摘要:
Monocyclometalated Au(III) complexes, cis-[(N̂C)AuL1L2] and cis-[(N̂C)Au L1̂L2] represented by generic chemical formulae 1a and 1b respectively with ligands L1 and L2 being either similar (L1=L2) or dissimilar (L1≠L2) but with at least one of either (L1 or L2) comprising a σ-donating carbanionic group is described here. Also described are Au(III) complexes of formula in which L3 denotes a neutral donor ligand bound in a tridentate fashion. The complexes depicted by the formulae 1a, 1b and 1c in the present invention are suitable as emissive phosphorescent organometallic materials in OLEDs.
摘要:
The present invention provides a method for preparing colorless sucralose, wherein 4,1′,6′-trichloro-4,1′,6′-trideoxy-galactosucrose-6-acetate containing colored impurities formed during chlorination of sucrose-6-acetate is treated with sodium hypochlorite, where sodium hypochlorite acts both as a decolorizing agent and as a reagent for the ester hydrolysis.
摘要:
A process for (R,S)-nicotine is described. Condensation of 1-(but-1-enyl)pyrrolidin-2-one with nicotinic acid ester gave 1-(but-1-enyl)-3-nicotinoylpyrrolidin-2-one which on treatment with an acid and a base gave myosmine. Myosmine was converted to (R,S)-nicotine by reduction followed by N-methylation.
摘要:
A process for (R,S)-nicotine is described. Condensation of 1-(but-1-enyl)pyrrolidin-2-one with nicotinic acid ester gave 1-(but-1-enyl)-3-nicotinoylpyrrolidin-2-one which on treatment with an acid and a base gave myosmine. Myosmine was converted to (R,S)-nicotine by reduction followed by N-methylation.
摘要:
(R,S)-Nicotine was resolved through diastereomeric salt formation using dibenzoyl-d-tartaric acid and dibenzoyl-l-tartaric acid to obtain enantiomerically pure (S)-nicotine and (R)-nicotine.
摘要:
The present invention relates to a process for preparation of Dronedarone or pharmaceutically acceptable salts thereof. More particularly, the present invention provides a process for preparation of Dronedarone hydrochloride, without the isolation of Dronedarone base.
摘要:
A player decodes and renders encoded digital data received from an encoder. During processing, the player periodically monitors dropped frames as well as time spent. If the dropped frames are below a minimum, the player determines to signal the encoder to increase bit rate or frame rate by consulting a table. If the player determines to increase bit rate, the player signals accordingly. However, if the player determines to increase frame rate, the player first verifies that the spent time is below a minimum. To the contrary, if the dropped frames are both above the minimum and a first maximum but nota second maximum, the player determines to signal the encoder to decrease bit rate or frame rate by consulting the table and signaling accordingly. However, if the dropped frames are above the second maximum, the player signals the encoder to decrease the frame rate without consulting the table.
摘要:
The present invention relates to a process for the preparation of 2-butyl-3-[[2′-(1H-tetrazol-5-yl)[1,1′-biphenyl]-4-yl]-1,3-diazaspiro[4,4]non-1-en-4-one by reaction of the corresponding nitrile with sodium azide and piperazine or its acid salt.
摘要:
Exemplary embodiments of the present disclosure are directed towards a physiologically acceptable visualisable contrast medium for the diagnosis of patency of conduits and method of its preparation comprising of an active ingredient comprising of a local anesthetic, whereby the active ingredient incorporated is 2% weight by weight of lidocaine hydrochloride; a sterile mixture comprising of sodium chloride and water, whereby the strength of the sodium chloride incorporated is 0.9% weight by volume in a solution of water.
摘要:
The present invention relates to polymer composite materials, more particularly relates to composite materials with tailor made surface electrical resistivities in the range of 109 to 10−1 Ω/sq. and process of making the same. The process for preparing Fiber Reinforced Polymeric (FRP) Composite, said process comprising acts of homogeneously mixing 1-30% by weight of different electrically conducting fillers in matrix resin system to obtain resin mix; wetting dry preforms using the resin mix; compacting the wetted preforms to obtain green composite; curing the green composite; and post-curing the cured composite to prepare the FRP Composite.