摘要:
Disclosed herein are a process for producing an epoxy adhesive auxiliary which is a liquid reclaimed from rigid polyurethane foam and an epoxy adhesive which contains the auxiliary. The epoxy adhesive auxiliary can be produced, without requiring any special apparatus for purification, by incorporating rigid polyurethane foam (200 g) in powder form (5-10 mm in size) with glycol such as polyethylene glycol (100 g) and amino alcohol such as 2-aminoethanol (5 g), and heating them at 150.degree.-280.degree. C., thereby chemically decomposing the rigid polyurethane foam into a viscous liquid. This reclaimed liquid (50-300 g) is incorporated as such into an epoxy resin adhesive base such as bisphenol A-type epoxy resin (100 g), containing optional diethylamine (6-8 g). The resulting epoxy resin adhesive is superior in tensile shear bond strength.
摘要:
An aromatic compound having sulfonyl groups, as an intermediate or raw material of polyimides having a good and well-balanced heat resistance and moldability is effectively produced by reacting a compound represented by the general formula,R--Ar--Rwherein Ar is ##STR1## Y is a bond, oxygen atom, sulfur atom, SO.sub.2, CH.sub.2 or ##STR2## and R is a hydrogen atom or --SO.sub.2 X and X is a halogen atom or alkali metal, with a compound represented by the following general formula, ##STR3## wherein X.sup.1 and X.sup.2 are simultaneously methyl groups or form ##STR4## and Z is a hydrogen atom, alkyl group having 1 to 6 carbon atoms or aryl group having 6 to 8 carbon atoms and R.sup.1 is a hydrogen atom, --SO.sub.2 X, halogen atom or nitro group, X is a halogen atom or alkali metal and R and R.sup.1 are not same simultaneously, either of which contains --SO.sub.2 X group as a necessary group.
摘要:
A polyamide resin having double bonds in its main chain and containing repeating units represented by the formula (I):[--Ar.sup.1 --CR.sup.1 .dbd.CR.sup.2 --CO--NR.sup.3 --R.sup.4 --NR.sup.3 --CO--CR.sup.2 .dbd.CR.sup.1 --] (I)wherein Ar.sup.1 is a bivalent aromatic radical, R.sup.1, R.sup.2 and R.sup.3 each independently represent a hydrogen atom, a univalent aromatic or an aliphatic radical, and R.sup.4 is a bivalent aromatic or aliphatic radical, said polyamide resin having a reduced viscosity (.eta.sp/c) of 0.1-5.0 dl/g at a concentration of 0.5 g/dl in N,N-dimethylacetamide at 30.degree. C. is prepared by reacting a bis-alkenoic amide of formula (II):CHR.sup.1 .dbd.CR.sup.2 --CO--NR.sup.3 --R.sup.4 --NR.sup.3 --CO--CR.sup.2 .dbd.CHR.sup.1 (II)wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are as defined above with an aromatic dihalide represented by formula (III):X--Ar.sup.1 --X (III)wherein Ar.sup.1 is bivalent aromatic radical and X is a halogen atom, in the presence of a palladium catalyst and a base in an organic solvent.
摘要:
A liquid crystal element comprising opposed substrates, a liquid crystal nipped between said opposed substrates, and an aligning film formed on the surface of at least one of said substrates to effect substantially horizontal alignment of the liquid crystal molecules relative to said surface, which liquid crystal element is characterized by the fact that the molecules forming said aligning film are substantially aligned in themselves.
摘要:
A capacitance humidity sensor according to the disclosure a non-conductive base plate, electrodes oppositely arranged on the base plate, a metal compound membrane formed by ion-plating independently on the electrodes, the metal compound membrane being roughened on its surface by plasma etching and being active to the humidity, and a moisture permeable metal skin formed on the metal compound membrane. The metal compound is preferably an oxide or nitride of aluminum or magnesium.
摘要:
The present invention is to provide a liquid crystal monomeric compound where a liquid crystal phase readily appears, which is excellent in alignment control, film-formability, durability, heat-stability and compatibility, and is able to be applied to electro-optical liquid crystal elements and recording elements; and a side-chain liquid crystal polymer compound modified with such a monomeric compound.The liquid crystal monomeric compound is represented by the following formula:CH.sub.2 .dbd.CH--(CH.sub.2).sub.m --R [1]wherein m is an integer of 2 to 20 and R is a group selected from the group consisting of ##STR1## wherein p is 1 or 2, Rf is CF.sub.3 or CF.sub.2 F.sub.5, R.sup.1 is an alkyl group having 3-18 carbon atoms, * means an optically active carbon atom, (A) and (B) each is a group independently selected from the group consisting of ##STR2## which may be substituted with one or more halogen atoms, and X is --O--, --COO--or a direct linkage, and ##STR3## wherein p, Rf, R.sup.1, (A), (B), X and * have the same meanings as above.
摘要翻译:本发明提供一种容易出现液晶相的液晶单体化合物,其取向控制,成膜性,耐久性,热稳定性和相容性优异,能够应用于电光液晶 元素和记录元素; 和用这种单体化合物改性的侧链液晶高分子化合物。 液晶单体化合物由下式表示:CH 2 = CH-(CH 2)m R [1]其中m为2至20的整数,R为选自下组的基团:其中p 是1或2,Rf是CF 3或CF 2 F 5,R 1是具有3-18个碳原子的烷基,*表示光学活性碳原子,(A)和(B)各自独立地选自 其中p,R f,R 1,(A),(B),X和*具有相同的基团,X是-O-,-COO-或直链, 意义如上。
摘要:
A memory card having a printed circuit board mounted with semiconductor elements and provided with terminal portions along one side thereof and a card basic board formed with a broad recess on the lower surface thereof for receiving said printed circuit board therein. Void contact spaces are provided along one side thereof. The card basic board is formed with upper openings for communicating with the contact spaces on the upper surface of the card basic board and with inserting ports for communicating with the contact spaces on a side surface of the card basic board. Upper beams are provided between the upper openings and the corresponding inserting ports, and lower beams are provided near the inserting ports.
摘要:
An aromatic polythiazole is produced from a salt of an aromatic diaminodithiol compound and a dicarboxylic acid derivative, by a method comprising the steps of: (a) reacting the aromatic diaminodithiol compound salt with an alkyl halide having a substituted or unsubstituted alkyl group in an alkaline aqueous solvent, so that hydrogen atoms in thiol groups of the aromatic diaminodithiol compound are substituted with the alkyl groups; (b) polymerizing the resulting alkyl group-substituted aromatic diaminodithiol compound with the dicarboxylic acid derivative to form an aromatic polythiazole prepolymer; and (c) heating the aromatic polythiazole prepolymer to cause a thiazole ring closure reaction, thereby producing the aromatic polythiazole. By this method, the amino groups of the aromatic diaminodithiol compound salt are selectively reacted with the dicarboxylic acid derivative.
摘要:
A heating furnace for semiconductor wafers having a heater arranged around a core tube, layers of a heat insulating material made of a porous heat insulating material or ceramic fibers arranged around the heater, and layers of a heat reflecting material arranged in the layers of the heat insulating material.
摘要:
A process for manufacturing an aromatic polyester resin represented by the general formula: ##STR1## wherein Ar.sup.1 and Ar.sup.2 represent a bivalent aromatic radical and n is an integer of 10 to 100, comprising reacting an aromatic diol represented by the general formula:HO-Ar.sup.1 -OHwherein Ar.sup.1 is a bivalent aromatic radical with a bivalent dibromide represented by the general formula:Br-Ar.sup.2 -Brwhere Ar.sup.2 is a bivalent radical and with carbon monoxide in the presence of a palladium catalyst and an organic base in an organic solvent.