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公开(公告)号：US10410838B2
公开(公告)日：2019-09-10
申请号：US13318962
申请日：2010-05-06
摘要： An apparatus (9) for plasma treating multiple containers. The apparatus includes a manifold (2) comprising at least a first chamber with multiple outlet openings and multiple hollow, electrically-conductive nozzles (10) for at least one of delivering or exhausting plasma-generating gas. The multiple hollow, electrically-conductive nozzles are connected to the multiple outlet openings and protrude from the manifold. A method of plasma treating multiple containers is also disclosed. The method includes providing a reactor system comprising an apparatus disclosed herein, inserting the multiple hollow, electrically-conductive nozzles into the multiple containers (30), evacuating the multiple containers, grounding the multiple hollow, electrically-conductive nozzles while applying radio frequency power to the multiple containers, providing a gas inside the containers, and generating a plasma. At least one of evacuating or providing the gas is carried out through the hollow, electrically-conductive nozzles.
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公开(公告)号：US20120045590A1
公开(公告)日：2012-02-23
申请号：US13318962
申请日：2010-05-06
IPC分类号： C23C16/50 , C23C16/22 , C23C16/505
CPC分类号： H01J37/32394 , A61M15/009 , A61M2205/0238 , B05D1/62 , B05D3/142 , B05D5/083 , B05D7/227 , B05D2202/25 , C23C16/045 , C23C16/45578 , H01J37/32366 , H01J37/3244
摘要： An apparatus (9) for plasma treating multiple containers. The apparatus includes a manifold (2) comprising at least a first chamber with multiple outlet openings and multiple hollow, electrically-conductive nozzles (10) for at least one of delivering or exhausting plasma-generating gas. The multiple hollow, electrically-conductive nozzles are connected to the multiple outlet openings and protrude from the manifold. A method of plasma treating multiple containers is also disclosed. The method includes providing a reactor system comprising an apparatus disclosed herein, inserting the multiple hollow, electrically-conductive nozzles into the multiple containers (30), evacuating the multiple containers, grounding the multiple hollow, electrically-conductive nozzles while applying radio frequency power to the multiple containers, providing a gas inside the containers, and generating a plasma. At least one of evacuating or providing the gas is carried out through the hollow, electrically-conductive nozzles.
摘要翻译： 一种用于等离子体处理多个容器的装置（9）。 该装置包括歧管（2），其包括至少具有多个出口开口的第一室和用于输送或排出等离子体产生气体的至少一个的多个中空的导电喷嘴（10）。 多个中空的导电喷嘴连接到多个出口开口并从歧管突出。 还公开了一种等离子体处理多个容器的方法。 该方法包括提供包括本文公开的装置的反应器系统，将多个中空的导电喷嘴插入多个容器（30）中，抽空多个容器，将多个中空的导电喷嘴接地，同时施加射频功率 多个容器，在容器内提供气体，并产生等离子体。 抽空或提供气体中的至少一个通过中空的导电喷嘴进行。
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公开(公告)号：US08815325B2
公开(公告)日：2014-08-26
申请号：US13318277
申请日：2010-05-06
申请人： Moses M. David , Daniel R. Hanson , Philip A. Jinks , Christopher G. Blatchford , Vicki M. Lietzau , Jean A. Kelly , Suresh Iyer
发明人： Moses M. David , Daniel R. Hanson , Philip A. Jinks , Christopher G. Blatchford , Vicki M. Lietzau , Jean A. Kelly , Suresh Iyer
CPC分类号： C23C16/325 , A61M15/009 , Y10T428/265 , Y10T428/31663 , Y10T428/31667
摘要： A medical inhalation device or a component thereof having a diamond-like glass coating comprising hydrogen and on a hydrogen free basis about 20 to about 40 atomic percent of silicon, greater than 39 atomic percent of carbon, and less than 33 down to and including zero atomic percent of oxygen.
摘要翻译： 一种医用吸入装置或其组件，其具有包含氢并且在无氢的基础上为约20至约40原子％的硅，大于39原子％的碳，小于33的金刚石状玻璃涂层，低于和包括零 原子百分比的氧气。
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公开(公告)号：US20120103330A1
公开(公告)日：2012-05-03
申请号：US13318277
申请日：2010-05-06
申请人： Moses M. David , Daniel R. Hanson , Philip A. Jinks , Christopher G. Blatchford , Vicki M. Lietzau , Jean A. Kelly , Suresh lyer
发明人： Moses M. David , Daniel R. Hanson , Philip A. Jinks , Christopher G. Blatchford , Vicki M. Lietzau , Jean A. Kelly , Suresh lyer
CPC分类号： C23C16/325 , A61M15/009 , Y10T428/265 , Y10T428/31663 , Y10T428/31667
摘要： A medical inhalation device or a component thereof having a diamond-like glass coating comprising hydrogen and on a hydrogen free basis about 20 to about 40 atomic percent of silicon, greater than 39 atomic percent of carbon, and less than 33 down to and including zero atomic percent of oxygen.
摘要翻译： 一种医用吸入装置或其组件，其具有包含氢并且在无氢的基础上为约20至约40原子％的硅，大于39原子％的碳，小于33的金刚石状玻璃涂层，低于和包括零 原子百分比的氧气。
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公开(公告)号：US20120097159A1
公开(公告)日：2012-04-26
申请号：US13318270
申请日：2010-05-06
CPC分类号： B05D5/083 , A61M15/00 , A61M15/009 , A61M2202/064 , A61M2205/02 , A61M2205/0222 , A61M2205/0238 , B05D1/34 , B05D3/142 , B05D2350/63 , B65D83/38 , C08G65/007 , C08G65/336 , C08G77/24 , C08G77/46 , C09D183/12
摘要： A composition for modifying a surface of a substrate, the composition comprising: (a) a first polyfluoropolyether silane of the Formula Ia: CF3CF2CF2O(CF(CF3)CF2O)pCF(CF3)—C(O)NH(CH2)3Si(Y)3 wherein each Y is independently a hydrolyzable group and wherein p is 3 to 50; and (b) a second polyfluoropolyether silane of the Formula IIa: (Y′)3Si(CH2)3NHC(O)—CF2O(CF2O)m(C2F4O)qCF2-C(O)NH(CH2)3Si(Y′)3 wherein each Y′ is independently a hydrolyzable group and wherein m is 1 to 50 and q is 3 to 40. A method of making a medicinal inhalation device or a component of a medicinal inhalation device comprising a step of applying to at least a portion of a surface of the device or the component, respectively, the composition.
摘要翻译： 一种用于改性基材表面的组合物，该组合物包含：（a）式Ia的第一多氟聚醚硅烷：CF 3 CF 2 CF 2 O（CF（CF 3）CF 2 O）p CF（CF 3）-C（O）NH（CH 2）3 Si ）3，其中每个Y独立地为可水解基团，其中p为3-50; 和（b）式IIa的第二多氟聚醚硅烷：（Y'）3 Si（CH 2）3 NHC（O）-CF 2 O（CF 2 O）m（C 2 F 4 O）q CF 2 -C（O）NH（CH 2）3 Si（Y' 其中每个Y'独立地是可水解基团，并且其中m为1至50且q为3至40.制备药物吸入装置或药物吸入装置的组分的方法包括以下步骤：将至少一部分 该装置或组件的表面分别为组合物。
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6.发明申请OPTICAL DEVICE SURFACE TREATMENT PROCESS AND SMUDGE-RESISTANT ARTICLE PRODUCED THEREBY 审中-公开光学设备表面处理工艺和抗菌品生产公开(公告)号：US20130229378A1
公开(公告)日：2013-09-05
申请号：US13883368
申请日：2011-11-07
申请人： Suresh S. Iyer , Richard M. Flynn , Rama V. Rajagopal , Erik D. Olson , Karl J. Manske , Moses M. David , Jean A. Kelly
发明人： Suresh S. Iyer , Richard M. Flynn , Rama V. Rajagopal , Erik D. Olson , Karl J. Manske , Moses M. David , Jean A. Kelly
IPC分类号： G06F3/041
摘要： A surface treatment process comprises (a) providing at least one optical device; (b) providing a curable surface treatment composition comprising (1) at least one fluorinated organosilane compound comprising (i) a monovalent segment selected from polyfluoroalkyl, polyfluoroether, polyfluoropolyether, and combinations thereof and (ii) a monovalent endgroup comprising at least one silyl moiety comprising at least one group selected from hydrolyzable groups, hydroxyl, and combinations thereof, and (2) at least one fluorinated organosilane compound comprising (i) a multivalent segment selected from polyfluoroalkane, polyfluoroether, polyfluoropolyether, and combinations thereof and (ii) at least two monovalent endgroups, each independently comprising at least one silyl moiety comprising at least one group selected from hydrolyzable groups, hydroxyl, and combinations thereof; (c) applying the curable surface treatment composition to the optical device; and (d) curing the applied, curable surface treatment composition.
摘要翻译： 表面处理方法包括（a）提供至少一个光学装置; （b）提供可固化的表面处理组合物，其包含（1）至少一种氟化有机硅烷化合物，其包含（i）选自多氟烷基，多氟醚，多氟聚醚及其组合的单价链段和（ii）包含至少一个甲硅烷基部分的单价末端基 包括选自可水解基团，羟基及其组合中的至少一个基团，和（2）至少一种氟化有机硅烷化合物，其包含（i）选自多氟烷烃，多氟醚，多氟聚醚及其组合的多价链段和（ii）至少 两个单价端基，各自独立地包含至少一个含有至少一个选自可水解基团，羟基及其组合的基团的甲硅烷基部分; （c）将可固化表面处理组合物施加到光学装置上; 和（d）固化所施加的可固化表面处理组合物。
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7.发明授权Fluorinated composition, method of coating the composition, and article thereby 有权氟化组合物，涂覆组合物的方法和由此制成的制品公开(公告)号：US08664323B2
公开(公告)日：2014-03-04
申请号：US13111504
申请日：2011-05-19
申请人： Suresh S. Iyer , Richard M. Flynn , Moses M. David
发明人： Suresh S. Iyer , Richard M. Flynn , Moses M. David
IPC分类号： C09D181/02
CPC分类号： G02B1/14 , C08G77/24 , C08G77/28 , C09D4/00 , C09D183/08 , G02B1/10 , G02B1/18 , G02B27/0006
摘要： A fluorinated composition includes: a polyfluoropolyether silane represented by the formula: RfaO(CF(CF3)CF2O)pCF(CF3)CH2OZ1Si(Y1)3; and a polyfluoropolyether silane represented by the formula: Rfb[R5CH2OZ2Si(Y2)3]2 Rfa represents a perfluoroalkyl group having from 1 to 12 carbon atoms, optionally substituted with at least one catenated oxygen atom or —NR8— group, wherein R8 represents a perfluoroalkyl group; Z1 represents —R1SR2—, —R1S(═O)R2—, or —R1S(═O)2R2, wherein R1 and R2 independently represent alkylene groups having from 1 to 12 carbon atoms; each Y1 independently represents a hydrolyzable group; and p is a number in a range of from 3 to 50; Z2 independently represents —R3SR4—, —R3S(═O)R4—, or —R3S(═O)2R4, wherein R3 and R4 independently represent alkylene groups having from 1 to 12 carbon atoms; Y2 independently represents a hydrolyzable group; Rfb represents a perfluoroalkylene group having at least 3 carbon atoms, optionally substituted with at least one catenated oxygen atom or —NR6— group, wherein R6 represents a perfluoroalkyl group; R5 independently represents a covalent bond, or —(OR7)b—, and wherein R7 independently represents a branched perfluoroalkylene group, and b independently represents a number greater than or equal to one.
摘要翻译： 氟化组合物包括：由式：RfaO（CF（CF 3）CF 2 O）pCF（CF 3）CH 2 OZ 1 Si（Y 1）3表示的多氟聚醚硅烷; 和由式Rfb [R5CH2OZ2Si（Y2）3] 2表示的多氟聚醚硅烷，Rfa表示任选被至少一个连接的氧原子或-NR 8 - 基团取代的具有1至12个碳原子的全氟烷基，其中R 8表示 全氟烷基 Z1表示-R1SR2-，-R1S（= O）R2-或-R1S（= O）2R2，其中R1和R2独立地表示具有1至12个碳原子的亚烷基; 每个Y1独立地表示可水解基团; 并且p是3至50范围内的数字; Z2独立地表示-R3SR4-，-R3S（= O）R4-或-R3S（= O）2R4，其中R3和R4独立地表示具有1至12个碳原子的亚烷基; Y2独立地表示可水解基团; Rfb表示具有至少3个碳原子的全氟亚烷基，任选被至少一个连接的氧原子或-NR 6 - 基团取代，其中R 6表示全氟烷基; R5独立地表示共价键，或 - （OR7）b-，其中R7独立地表示支链全氟亚烷基，b独立地表示大于或等于1的数。
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公开(公告)号：US08444458B2
公开(公告)日：2013-05-21
申请号：US12742349
申请日：2008-12-08
CPC分类号： B24D11/00 , B24D2203/00 , Y10T428/24372
摘要： An abrasive article, such as a structured abrasive article, can be treated by subjecting it to plasma whereby the outer surface can be eroded exposing at least a portion of the abrasive particles dispersed within a cross-linked binder forming the abrasive composites. Depending on the process conditions for the plasma treatment, it is possible to erode only a small portion or substantially all of the cross-linked binder from the outer surface. Thus, the initial cut-rate of the abrasive article can be controlled since it is possible to precisely control the degree, height, or area of the exposed abrasive particles.
摘要翻译： 磨料制品，例如结构化磨料制品，可以通过使其等离子体进行处理，从而可以侵蚀外表面，使至少一部分磨料颗粒分散在形成磨料复合材料的交联粘合剂中。 根据等离子体处理的工艺条件，可能仅从外表面侵蚀少部分或基本上所有的交联粘合剂。 因此，可以控制磨料制品的初始切割速度，因为可以精确地控制暴露的磨料颗粒的程度，高度或面积。
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公开(公告)号：US20120295119A1
公开(公告)日：2012-11-22
申请号：US13497298
申请日：2010-09-17
申请人： Moses M. David
发明人： Moses M. David
IPC分类号： C23C14/06 , C23C16/40 , C23C16/30 , B32B27/06 , C23C16/26 , C23C14/24 , C23C14/35 , C23C14/04 , C23C16/50 , C23C16/32
CPC分类号： A63B53/007 , A63B53/0487 , A63B53/12 , A63B53/14 , A63B60/06 , A63B60/08 , A63B60/10 , A63B60/22 , A63B2053/005 , A63B2209/00 , A63B2209/02 , A63B2210/50 , B25G3/26 , C23C14/0641 , Y10T428/31663
摘要： A method of making a coated metal article comprises (a) forming a hardcoat layer on at least a portion of a surface of a metal or metalized substrate by physical vapor deposition; (b) forming a tie layer comprising silicon, oxygen, and hydrogen on at least a portion of the surface of the hardcoat layer by plasma deposition; and (c) applying an at least partially fluorinated composition comprising at least one silane group to at least a portion of the surface of the tie layer.
摘要翻译： 制备涂覆金属制品的方法包括（a）通过物理气相沉积在金属或金属化基材的至少一部分表面上形成硬涂层; （b）通过等离子体沉积在所述硬涂层表面的至少一部分上形成包含硅，氧和氢的粘结层; 和（c）将包含至少一个硅烷基团的至少部分氟化的组合物施加到粘结层表面的至少一部分上。
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公开(公告)号：US08241713B2
公开(公告)日：2012-08-14
申请号：US11677327
申请日：2007-02-21
IPC分类号： H05H1/24
CPC分类号： H01L51/5237 , H01L51/524 , H01L51/5253 , H01L2224/48472 , H01L2251/5338 , H01L2924/12044 , H01L2924/00
摘要： A process for fabricating an amorphous diamond-like film layer for protection of a moisture or oxygen sensitive electronic device is described. The process includes forming a plasma from silicone oil, depositing an amorphous diamond-like film layer from the plasma, andcombining the amorphous diamond-like film layer with a moisture or oxygen sensitive electronic device to form a protected electronic device. Articles including the amorphous diamond-like film layer on an organic electronic device are also disclosed.
摘要翻译： 描述了一种用于制造用于保护水分或氧气敏感的电子设备的非晶类金刚石膜层的方法。 该方法包括从硅油形成等离子体，从等离子体沉积无定形类金刚石薄膜层，以及将无定形金刚石薄膜层与水分或氧气敏感的电子器件组合以形成受保护的电子器件。 还公开了在有机电子器件上包括无定形类金刚石膜层的制品。
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