % of recurring units comprising sulfonic acid or sulfonate groups, at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally at least 1 mol % of recurring units comprising a pendant amide, amine, hydroxyl, lactam, phosphonic acid, or carboxylic acid group.
摘要翻译： 水溶性组合物包括可还原的铜离子或与反应性聚合物络合的铜纳米颗粒。 反应性聚合物可以使用合适的照射进行交联以提供含铜的水不溶性络合物。 水溶性组合物可用于提供可组装在电子设备中的各种制品和导电材料。 反应性聚合物具有大于1摩尔％的包含磺酸或磺酸盐基团的重复单元，至少5摩尔％的包含能够通过[2 + 2]光环加成交联的侧基的重复单元和任选至少1摩尔％ 包含酰胺，胺，羟基，内酰胺，膦酸或羧酸基的重复单元。
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公开(公告)号：US20190233660A1
公开(公告)日：2019-08-01
申请号：US15880830
申请日：2018-01-26
IPC分类号： C09D5/16 , C09D5/14 , C09D133/14 , C08F220/06 , C09D125/16 , C08F212/14 , C08F220/58 , C09D133/26 , C23C18/40
摘要： A water-soluble composition includes reducible copper ions or copper nanoparticles complexed with a reactive polymer. The reactive polymer can be crosslinked using suitable irradiation to provide copper-containing water-insoluble complexes. The water-soluble composition can be used to provide various articles and electrically-conductive materials that can be assembled in electronic devices. The reactive polymer has greater than 1 mol % of recurring units comprising sulfonic acid or sulfonate groups, at least 5 mol % of recurring units comprising a pendant group capable of crosslinking via [2+2] photocycloaddition, and optionally at least 1 mol % of recurring units comprising a pendant amide, amine, hydroxyl, lactam, phosphonic acid, or carboxylic acid group.
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