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    Process for Regasifying a Gas Hydrate Slurry
    1.
    发明申请
    Process for Regasifying a Gas Hydrate Slurry 失效
    再生天然气水合物浆料的工艺

    公开(公告)号：US20090230025A1

    公开(公告)日：2009-09-17

    申请号：US12085965

    申请日：2006-11-22

    申请人： Carl Boles Argo ,  Roger Neil Harper ,  David Charles King ,  Michael Bernard Power ,  Peter Willcox

    发明人： Carl Boles Argo ,  Roger Neil Harper ,  David Charles King ,  Michael Bernard Power ,  Peter Willcox

    IPC分类号： C10G33/00

    CPC分类号： F17D1/05 ,  F17C7/04 ,  F17C2221/036 ,  F17C2223/0153 ,  F17C2223/033 ,  F17C2225/0123 ,  F17C2225/036 ,  F17C2227/0135 ,  F17C2227/0157 ,  F17C2227/0306 ,  F17C2227/0311 ,  F17C2227/0327 ,  F17C2227/0339 ,  F17C2227/0388 ,  F17C2265/015 ,  F17C2265/05 ,  F17C2270/0123 ,  F17C2270/0136 ,  F17D3/14

    摘要： A continuous process for regasifying a feed stream comprising (i) a slurry phase comprising gas hydrate particles suspended in a produced liquid hydrocarbon and optionally free produced water and (ii) optionally a gaseous phase comprising free produced gaseous hydrocarbon thereby generating a regasified multiphase fluid and for separating the regasified multiphase fluid into its component fluids, comprising the steps of: (a) heating the feed stream to above the dissociation temperature of the gas hydrate thereby regasifying the feed stream by converting the gas hydrate particles into gaseous hydrocarbon and water; (b) separating a gaseous hydrocarbon phase from the regasified multiphase fluid thereby forming a gaseous hydrocarbon product stream and a liquid stream comprising a mixture of liquid hydrocarbon and water; (c) separating the liquid stream comprising a mixture of the liquid hydrocarbon and water into a liquid hydrocarbon phase and an aqueous phase; and (d) removing the liquid hydrocarbon phase as a liquid hydrocarbon product stream.

    摘要翻译： 一种用于再气化进料流的连续方法，其包括（i）包含悬浮在所生产的液体烃和任选的游离生成水中的气体水合物颗粒的淤浆相和（ii）任选的包含游离产生的气态烃的气相，从而产生再溶解的多相流体， 用于将再分散的多相流体分离成其组分流体，包括以下步骤：（a）将进料流加热至高于气体水合物的解离温度，从而通过将气体水合物颗粒转化为气态烃和水来再气化进料流; （b）从再分散的多相流体中分离出气态烃相，从而形成气态烃产物流和包含液态烃和水的混合物的液体流; （c）将包含液态烃和水的混合物的液体流分离成液态烃相和水相; 和（d）作为液态烃产物流除去液态烃相。

    Degassing process
    2.
    发明授权
    Degassing process 失效
    脱气过程

    公开(公告)号：US07582710B2

    公开(公告)日：2009-09-01

    申请号：US10485222

    申请日：2002-07-15

    申请人： Andrew David Bell ,  David Andrew Fargie ,  David Edward Noble ,  Michael Bernard Power ,  Iain David Ross

    发明人： Andrew David Bell ,  David Andrew Fargie ,  David Edward Noble ,  Michael Bernard Power ,  Iain David Ross

    IPC分类号： C08F2/00 ,  C08F210/00

    CPC分类号： C08F6/001 ,  C08F10/00 ,  C08F210/16 ,  Y10S526/901 ,  C08L23/00 ,  C08F2/34 ,  C08F210/14

    摘要： An improved process for the polymerization of olefin monomer selected from (a) ethylene, (b) propylene, (c) mixtures of ethylene and propylene and (d) mixtures of (a), (b) or (c) with one or more alpha-olefins in a fluidized bed gas phase reactor, said process comprising passing a gaseous mixture of said olefin monomers(s) through the fluidized bed under effective polymerization conditions to provide a polymer product containing unreacted monomer(s) and a gaseous effluent stream comprising unreacted monomer(s), removing the polymer product to a degassing vessel, recycling a first portion of the gaseous effluent stream to the fluidized bed and passing a second portion of the gaseous effluent stream to counter currently contact the polymer product in said degassing vessel to produce a polymer product having a reduced amount of unreacted monomer(s), characterized in that the improvements to the process comprise: (i) removing heavy hydrocarbons from the second portion of the effluent stream and returning said hydrocarbons to the first portion of the effluent stream for recycle to the fluidized bed, (ii) removing substantially all of the monomer(s) from the second portion of the effluent stream and returning said monomers(s) to the first portion of the effluent stream for recycle to the fluidized bed, and (iii) recycling the second effluent stream after passage through the degassing vessel to the gaseous effluent stream.

    摘要翻译： 选自（a）乙烯，（b）丙烯，（c）乙烯和丙烯的混合物和（d）（a），（b）或（c）与一种或多种的混合物的烯烃单体的聚合的改进方法 α-烯烃在流化床气相反应器中，所述方法包括在有效聚合条件下使所述烯烃单体的气态混合物通过流化床，以提供含有未反应单体的聚合物产物和包含 将未反应的单体除去聚合物产物至脱气容器，将第一部分气态流出物料流再循环到流化床中，并将第二部分气态流出物流转移至目前与所述脱气容器中的聚合物产物接触， 产生具有减少量的未反应单体的聚合物产物，其特征在于该方法的改进包括：（i）从流出物流的第二部分除去重质烃 并将所述烃返回到流出物流的第一部分以再循环到流化床，（ii）从流出物流的第二部分基本上除去所有单体，并将所述单体返回到第一 流出物流的一部分用于再循环到流化床，和（iii）在通过脱气容器之后再循环第二流出物流至气态流出物流。

    Process for polymerising olefin in gas phase
    3.
    发明授权
    Process for polymerising olefin in gas phase 失效
    在气相中聚合烯烃的方法

    公开(公告)号：US5789501A

    公开(公告)日：1998-08-04

    申请号：US782261

    申请日：1997-01-15

    申请人： Geoffrey Chapman ,  Stephen Kevin Lee ,  Michael Bernard Power ,  Bruno Grenouiller

    发明人： Geoffrey Chapman ,  Stephen Kevin Lee ,  Michael Bernard Power ,  Bruno Grenouiller

    IPC分类号： C08F2/34 ,  C08F6/00 ,  C08F6/02 ,  C08F10/02

    CPC分类号： C08F6/02 ,  C08F10/02 ,  C08F6/005

    摘要： The present invention relates to a process for continuously manufacturing ethylene (co-)polymer in a gaseous phase in a polymerization zone through which passes an essentially gaseous reaction mixture comprising the (co-)monomers(s). In addition the process comprises transferring a mixture (A) formed by the gaseous reaction mixture and the solid (co-)polymer in a depressurization zone, and separating the mixture (A) into a solid phase (B) and a gaseous phase (C) returned into the polymerization zone. The solid phase (B) is subjected to (1) at least one non-deactivating flushing with respect to the active catalytic residues, and subsequently (2) a deactivating flushing with a gaseous mixture of nitrogen, water and oxygen. The (co-)polymer thus obtained has very low contents of unreacted (co-)monomer(s) and volatile organic compounds, and exhibits a high whiteness index and a long thermal stability with time.

    摘要翻译： 本发明涉及一种在聚合区中气相中连续制造乙烯（共）聚合物的方法，通过该方法通过包含（共）单体的基本上气态的反应混合物。 此外，该方法包括在减压区中转移由气态反应混合物形成的混合物（A）和固体（共）聚合物，并将混合物（A）分离成固相（B）和气相（C ）返回聚合区。 相对于活性催化剂残余物，固相（B）进行（1）至少一种非钝化冲洗，随后（2）用氮气，水和氧气的气态混合物进行钝化冲洗。 由此获得的（共）聚合物具有非常低的未反应（共）单体和挥发性有机化合物的含量，并且表现出高的白度指数和长时间的热稳定性。

    Gas fluidized bed polymerization process for olefins
    4.
    发明授权
    Gas fluidized bed polymerization process for olefins 失效
    烯烃气体流化床聚合方法

    公开(公告)号：US06225422B1

    公开(公告)日：2001-05-01

    申请号：US08907875

    申请日：1997-08-11

    申请人： Michael Bernard Power ,  Jean-Claude Chinh

    发明人： Michael Bernard Power ,  Jean-Claude Chinh

    IPC分类号： C08F234

    CPC分类号： C08F10/00 ,  C08F2/34

    摘要： A process for the continuous gas fluidised bed polymerisation of olefins, especially ethylene, propylene, or mixtures of these with other alpha olefins, wherein the monomer containing recycle gas employed to fluidise the bed is passed through a separator. The separator is charged with and maintained at least partially filled with liquid. Entrained catalyst and/or polymer particles are separated from the recycle gas in the separator and these separated particles are maintained in a suspended state in the liquid in the separator. The recycle stream can be cooled to condense out at least some liquid hydrocarbon; the condensed liquid, which can be a monomer or an inert liquid, is separated from the recycle gas in the separator and is fed directly to the bed to produce cooling by latent heat of evaporation. The process reduces fouling of the separator.

    摘要翻译： 用于烯烃，特别是乙烯，丙烯或它们与其它α-烯烃的混合物的连续气体流化床聚合的方法，其中用于流化床的含单体的循环气体通过分离器。 分离器装满并保持至少部分填充有液体。 夹带的催化剂和/或聚合物颗粒与分离器中的再循环气体分离，并且这些分离的颗粒在分离器中的液体中保持悬浮状态。 再循环物流可冷却至少一些液态烃; 可以将单体或惰性液体的冷凝液从分离器中的再循环气体中分离出来，并直接送入床中，以通过蒸发潜热产生冷却。 该过程减少了分离器的结垢。

    Process for regasifying a gas hydrate slurry
    5.
    发明授权
    Process for regasifying a gas hydrate slurry 失效
    再生气体水合物浆料的方法

    公开(公告)号：US08008533B2

    公开(公告)日：2011-08-30

    申请号：US12085965

    申请日：2006-11-22

    申请人： Carl Boles Argo ,  Roger Neil Harper ,  David Charles King ,  Michael Bernard Power ,  Peter Willcox

    发明人： Carl Boles Argo ,  Roger Neil Harper ,  David Charles King ,  Michael Bernard Power ,  Peter Willcox

    IPC分类号： C10G33/00

    CPC分类号： F17D1/05 ,  F17C7/04 ,  F17C2221/036 ,  F17C2223/0153 ,  F17C2223/033 ,  F17C2225/0123 ,  F17C2225/036 ,  F17C2227/0135 ,  F17C2227/0157 ,  F17C2227/0306 ,  F17C2227/0311 ,  F17C2227/0327 ,  F17C2227/0339 ,  F17C2227/0388 ,  F17C2265/015 ,  F17C2265/05 ,  F17C2270/0123 ,  F17C2270/0136 ,  F17D3/14

    摘要： Continuous process for regasifying a feed stream having (i) a slurry phase comprising gas hydrate particles suspended in a produced liquid hydrocarbon and optionally free produced water and (ii) optionally a gaseous phase comprising free produced gaseous hydrocarbon thereby generating a regasified multiphase fluid and for separating the regasified multiphase fluid into its component fluids. The method includes (a) heating the feed stream to above the dissociation temperature of the gas hydrate thereby regasifying the feed stream by converting the gas hydrate particles into gaseous hydrocarbon and water, (b) separating a gaseous hydrocarbon phase from the regasified multiphase fluid thereby forming a gaseous hydrocarbon product stream and a liquid stream comprising a mixture of liquid hydrocarbon and water, (c) separating the liquid stream comprising a mixture of the liquid hydrocarbon and water into a liquid hydrocarbon phase and an aqueous phase; and (d) removing the liquid hydrocarbon phase as a liquid hydrocarbon product stream. The regasification production facility additionally has a concentrator vessel and the feed stream is passed to the concentrator vessel prior to being heated in step (a) to above the dissociation temperature of the gas hydrate particles wherein a gaseous phase comprising free gaseous hydrocarbon separates from the feed stream in the concentrator vessel and is removed from the concentrator as a gaseous hydrocarbon stream.

    摘要翻译： 用于再气化进料流的连续方法，其具有（i）包含悬浮在所生产的液体烃中的气体水合物颗粒和任选的游离生成水的浆料相和（ii）任选的包含游离产生的气态烃的气相，从而产生再分散的多相流体， 将再分散的多相流体分离成其组分流体。 该方法包括（a）将进料流加热至高于气体水合物的解离温度，从而通过将气体水合物颗粒转化为气态烃和水来再气化进料流，（b）从再分散的多相流体中分离气态烃相，从而 形成气态烃产物流和包含液体烃和水的混合物的液体流，（c）将包含液体烃和水的混合物的液体流分离成液态烃相和水相; 和（d）作为液态烃产物流除去液态烃相。 再气化生产设备另外具有浓缩器容器，并且在步骤（a）中被加热之前，将进料流送至浓缩器容器，使其高于气体水合物颗粒的解离温度，其中包含游离气态烃的气相与进料分离 在浓缩器容器中流动并且作为气态烃流从浓缩器中除去。

    Nozzle for atomizing a fluid in a fluidized bed
    6.
    发明授权
    Nozzle for atomizing a fluid in a fluidized bed 失效
    用于在流化床中雾化流体的喷嘴

    公开(公告)号：US06214943B1

    公开(公告)日：2001-04-10

    申请号：US09299884

    申请日：1999-04-27

    申请人： David Newton ,  Michael Bernard Power

    发明人： David Newton ,  Michael Bernard Power

    IPC分类号： C08F234

    CPC分类号： B01J8/1827 ,  B01J19/26 ,  B01J2208/00061 ,  B01J2208/00256 ,  B01J2208/00274 ,  B01J2208/00362 ,  B01J2208/00548 ,  B01J2208/0061 ,  B05B1/14 ,  B05B1/265 ,  B05B1/267 ,  B05B1/341 ,  B05B7/0458 ,  B05B7/08 ,  C08F10/00 ,  Y10S526/901 ,  C08F2/34 ,  C08F2/01

    摘要： A continuous gas fluidized bed process for the polymerization of olefins, especially ethylene, propylene, or mixtures thereof with other alpha-olefins by cooling the recycle gas stream to condense some liquid (e.g., a comonomer), separating at least part of the liquid and spraying it under pressure through a nozzle (1) directly into the fluidized bed by pressurizing the liquid and feeding it to a spray nozzle (1) having a mechanical device (6) for atomizing the liquid, under conditions such that the spray is formed within a spray-forming zone (5) of the nozzle outlet. The spray-forming zone (5) is preferably shielded from the fluidized bed particles by a wall or walls which can be, for example, a tube or a plate. Also described is a nozzle having two or more series of outlets, each series being fed and controlled independently to enable improved turn-up/turn-down of the liquid supply to the bed.

    摘要翻译： 一种连续气体流化床方法，用于通过冷却循环气流以使某些液体（例如共聚单体）冷凝，将至少部分液体分离出来，使烯烃，特别是乙烯，丙烯或其混合物与其它α-烯烃聚合， 在压力下通过喷嘴（1）将其喷射到流化床中，通过加压液体并将其输送到具有用于使液体雾化的机械装置（6）的喷嘴（1），使得在 喷嘴出口的喷雾形成区（5）。 喷雾形成区（5）优选通过可以是例如管或板的壁或壁来防止流化床颗粒。 还描述了具有两个或更多个系列出口的喷嘴，每个系列被独立地进给和控制，以使得能够改善液体供应到床的向上/向下。

    Fluidized bed polymerization reactor
    8.
    发明授权
    Fluidized bed polymerization reactor 失效
    流化床聚合反应器

    公开(公告)号：US5733510A

    公开(公告)日：1998-03-31

    申请号：US602013

    申请日：1996-02-15

    申请人： Jean-Claude Chinh ,  Michel C. H. Filippelli ,  David Newton ,  Michael Bernard Power

    发明人： Jean-Claude Chinh ,  Michel C. H. Filippelli ,  David Newton ,  Michael Bernard Power

    IPC分类号： C08F10/02 ,  B01J8/18 ,  B01J8/24 ,  B01J19/26 ,  B05B7/04 ,  B05B7/08 ,  C08F2/34 ,  C08F10/00 ,  C08F10/06 ,  C08F210/16

    CPC分类号： B01J8/1809 ,  B01J19/26 ,  B01J8/1827 ,  B01J8/1836 ,  B05B7/0433 ,  B05B7/08 ,  C08F10/00 ,  B01J2208/00061 ,  B01J2208/00088 ,  B01J2208/00256 ,  B01J2208/00274 ,  B01J2208/00362 ,  B01J2208/00539 ,  B01J2208/00548 ,  B01J2219/00119 ,  B01J2219/00128 ,  Y10S526/901

    摘要： A fluidized bed polymerization reactor which is a generally cylindrical vessel having a longitudinal axis and a fluidization grid located in the vessel generally perpendicular to the longitudinal axis of the vessel and defining a fluidized bed region above the fluidization grid. The reactor has an inlet for continuously introducing a gaseous stream of polymerizable monomers into the vessel below the fluidization grid at a gas velocity sufficient to maintain particles in the fluidized bed region in a suspended and fluidized condition; an outlet for removing polymer product from the fluidized bed region and an outlet for continuously removing an outlet stream of gaseous unreacted polymerizable monomer from the fluidized bed region. A cooling device cools at least a part of the outlet stream to a temperature at which liquid condenses out of the outlet stream, and a separating device separates at least a part of the cooled outlet stream into condensed liquid and a cooled gaseous stream. The separated cooled gaseous stream is returned to the inlet and an injection device injects at least a part of the condensed liquid into the fluidized bed region at a point where the gaseous stream of polymerizable monomers passing through the vessel has substantially reached the operating temperature of the polymerization reactor. The injection device includes at least one gas induced atomizing nozzle for injecting an atomized stream of the condensed liquid into the fluidized bed region in a direction generally perpendicular to the longitudinal axis of the vessel.

    摘要翻译： 一种流化床聚合反应器，其是通常为圆柱形的容器，其具有纵向轴线和位于容器中的流化格栅，其大致垂直于容器的纵向轴线并且在流化网格上方限定流化床区域。 反应器具有入口，用于以足以将流化床区域中的颗粒保持在悬浮和流化状态的气体速度将可聚合单体的气态流连续引入容器中; 用于从流化床区域除去聚合物产物的出口和用于从流化床区域连续地除去气态未反应的可聚合单体的出口流的出口。 冷却装置将出口流的至少一部分冷却至液体从出口流冷凝的温度，并且分离装置将冷却的出口物流的至少一部分分离成冷凝的液体和冷却的气态物流。 分离的冷却的气流返回到入口，注射装置将至少一部分冷凝的液体注入到流化床区域中，其中通过容器的可聚合单体的气态流基本达到 聚合反应器。 注射装置包括至少一个气体诱导的雾化喷嘴，用于将冷凝的液体的雾化流在大致垂直于容器的纵向轴线的方向上喷射到流化床区域中。